Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 61| Part 3

ISSN: 2056-9890

March 2005 issue

Highlighted illustration

Cover illustration: In this N-imidazole-boron trichloride adduct, the B-N bond length of 1.543 (3) Å is one of the shortest on record. See Baber, Bull, Charmant, Norman & Orpen [Acta Cryst. (2005), E61, o553-o554].

inorganic compounds

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K₄Ta₄P₄S₂₄

A. Gutzmann, C. Näther and W. Bensch

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Eu_1.8La_0.2BaZnO₅: a Rietveld refinement using X-ray powder diffraction

J. A. Hernández-Pérez, M.-E. Villafuerte-Castrejón and L. Bucio

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Dipotassium sodium hexacyanocobalt(III)

A. B. Ilyukhin and V. Y. Kotov

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A lanthanum(III) complex with a lacunary polyoxotungstate: Na₂(NH₄)₇[La(W₅O₁₈)₂]·16H₂O

F. A. Almeida Paz, M. S. S. Balula, A. M. V. Cavaleiro, J. Klinowski and H. I. S. Nogueira

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Synthesis, crystal structure and vibrational spectra of a new diammonium zinc(II) dihydrogendiphosphate dihydrate, (NH₄)₂Zn(H₂P₂O₇)₂·2H₂O

R. Essehli, M. Lachkar, I. Svoboda, H. Fuess and B. El Bali

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K₆H₂[TiW₁₁CoO₄₀]·13H₂O, with a monotitanoundecatungstocobaltate(II) anion

W. Kraus, H. Stephan, A. Röllich, Z. Mate˘jka and G. Reck

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Ammonium chlorite, NH₄ClO₂, at 150 K

A. I. Smolentsev and D. Y. Naumov

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Cerium(III) hydroxide sulfate, Ce(OH)SO₄

Y. Yang, L.-H. Zhu, M.-H. Zeng and X.-L. Feng

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Trirubidium cobalt tetrachloride nitrate(V), Rb₃CoCl₄NO₃

R. Ouarsal, M. Lachkar, M. Bolte and B. El Bali

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metal-organic compounds

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Chloro[N,N′-dimethyl-N,N′-bis(2-pyridylmethyl)ethane-1,2-diamine]oxovanadium(IV) perchlorate

R. K. Egdal, A. D. Bond and C. J. McKenzie

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Butane-1,4-diammonium diphosphopentamolybdate: a new inorganic–organic hybrid solid

S. Upreti and A. Ramanan

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catena-Poly[[[tetraaqua(3-carboxy-4-hydroxybenzenesulfonato)strontium(II)]-μ₃-3-carboxy-4-hydroxybenzenesulfonato] dihydrate]

S. Gao, L.-H. Huo, Z.-B. Zhu and J.-R. Li

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catena-Poly[[aquadicinnamatocadmium]-μ-1,4-diazabicyclo[2.2.2]octane]

Y. Qu, Z.-D. Liu, M.-Y. Tan and H.-L. Zhu

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trans-Bis[4-(4-methylphenyl)-3,5-di-2-pyridyl-4H-1,2,4-triazole]diperchlorato-κ²O-copper(II)

S.-P. Zhang, Z.-D. Liu, J.-L. Ma, S. Yang and S.-C. Shao

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Diisothiocyanatobis(2-methyl-1H-imidazole)cobalt(II)

F.-Q. Liu, F.-F. Jian, L.-D. Lu, X.-J. Yang, X. Wang and H.-L. Xiao

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Chloro[2-(2,2′-bipyridyl-6-yl)-5-methylphenyl]platinum(II)

Q.-Y. Cao, W.-F. Fu and X.-J. Zhao

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Bis(1,1,1,5,5,5-hexafluoroacetylacetonato-κ²O,O′)bis(tetrahydrofuran-κN)iron(II)

K. E. Preuss, J. Wu and M. Jennings

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Bis(μ-5-chloro-2-hydroxyacetophenone 4-nitrobenzoylhydrazonato)bis[dipyridinecadmium(II)]

H. M. Ali, N. F. Kamalul Aripin and S. W. Ng

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catena-Poly[[cis-diaqua(2,2′-bipyridine)cobalt(II)]-μ-3-carboxylato-4-hydroxybenzenesulfonato]

S.-R. Fan, L.-G. Zhu, H.-P. Xiao and S. W. Ng

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Tris{trans-4-[p-(N,N-diethylamino)styryl]-N-methylpyridinium} dodecatungstophosphate

X.-J. Tan, S.-X. Sun, S.-L. Liu, J.-P. Ma and D.-X. Xing

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(Nitrato-κO)(1,10-phenanthroline-κ²N,N′)(picolinato N-oxide-κ²O,O′)copper(II)

L. Gou, X.-W. Qu, B. Zheng, D.-Y. Wang and H.-M. Hu

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Bis(μ-4-bromoisophthalato)bis[bis(1,10-phenanthroline)manganese(II)] tetrahydrate

H.-P. Xiao, M.-L. Hu and J.-X. Yuan

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Aqua{2-[(E)-(3,5-dibromo-2-oxidophenyl)methyleneamino]ethanesulfonato-κ³O,N,O′}(1,10-phenanthroline-κ²N,N′)nickel(II) ethanol solvate

S.-H. Zhang, Y.-M. Jiang, Z. Liu and K.-B. Yu

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Hexaaquazinc(II) naphthalene-1,5-disulfonate

L.-H. Huo, S. Gao, S.-X. Xu and H. Zhao

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catena-Poly[[diaquacadmium(II)]-μ-benzene-1,4-dioxyacetato-κ⁴O,O′:O′′,O′′′]

S. Gao, J.-W. Liu, L.-H. Huo and H. Zhao

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Bis[μ-1-(2-pyridyl-κN)ethanone 4-phenylthiosemicarbazonato-κ²N¹,S]bis[iodomercury(II)]

B. M. Yamin and M. S. M. Yusof

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(4-tert-Butylphenyl)phospha[1]ferrocenophane

P. W. Cyr, A. J. Lough and I. Manners

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catena-Poly[[diaqua[3-(2-pyridyl)-1H-pyrazole-κN²]cadmium(II)]-μ-squarato-κ²O:O′]

L.-H. Huo, X. L. Cheng, H. Zhao and S. W. Ng

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[μ₈-η⁴-2,5-Bis(oct-1-ynyl)thiophene]bis[octacarbonylbis(η⁵-methylcyclopentadienyl)-tetrahedro-diiridiumdimolybdenum] dichloromethane hemisolvate

N. T. Lucas, M. G. Humphrey and A. C. Willis

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Bis(3-tert-butyl-N,5-dimethylsalicylaldiminato)cobalt(II)

X. Li, L. Huang, S. Dong, M. Li and H. Sun

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mer-(2-Formylatocyclohexen-1-olato-κ²C²,O¹)iodotris(trimethylphosphine-κP)cobalt(III)

F. Yu, S. Dong, J. Zhou, A. Wang, H. Sun and X. Li

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catena-Poly[[(2,2′-bipyridine)nickel(II)]-μ-4,4′-oxydibenzoato]

H.-P. Xiao, Y.-Q. Cheng and X.-H. Li

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Tris(phenanthroline-κ²N,N′)nickel(II) dibromosuccinate heptahydrate

D.-X. Li, D.-J. Xu and Y.-Z. Xu

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catena-Poly[[[diaquahexapyridine-μ-sulfato-dicobalt(II)]-μ-sulfato] tetrahydrate]

H. M. Ali, S. Puvaneswary and S. W. Ng

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catena-Poly[[tetrapyridinecopper(II)]-μ₂-naphthalene-1,5-disulfonato]

S. Gao, L.-H. Huo, Z.-B. Zhu and S. W. Ng

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Acetato(methanol)[N-phenyl-N,N-bis(2-pyridylmethyl)amine]copper(II) hexafluorophosphate

A. Nielsen, A. D. Bond and C. J. McKenzie

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Tris(pyridine-2-carboxylato-κ²O,N)cobalt(III) monohydrate

A.-Y. Fu and D.-Q. Wang

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Poly[[[(2,2′-bipyridine)copper(II)]-hemi-μ₂-2-nitroterephthalato-hemi-μ₄-2-nitroterephthalato] monohydrate]

A.-Q. Ma, L.-G. Zhu and S. W. Ng

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Diaquabis(2,5-di-3-pyridyl-1,3,4-oxadiazole)dithiocyanatomanganese(II): a three-dimensional supramolecular network formed through O—H⋯N and C—H⋯S interactions

M. Du, X.-J. Jiang and X.-J. Zhao

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Azido(2,2′-bipyridine)(η⁵-pentamethylcyclopentadienyl)iridium(III) hexafluorophosphate

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catena-Poly[N-methylpiperazinium(2+) [[bis(oxalato-κ²O,O′)zirconate(IV)]-μ₂-oxalato-κ⁴O,O′:O′′,O′′′]]

Y.-L. Fu, J.-L. Ren and S. W. Ng

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catena-Poly[[bis(1H-benzimidazole-κN³)zinc(II)]-μ-3-carboxyphenoxyacetato-κ²O:O′]

S. Gao, L.-H. Huo, J.-W. Liu and C.-S. Gu

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catena-Poly[[aqua(1,10-phenanthroline-κ²N,N′)cobalt(II)]-μ-4-carboxyphenoxyacetato-κ³O,O′:O′′]

S. Gao, L.-H. Huo, C.-S. Gu, J.-W. Liu and J.-G. Zhao

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A one-dimensional coordination polymer of copper(II) with 2-pyrazinecarboxylate

B. Zheng, G. Liu, L. Gou, D.-Y. Wang and H.-M. Hu

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(SP-4-1)-Bis{aqua[(1R,2R)-N,N′-bis(salicylidene)cyclohexane-1,2-diamine-κ⁴O,N,N′,O′]manganese(III)}-di-μ-cyano-κ⁴N:C-[dicyanonickel(II)]

T. Akitsu, Y. Takeuchi and Y. Einaga

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catena-Poly[[[diaqua(2-sulfonatobenzoato)nickel(II)]-μ-1,2-di-4-pyridylethylene] 0.25-hydrate]

H.-P. Xiao, X.-H. Li and M.-L. Hu

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Poly[[cis-diaqua(2,2′-bipyridine)copper(II)]-μ-3-carboxylato-4-hydroxybenzenesulfonato]

S.-R. Fan, L.-G. Zhu, H.-P. Xiao and S. W. Ng

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The tris(dimethoxyethane) adduct of strontium iodide

F. Weber, G. Wolmershäuser and H. Sitzmann

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A one-dimensional Cl-bridged Pt^II/Pt^IV mixed-valence complex, catena-poly[[[bis(ethylenediamine)platinum(II)]-μ-chloro-[bis(ethylenediamine)platinum(IV)]-μ-chloro] tetrakis(tetrafluoroborate)]

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Polymeric triaquabis(μ₃-3-carboxybenzenesulfonato)barium(II)

S. Gao, Z.-B. Zhu, L.-H. Huo and S. W. Ng

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A trigonal prismatic coordination geometry for vanadium in bis(2-oxidonaphthalene-1-carbaldehyde benzoylhydrazonato)vanadium(IV) dichloromethane hexane hemisolvate

S. Gao, L.-H. Huo, H. Zhao and S. W. Ng

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Bis(adamantylamine-κN)bis(1-phenylbutane-1,3-dionato-κ²O,O′)nickel(II)

E. Meštrović and D.-K. Bučar

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Diaquabis(biuretato-κ²O,O′)nickel(II) dichloride

J. Lawson and W. T. A. Harrison

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Polymeric diaqua(μ₆-1,5-naphthalenedisulfonato)barium(II)

S. Gao, Z.-B. Zhu, L.-H. Huo and S. W. Ng

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Poly[[(1,10-phenanthroline)lead(II)]-μ₅-1,3-benzenedicarboxylato]

H.-D. Wang, H.-Y. He, Y.-J. Wang, L.-G. Zhu and S. W. Ng

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fac-Tricarbonyl(2,9-dimethyl-1,10-phenanthroline)(2,6-dimethylphenyl isocyanide)rhenium(I) hexafluorophosphate

J. M. Villegas, S. R. Stoyanov, C. E. Moore, D. M. Eichhorn and D. P. Rillema

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Bis(1,2-di-4-pyridylethene)bis(5-hydroxyisophthalato)zirconium(II) monohydrate

Y.-J. Zhao, R.-W. Liu and X.-H. Li

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Tris(biacetyl dihydrazone-κ²N,N′)zinc(II) bis(perchlorate) at 110 K

H. Elengoz, R. Shoshnik and I. Goldberg

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Tris(biacetyl dihydrazone-κ²N,N′)cadmium(II) bis(perchlorate) at 110 K

E. Tirosh, R. Maman and I. Goldberg

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Bis(imidazolium) hexachlorostannate(IV)

H. Zhang, L. Fang, R. Dronskowski, K. Kruse and R. Yuan

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Chloro(4,7-diphenyl-1,10-phenanthroline)(2,2′:6′,2′′-terpyridine)ruthenium(II) hexafluorophosphate

N. Yoshikawa, N. Kanehisa, Y. Kai, H. Takashima and K. Tsukahara

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Poly[[bis(triphenylphosphine)mercury(II)]-μ-thiocyanato-cadmium(II)-tri-μ-thiocyanato]

X. Q. Wang, W. T. Yu, D. Xu and H. Q. Sun

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Diaquabis(1,1,4-trimethylthiosemicarbazide)nickel(II) dinitrate

A. D. Burrows, R. W. Harrington and M. F. Mahon

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Disodium cytidine-5′-monophosphate 6.07-hydrate methanol 0.27-solvate

S. V. Gonzalez, K. Larsen, W. H. Nelson, E. Sagstuen and C. H. Görbitz

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Chloro{μ-2-[(E)-1-(2-oxido-3-methylphenyl)ethylideneamino]acetato}pentaphenylditin(IV)

A. Linden, T. S. Basu Baul and C. Masharing

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A copper(II) complex of the fungicide tebuconazole

P.-Z. Zhang and J. Wu

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cis-Diaquabis(1,10-phenanthroline)manganese(II) 3-carboxylato-4-hydroxybenzenesulfonate tetrahydrate

S.-R. Fan, L.-G. Zhu, H.-P. Xiao and S. W. Ng

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[N,N′-Bis(2,4-dimethylbenzene)-2,3-dimethyl-1,4-diazabuta-1,3-diene]-fac-tricarbonyl(trifluoroacetato)rhenium(I)

R. Kia, V. Mirkhani, A. Deák and A. Kálmán

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Aqua(1,10-phenanthroline)(thiodiglycolato)cobalt(II)

J.-Y. Wu, L.-M. Xie, H.-Y. He, X. Zhou and L.-G. Zhu

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Bis[1,3-bis(diphenylphosphino)propane-κ²P,P′]nickel(0)

S. C. Davies, S. E. Duff and D. J. Evans

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catena-Poly[lithium(I)-μ-1-tert-butyl-3-(3-pyridyl)-N,N′-bis(trimethylsilyl)propane-1,3-diiminato]

X. Chen, L. Wang, J.-P. Guo, S.-P. Huang and D.-S. Liu

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Bis(3-carboxyanilinium) hexafluorostannate(IV)

S. Bouacida, H. Merazig, A. Beghidja and C. Beghidja

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trans-4-(Ferrocenylideneamino)-1,5-dimethyl-2-phenyl-1H-pyrazol-3(2H)-one

H.-F. Wu and H.-X. Wang

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Acetato[1-(oxazolin-2-ylmethyl-κN)-1H-indolyl-κC²](triphenylphosphine)palladium(II) dichloromethane solvate

A. R. Cowley, R. I. Cooper, E. Capito, J. M. Brown and A. Ricci

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Chloro{1-[(dimethylamino)methyl-κN]-1H-indolyl-κC²}(triphenylphosphine-κP)palladium(II) dichloromethane solvate

R. I. Cooper, A. R. Cowley, E. Capito, J. M. Brown and A. Ricci

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μ-Oxo-κ²O:O-bis[bis(1,10-phenanthroline-κ²N,N′)(sulfato-κO)iron(III)] octahydrate

M. Odoko and N. Okabe

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Diaquabis(propane-1,2-diamine-κ²N,N′)copper(II) terephthalate dihydrate

Z.-D. Lin, L.-M. Liu, J.-Y. Lu and X.-G. Meng

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catena-Poly[diethylenetriaminium [ferrate(III)-tri-μ-sulfato-κ⁶O:O′] monohydrate]

Y.-L. Fu, Z.-W. Xu, J.-L. Ren and S. W. Ng

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catena-Poly[hexamethylenediaminium [ferrate(III)-μ-hydroxo-κ²O:O-di-μ-sulfato-κ⁴O:O′] monohydrate]

Y.-L. Fu, Z.-W. Xu, J.-L. Ren and S. W. Ng

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mer-Bis(diethylenetriamine)zinc(II) dichloride monohydrate

B. Liu, F.-J. Huo, X.-M. Jiang and B.-S. Yang

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catena-Poly[[[μ-4,4′-bipyridine-bis[aquacopper(II)]]-di-μ-2-nitroterephthalato]

H.-Y. He, L.-G. Zhu and S. W. Ng

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Dichlorobis(phenothiazine-κS)palladium(II)

X. Zhang, D. Li, X.-P. Zhou and S. W. Ng

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trans-trans-trans-Bis(benzyl isocyanide-κC)dichlorobis(triphenylphosphine-κP)ruthenium(II) dichloromethane solvate

J. L. Look, O. P. M. Horwood, D. C. Levendis and N. J. Coville

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Bis(pyridinium) tetrabromocobaltate(II)

H. Zhang, L. Fang and R. Yuan

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organic compounds

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N,N-Bis(2-pyridiniomethyl)glycine diperchlorate

A. Nielsen, A. D. Bond and C. J. McKenzie

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Tetrakis(4-carboxyphenyl)methane–dimethyl sulfoxide–toluene (1/4/1)

N. Malek, T. Maris, M. Simard and J. D. Wuest

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3-Benzyl-2-methyl-1-phenylsulfonyl-1H-indole

S. M. Malathy Sony, K. Palani, P. Charles, M. N. Ponnuswamy, N. Sureshbabu, P. C. Srinivasan and M. Nethaji

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L-Asparaginyl-L-valine 1.33-hydrate

H. T. Bonge, M. L. Rosenberg, M. Riktor and C. H. Görbitz

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1-Napthyl 4-toluenesulfonate: supramolecular aggregation through weak C—H⋯O and C—H⋯π interactions

V. Manivannan, N. Vembu, M. Nallu, K. Sivakumar and F. R. Fronczek

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Ethyl 4-(4-hydroxyphenyl)-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate

M. Li, W.-S. Guo, L.-R. Wen and W.-Y. Qi

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(Z)-3-[(2,4-Dinitrophenyl)hydrazono]-4,4,4-trifluoro-1-(2-thienyl)butan-1-one

Z.-L. Jing, M. Yu, X. Chen, C.-H. Diao, Q.-L. Deng and Z. Fan

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N,N′-Bis[(R)-2-hydroxy-2-phenylethyl]-N,N′-bis[(S)-1-phenylethyl]pyridine-2,6-dicarboxamide: stabilization of an asymmetric conformer through the formation of a double intramolecular hydrogen bond

M. Sosa-Rivadeneyra, L. Quintero, C. A. Parrodi, E. Juaristi and S. Bernès

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3-Ammonio-4-methoxybenzenesulfonate

S. Gao, L.-H. Huo and S. W. Ng

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3-[(4-Hydroxy-3-methoxyphenyl)methylene]-2,4-pentanedione

L.-X. Pei, X.-Z. Bu, L.-Q. Gu and S. W. Ng

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2-Methyl-7-oxo-5,6,7,8-tetrahydropyrimido[4,5-d]pyrimidin-3-ium chloride, a product of the thermal decomposition of nimustine hydrochloride (ACNU)

I. V. Chernyshev and A. I. Tursina

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(1RS,2SR,7RS,8RS)-N-Benzoyltricyclo[6.2.2.0^2,7]dodeca-9,11-diene-1,10-dicarboximide

N. McSweeney, A. C. Pratt, C. Long and R. A. Howie

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2-{3-[(E)-(3,4-Dimethoxyphenyl)ethenyl]-5,5-dimethylcyclohex-2-enylidene}malononitrile

T. Kolev, D. Yancheva, B. Shivachev, R. Petrova and M. Spiteller

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N-Imidazole–boron trichloride adduct

R. A. Baber, A. E. A. Bull, J. P. H. Charmant, N. C. Norman and A. G. Orpen

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3-Butyl-4-(3-methyl-3-phenylcyclobut-1-yl)-1,3-thiazole-2(3H)-thione

C. Kırılmış, M. Koca, C. Arıcı, F. W. Heinemann and M. Ahmedzade

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3-Benzyl-4-phenyl-1H-1,2,4-triazole-5(4H)-thione

F. Jian, Z. Bai, H. Xiao and K. Li

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1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(4-methylbenzylidene)amino]-1H-pyrazole-3-carbonitrile

P. Zhong, Z. Yang, Q. Shi, S. Li and R. Tang

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n-Butyl acetate

H. A. Shallard-Brown, D. J. Watkin and A. R. Cowley

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16β-Bromo-17α-hydroxypregn-4-ene-3,20-dione methanol solvate

S. Wang, Y. Wang, Q. Nie, A. Xiang and L. Zhou

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4-(9-Acridin-9-ylamino)-2,2,6,6-tetramethylpiperidine N-oxide

Q. Yuan, S.-Z. Jian and Y.-G. Wang

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Bis(2-pyridylmethyl)amine–borane

N. Sanchez Ballester, J. Barreira Fontecha, J. Wikaira and V. McKee

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2-(1-Piperidinyl)-1,3-benzothiazole

R. G. Alvarez, A. R. Kennedy, A. I. Khalaf, C. J. Suckling and R. D. Waigh

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2-(4-Methylbenzoyl)-N-phenyl-2-(1H-1,2,4-triazol-1-yl)ethanethioamide

L.-Z. Xu, G.-D. Si, Z.-F. Li, G.-P. Yu and Y.-W. Huang

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5,6,7,8-Tetrahydro-4aH-thieno[3,2-b]quinolizin-4(10H)-one

V. Vrábel, J. Kožíšek, Š. Marchalín and Z. Žák

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tert-Butyl 4-[2-(methoxycarbonyl)ethyl]-3,5-dimethyl-1H-pyrrole-2-carboxylate

M. Ramos Silva, A. Matos Beja, J. A. Paixão, S. H. Lopes, A. M. T. D. P. V. Cabral, A. M. d'A. Rocha Gonsalves and A. J. F. N. Sobral

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2-(1-Benzoyl-1-phenylethyl)-3-phenylsulfanyl-1-phenylsulfonyl-1H-indole

S. M. Malathy Sony, K. Palani, P. Charles, M. N. Ponnuswamy, N. Sureshbabu, P. C. Srinivasan and M. Nethaji

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(R,S)-1,4-Bis(benzylsulfinyl)butane

J.-R. Li, R.-H. Zhang and X.-H. Bu

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Methyl [4-methoxy-3-(methylsulfonyloxy)benzoyl]formate

D. Schollmeyer, C. Peifer and G. Dannhardt

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(R)-(–)-Mepivacaine hydrochloride enantiomer: a low-temperature study

M. A. Bambagiotti, B. Bruni, M. Di Vaira and V. Giannellini

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(2E,6E)-2,6-Bis(3,5-di-tert-butyl-4-hydroxybenzylidene)cyclohexanone acetic acid solvate

Z.-Y. Du, Y.-F. Wang, X.-P. Mao, J.-K. Qin, L. Ma and L.-Q. Gu

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DL-Phenylalanine DL-phenylalaninium picrate

K. Anitha and R. K. Rajaram

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10-(4-Fluorobenzylidene)anthrone

W. Zhou, W. Hu, L. Lv and C. Xia

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1,3-Bis(pyrimidin-2-ylsulfanyl)propan-2-one

B.-L. Wu, B.-Y. Lou, L. Han and M.-C. Hong

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Scandenin

K. Ravikumar, B. Sridhar, A. Sridhar Rao and J. Madhusudana Rao

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3β-Taraxerol from Bridelia micrantha

S. F. Kouam, U. Flörke, K. Krohn, M. N. Akhtar, B. T. Ngadjui and B. M. Abegaz

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Pentaerythrityl tetrakis(4-bromobenzyl ether)

D. Laliberté, N. Raymond, T. Maris and J. D. Wuest

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4-(3-Hydroxy-4-methoxyphenyl)-3-(3,4,5-trimethoxyphenyl)-2,5-dihydro-1H-pyrrole-2,5-dione

D. Schollmeyer, C. Peifer and G. Dannhardt

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1-(3,4,5-Trimethoxyphenyl)naphthalene

B. Suthar, A. Fowler, D. S. Jones and C. A. Ogle

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3,5-Dinitrobenzoic acid–dimethyl sulfoxide (1/1)

M. Abthorpe, A. V. Trask and W. Jones

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2,6-Diammonio-4-toluenesulfonate chloride dihydrate

S. Gao, L.-H. Huo and S. W. Ng

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2,3,5,6-Tetramethylpyrazine–p-nitrophenol (1/2)

X.-Q. Cai, M.-L. Hu, Y.-J. Zhao, Y.-Q. Cheng and S. Wang

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3,6-Di-2-pyridylpyrrolo[3,4-c]pyrrole-1,4(2H,5H)-dione

T. Imoda, T. Hirota, H. Takahashi and J. Mizuguchi

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4-Phenyl-3-(pyridin-4-yl)-1H-1,2,4-triazole-5(4H)-thione

S. Ö. Yıldırım, M. Akkurt, A. Çetin, A. Cansız, M. Şekerci and C. Kazak

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5-(4-Methoxybenzoyl)-4-(4-methoxyphenyl)-1-[1-(4-methoxyphenyl)ethylideneamino]pyrimidin-2(1H)-one

S. Özçelik, M. Dinçer, E. Sarıpınar and C. Yılmaz

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1-(Hydroxymethyl)-3,5-dimethylpyrazole

I. Radosavljević Evans, K. Mészáros Szécsényi and V. M. Leovac

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3-{[(2,6-Diisopropylphenyl)imino]methyl}-2-naphthol

J. Lin, G.-H. Cui, J.-R. Li and S.-S. Xu

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(2S,4R)-1-Benzyl 2-tert-butyl 4-[N,N′-bis(tert-butyloxycarbonyl)hydrazino]-5-oxopyrrolidine-1,2-dicarboxylate

K. Kaczmarek, W. M. Wolf and J. Zabrocki

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N-(2-Benzoyl-4-chlorophenyl)-2-chloroacetamide

S. M. Malathy Sony, P. Charles, M. N. Ponnuswamy and M. Nethaji

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4,7-Bis(4-methoxyphenyl)-1,3,7-triphenyl-2,3,5,6,7,7a-hexahydro-1H-pyrrolo[2,3-d]pyrimidine-2,5,6-trione

H. Adams, M. Saçmaci, Ş. H. Üngören and Y. Akçamur

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5-(4-Methoxybenzoyl)-4-(4-methoxyphenyl)-1-[1-(4-methoxyphenyl)ethylidenenamino]pyrimidin-2(1H)-one

S. Özçelik, M. Dinçer, E. Sarıpınar and Ç. Yılmaz

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N-Benzoylthiosemicarbazide

H.-D. Bian, G.-Q. Guo, Q. Yu, H. Liang, X.-E Yang and L.-G. Zhu

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1,4,11,12-Tetrahydro-9,10-anthraquinone

A. Decken, S. M. Mattar and A. Emwas

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Methyl 4-O-benzyl-6-deoxy-2,3-O-isopropylidene-α-L-talopyranoside

M. T. Maust, P. Norris and M. Zeller

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2,2′:6′,2′′-Terpyridine 1,1′′-dioxide dihydrate

K. A. Wheeler, S. E. McKay and R. W. Lashlee III

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4-[(Methoxyglycyl)carbonyl]tetrathiafulvalene

A. S. Batsanov, S. L. Viles and A. J. Moore

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trans-3-Bromo-2-chloroindan-1-one

P.-S. Yu, G. D. Thomas, A. G. Blackman and E. W. Tan

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4-Phenyl-1-(propan-2-ylidene)thiosemicarbazide

F.-F. Jian, Z.-S. Bai, H.-L. Xiao and K. Li

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3-(2-Bromo-4,5-dimethoxybenzyl)thiazolidine-2,4-dione

H. S. Yathirajan, S. L. Gaonkar, K. M. Lokanatha Rai and M. Bolte

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Di-tert-butylphosphine oxide

F. Dornhaus, H.-W. Lerner and M. Bolte

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1,4:8,11:15,18:22,25-Tetraethano-29H,31H-tetrabenzo[b,g,l,q]porphine toluene trisolvate

S. Aramaki, Y. Sakai, H. Yanagisawa and J. Mizuguchi

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Ethyl 2,3,5,6-tetramethylbenzoate

A. G. Pinkus, K. K. Klausmeyer, R. P. Feazell and E. C. H. Y. Lin

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1,6-Anhydro-2-iodo-2-deoxy-β-D-glucopyranose (Iodolevoglucosan)

D. Gehle, U. Flörke and K. Krohn

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2,2-Dimethyl-6-(4-nitrophenyl)-4-phenyl-1,3-diazabicyclo[3.1.0]hex-3-ene

V. V. Dyakonenko, O. V. Shishkin, A. V. Zbruev and S. M. Desenko

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N,N′-Bis[2-(4-pyridyl)ethyl]perylene-3,4:9,10-bis(dicarboximide) phenol disolvate

J. Mizuguchi and K. Hino

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N,N′-Bis[2-(4-pyridyl)ethyl]perylene-3,4:9,10-bis(dicarboximide) m-cresol disolvate

K. Hino and J. Mizuguchi

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(1RS,4SR,8SR,11RS,15SR,18RS,22RS,25SR)-1,4:8,11:15,18:22,25-Tetraethano-29H,31H-tetrabenzo[b,g,l,q]porphine chloroform disolvate

S. Aramaki, Y. Sakai, H. Yanagisawa, T. Senju and J. Mizuguchi

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1,1,2,2-Tetrachloro-1,2-diphenylethane

A. Garcia-Sanchez, I. I. Padilla-Martínez, F. J. Martínez-Martínez, H. Höpfl and E. V. García-Báez

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1-Chloromethyl-4-aza-1-azoniabicyclo[2.2.2]octane tetrafluoroborate deuterochloroform solvate

A. S. Batsanov, J. Trmcic and G. Sandford

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4-(2-Benzoylphenoxy)phthalonitrile

T. Akbal, N. Akdemir, E. Ağar, C. Kantar and A. Erdönmez

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2-Benzyloxy-3-nitropyridine

Y. Cui, H.-M. Liu and W.-Q. Zhang

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A stereoisomer of bharangin triacetate

K. Ravikumar, B. Sridhar and M. Marthanda Murthy

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Phenyl 4-toluenesulfonate: supramolecular aggregation through weak C—H⋯O and C—H⋯π interactions

V. Manivannan, N. Vembu, M. Nallu, K. Sivakumar and A. Linden

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1,4-Dimorpholinobenzene

J. W. Quail, A. Doroudi, U. Das and J. R. Dimmock

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2,3,5-Trichloro-6-(4-methylpiperidin-1-yl)-1,4-benzoquinone: a synchrotron study

K. F. Bowes, J. M. Cole and M. Szablewski

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[6-(Benzoyloxy)-1,4,5-trihydroxycyclohex-2-en-1-yl]methyl benzoate

S. Angchuan, S. Chantrapromma, H.-K. Fun and C. Karalai

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1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(4-dimethylaminobenzylidene)amino]-1H-pyrazole-3-carbonitrile

D. Chen, Z. Yang, P. Zhong and M. Hu

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2-(3-Benzyloxy-4-methoxyphenyl)-5-phenyl-1,3,4-oxadiazole

Z.-H. Shang, W. Li and S.-Q. Wang

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2-[(2-Chloro-5-phenyl-3-pyridinyl)(hydroxy)methyl]acrylonitrile

G. Y. S. K. Swamy, K. Ravikumar, P. Narender and V. Jayathirtha Rao

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2-[(2-Chloro-5-ethyl-3-pyridinyl)(hydroxy)methyl]acrylonitrile

G. Y. S. K. Swamy, K. Ravikumar, P. Narender and V. Jayathirtha Rao

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1,3-Di-tert-butyl-6-(trimethylsilylethynyl)fulvene

H. Berger, P. Bubenitschek, H. Hopf and P. G. Jones

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3-[(4-Fluorophenyl)methylenehydrazinocarbonyl]-1H-1,2,4-triazole monohydrate

F.-Y. Pan and J.-G. Yang

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4′-[2-Butyl-4-chloro-5-(hydroxyiminomethyl)-1H-imidazol-3-ylmethyl]biphenyl-2-carbonitrile

H. S. Yathirajan, B. Nagaraj, R. S. Narasegowda and M. Bolte

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2-tert-Butoxy-1-phenyl-1-(2,2,6,6-tetramethylpiperidin-1-yloxy)ethane

A. S. Batsanov, A. J. Reid and N. Cameron

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6-Methyl-N'-(1-methylethylidene)imidazo[2,1-b][1,3]thiazole-5-carbohydrazide monohydrate

M. Akkurt, S. Ö. Yıldırım, F. Ur, Z. Cesur, N. Cesur and O. Büyükgüngör

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3-(1H-Indol-3-yl)-4-(3,4,5-trimethoxyphenyl)-2,5-dihydro-1H-pyrrole-2,5-dione

C. Peifer, D. Schollmeyer and G. Dannhardt

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5,6,7-Trimethoxy-2,3-dihydro-1H,8H-benzo[a]pyrrolo[3,4-c]carbazole-1,3-dione dimethyl sulfoxide solvate

C. Peifer, D. Schollmeyer and G. Dannhardt

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A second polymorphic form of pentazocine hydrochloride at 105 K

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2,3,4-Tri-O-acetyl-β-L-fucopyranosyl azide

P. Norris and M. Zeller

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Tetramethylpyrazine–endo-norbornene-cis-5,6-dicarboxylic acid (1/2)

M.-L. Hu, Z.-M. Jin, Y.-J. Zhao, D.-M. Chen, S. Wang and X.-Q. Cai

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Methyl 2-methyl-5-oxo-4-(2-thienyl)-1,5,7,8,9,10-hexahydro-4H-pyrido[2′,3′:3,4]pyrrolo[1,2-a][1,3]diazepine-3-carboxylate

V. Vrábel, J. Kožíšek, Š. Marchalín and I. Svoboda

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Methyl 2,3,4-tri-O-acetyl-1-azido-1-deoxy-β-D-glucopyranuronate at 100 K

C. R. Smith, P. Norris and M. Zeller

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Methyl 2,3,4-tri-O-acetyl-1-azido-1-deoxy-β-D-glucopyranuronate at room temperature

B. L. Wilkinson, L. F. Bornaghi, T. A. Houston, S.-A. Poulsen and P. C. Healy

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meso-1,2-Bis(pyridin-2-yl)ethane-1,2-diol

J. K. Bjernemose and A. D. Bond

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3-(3-Hydroxyphenyl)-1-(4-methoxyphenyl)prop-2-en-1-one

S. Sathiya Moorthi, K. Chinnakali, S. Nanjundan, P. Selvam, H.-K. Fun and X.-L. Yu

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Cytosinium 3,5-dinitrosalicylate

G. Smith, U. D. Wermuth and P. C. Healy

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3-(Imidazolidin-2-ylidene)-6-methyl-3,4,5,6-tetrahydro-2H-pyran-2,4-dione

J.-J. Hao, H. Xu, H.-B. Song, Y.-M. Wang and Z.-M. Li

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4-[2-(5-Ethylpyridin-2-yl)ethoxy]benzaldehyde oxime

S. L. Gaonkar, H. S. Yathirajan, K. M. Lokanatharai, B. Nagaraj and M. Bolte

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2,2′-Diamino-4,4′-bi-1,3-thiazolium (2R,3R)-tartrate

B.-X. Liu and D.-J. Xu

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1,4-Dimethylpyridinium triiodide

X.-J. Tan, S.-X. Sun, S.-L. Liu, J.-P. Ma and D.-X. Xing

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4-Bromo-2,6-dichloroaniline

M. Arun Prasad, B. Varghese and M. V. Sangaranarayanan

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(2-exo,7-exo,9-endo,10-endo)-11-Oxatricyclo[6.2.1.0^2,7]undec-4-ene-9,10-diyl diacetate

M. Akkurt, S. Öztürk Yıldırım, A. Baran, H. Seçen and O. Büyükgüngör

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Nipecotic acid hydrochloride

R. S. Narasegowda, H. S. Yathirajan and M. Bolte

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2,3-Bis(2-cyanoethylsulfanyl)-6,7-bis(methylsulfanyl)tetrathiafulvalene

A. D. Bond and J. O. Jeppesen

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5-[4'-(Bromomethyl)biphenyl-2-yl]-2-trityl-2H-tetrazole

B. Nagaraj, R. S. Narasegowda, H. S. Yathirajan, S. L. Gaonkar and M. Bolte

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3-(4-Chlorophenyl)-2H-benz[b][1,4]oxazine

I. Vencato, P. H. Ferri, L. C. Faria, S. C. Santos and C. Lariucci

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Bis[diethylenetriaminium(3+)] tris(sulfate) monohydrate

Y.-L. Fu, Z.-W. Xu, J.-L. Ren and S. W. Ng

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Triethylenetetraminium(4+) bis(sulfate) monohydrate

Y.-L. Fu, Z.-W. Xu, J.-L. Ren and S. W. Ng

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(2-Chloropyridin-3-yl)(4-nitrobenzylidene)amine

M. Akkurt, S. Karaca, A. A. Jarrahpour, M. Zarei and O. Büyükgüngör

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6-O-Cyanomethyl-1,2:3,4-di-O-isopropylidene-α-D-galactopyranose

V. Langer, B. Steiner, J. Mičová and M. Koóš

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4-Chloro-3-(2,3,5-trimethylphenoxy)phthalonitrile

S. Yazıcı, N. Akdemir, E. Ağar, C. Kantar and İ. Şenel

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3,4-Dihydro-8-hydroxy-3,5-dimethyl-7-methoxyisocoumarin (avicennin B)

J. Wang, H.-R. Huang, X.-L. Feng, Y.-C. Lin and S.-N. Zhou

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1-[2,6-Dichloro-4-(trifluoromethyl)phenyl]-5-[(4-nitrophenyl)methyleneimino]-1H-pyrazole-3-carbonitrile

P. Zhong, Z. Yang and Q. Shi

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threo-3,4-Dihydroxyhexane-2,5-dione

S. Fang, C.-H. He, X.-R. Liang and W.-K. Su

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Ethyl 2-(2-chloro-1,4-dihydro-1,4-dioxonaphthalen-3-ylamino)-4-phenylthiazole-5-carboxylate

D. E. Lynch and I. McClenaghan

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Phenacyl (2S,4S)-1-tert-butoxycarbonyl-4-hydroxyprolinate

P. Chabaud, M. Worf, J. Courcambeck, M. Camplo and G. Pèpe

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1-Methyl-6,7-dihydropyrrolo[2,3-c]azepine-4,8(1H,5H)-dione

X.-C. Zeng, S.-H. Xu, J. Gu and D.-S. Deng

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Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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Acta E is now included in the Thomson Reuters Emerging Sources Citation Index.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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