Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 69| Part 6

ISSN: 2056-9890

June 2013 issue

Highlighted illustration

Cover illustration: The compound C₆₀H₇₆Si₂ possesses inversion symmetry and is formally an anti-aromatic system containing 20- [pi] electrons. It contains a rare [pi] -xylylene motif, which is displayed by alternating short and long bonds. The outer rings of the indeno[1,2-b]fluorene system possess nearly homogenous bond lengths. In the crystal, the molecules form layers perpendicular to the c axis and within these layers there are two one-dimensional stacks with one stack having an sp²sp² CC contact of only 3.283 (6) Å. See: Rose, Zakharov & Haley [Acta Cryst. (2013). E69, o890].

inorganic compounds

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(Thiocyanato-κS)tris(thiourea-κS)mercury(II) chloride

A. Shihabuddeen Syed, K. Rajarajan and M. NizamMohideen

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Synchrotron powder study of Na₃V(PO₃)₃N

M. Kim and S.-J. Kim

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Poly[tri-μ-aqua-diaqua-μ-phosphonoformato-cobalt(II)sodium]

X.-J. Luo and X.-Q. Zhang

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The low-symmetry lanthanum(III) oxotellurate(IV), La₁₀Te₁₂O₃₉

P. L. Wang and Y. Mozharivskyj

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K(MoO₂)₄O₃(AsO₄)

R. Jouini, M. F. Zid and A. Driss

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Na_2.9KMo₁₂S₁₄: a novel quaternary reduced molybdenum sulfide containing Mo₁₂ clusters with a channel structure

P. Gougeon, P. Gall and D. Salloum

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LiCo₂As₃O₁₀: une nouvelle structure à tunnels interconnectés

Y. Ben Smida, A. Guesmi and A. Driss

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metal-organic compounds

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Pyridinium bis(pyridine-κN)tetrakis(thiocyanato-κN)ferrate(III)

S. I. Shylin, I. A. Gural'skiy, M. Haukka, A. A. Kapshuk and E. V. Prisyazhnaya

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Bis{2-[2,5-bis(pyridin-2-yl)-1H-imidazol-4-yl]pyridinium} tetracyanidoplatinate(II) tetrahydrate

R. Gámez-Heredia, R. E. Navarro, H. Höpfl, A. Cruz-Enríquez and J. J. Campos-Gaxiola

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2-Amino-5-bromopyridin-1-ium (2-amino-5-bromopyridine-κN¹)trichloridozincate

Fitriani, K. Hansongnern, N. Leesakul, C. Pakawatchai and S. Saithong

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Poly[1H-imidazol-3-ium [di-μ-nitrato-sodium]]

C. Trifa, A. Bouhali, S. Bouacida, C. Boudaren and T. Bataille

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Poly[bis(piperazine-1,4-diium) [(μ₄-cyclo-hexaphosphato)dilithium] tetrahydrate]

I. Ameur, S. Abid, S. S. Al-Deyab and M. Rzaigui

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Sodium bis(ethylenediamine)copper(II) tetracyanidocuprate(I)

P. W. R. Corfield, R. K. Dobbs and B. Bell

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Bis(3-aminopyrazine-2-carboxylato-κ²N¹,O)diaquanickel(II) dihydrate

R. Bouchene, A. Khadri, S. Bouacida, F. Berrah and H. Merazig

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Tris(N,N-dimethylanilinium) hexabromidostannate(IV) bromide

H. Chouaib, S. Kamoun and H. F. Ayedi

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1,1′-(Ethane-1,2-diyl)dipyridinium bis(1,2-dicyanoethene-1,2-dithiolato-κ²S,S′)cuprate(II)

B.-X. Hu, C.-X. Zhou, Y.-M. Liu, L.-Z. Chen and F.-M. Wang

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Aquatrimethyl[2-(4-methylpyrimidin-2-ylsulfanyl)acetato-κO]tin(IV)

Z. Gao, J. Zhang, X. Hao, D. Wang and T. Zhang

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[Diaquasesqui(nitrato-κO)hemi(perchlorato-κO)copper(II)]-μ-{bis[5-methyl-3-(pyridin-2-yl)-1H-pyrazol-4-yl] selenide}-[triaqua(perchlorato-κO)copper(II)] nitrate monohydrate

M. Seredyuk, V. A. Pavlenko, K. O. Znovjyak, E. Gumienna-Kontecka and T. S. Iskenderov

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(O-Methyl dithiocarbonato-κS)triphenyltin(IV)

F. Javed, S. Ali, W. Shah, M. N. Tahir and H. Ullah

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catena-Poly[[[diaquabis[1,2-bis(pyridin-4-yl)diazene]copper(II)]-μ-1,2-bis(pyridin-4-yl)diazene] bis(perchlorate)]

E. Ballestero-Martínez, C. S. Campos-Fernández, V. H. Soto-Tellini, S. Gonzalez-Montiel and D. Martínez-Otero

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catena-Poly[[[bis(methanol-κO)bis(selenocyanato-κN)manganese(II)]-μ-1,2-bis(pyridin-4-yl)ethene-κ²N:N′] 1,2-bis(pyridin-4-yl)ethene monosolvate]

S. Wöhlert, I. Jess and C. Näther

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catena-Poly[[[diaquabis(selenocyanato-κN)iron(II)]-μ-1,2-bis(pyridin-4-yl)ethane-κ²N:N′] 1,2-bis(pyridin-4-yl)ethane disolvate dihydrate]

S. Wöhlert, I. Jess and C. Näther

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[Hexane-2,5-dione bis(thiosemicarbazonato)]nickel(II)

M. S. Shalamzari, A. V. Gurbanov, S. Heidic, R. Kia and S. Behrouzi

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Bis{(Z)-[(E)-2-(pyridin-2-ylmethylidene)hydrazin-1-ylidene][(pyridin-2-yl)methylsulfanyl]methanethiolato}nickel(II)

T.-J. Khoo, M. K. bin Break, M. I. M. Tahir, K. A. Krouse, A. R. Cowley and D. J. Watkin

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Bis(2,2′,2′′-nitrilotriacetamide-κ³O,N,O′)cobalt(II) dinitrate tetrahydrate

J.-W. Ran and J. Pei

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catena-Poly[[manganese(III)-bis{μ-2-[(2-hydroxyethyl)iminomethyl]-6-methoxyphenolato-κ³O¹,N:O²;κ³O²:N,O¹}] iodide]

S. R. Petrusenko, O. M. Stetsyuk and I. V. Omelchenko

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Tetraphenylphosphonium [μ₃-(4-methylphenyl)tellurolato]tris[tetracarbonyliron(0)]

Y.-L. Li, B. Xie and L.-K. Zou

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cis-Tetrakis(μ-N-phenylacetamidato)-κ⁴N:O;κ⁴O:N-bis[(benzonitrile-κN)rhodium(II)](Rh—Rh)

C. T. Eagle, F. Quarshie, M. E. Ketron and N. Atem-Tambe

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Bis(1,4-diazoniabicyclo[2.2.2]octane) di-μ-chlorido-bis[tetrachloridoantimonate(III)] dihydrate

T. Ben Rhaiem, H. Boughzala and A. Driss

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trans-Dichloridobis{2-chloro-6-[(3-fluorobenzyl)amino]-9-isopropyl-9H-purine-κN⁷}platinum(II)

Z. Trávníček and P. Štarha

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Tris(ethylenediamine)cobalt(II) dichloride

K. Cooke, A. V. Olenev and K. Kovnir

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Bis(but-2-enoato-κO)triphenylbismuth(V)

P. V. Andreev, N. V. Somov, O. S. Kalistratova, A. V. Gushchin and E. V. Chuprunov

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(Cyclobutane-1,1-dicarboxylato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)platinum(II) dihydrate

P. Štarha and Z. Trávníček

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(Adipato-κ²O,O′)diaqua[bis(pyridin-2-yl-κN)amine]cobalt(II) trihydrate

Z. Setifi, F. Setifi, G. Smith, M. El-Ghozzi, D.-A. Rouag, D. Avignant and H. Merazig

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Di-μ-azido-diazidodi-μ-oxalato-dihistaminetetracopper(II) 0.9-hydrate

C. Liu and K. A. Abboud

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Bis[μ-1,3-bis(diphenylphosphanyl)propane-κ²P:P′]digold(I) tetrachloridonickelate(II) diethyl ether monosolvate

A. Igashira-Kamiyama, T. Itai, Y. Arai and T. Konno

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Tris(acetonitrile-κN)dichlorido(triphenylphosphane-κP)ruthenium(II) acetonitrile monosolvate

X.-F. Yin, Y. Qin, H.-T. Shi, Q. Chen and Q.-F. Zhang

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Tris(diisopropyl dithiophosphato-κ²S,S′)ruthenium(III)

G.-P. Chao, X. Wu, H.-T. Shi, Q. Chen and Q.-F. Zhang

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catena-Poly[[(triphenylphosphane-κP)silver(I)]-μ-4,4′-bipyridine-κ²N:N′-[(triphenylphosphane-κP)silver(I)]-di-μ-chlorido]

X.-M. Song, F. Hu, H.-T. Shi, Q. Chen and Q.-F. Zhang

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Aquacarbonyl(ferrocenyldithiophosphonato-κ²S,S′)bis(triphenylphosphane-κP)ruthenium(II) dichloromethane monosolvate

H. Zhu, Q. Ma, H.-T. Shi, Q. Chen and Q.-F. Zhang

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Tetraethylammonium trichlorido(N,N′-dimethylformamide-κO)zinc

G.-P. Chao, H.-T. Shi, Q. Chen and Q.-F. Zhang

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catena-Poly[[bis(pyridine-κN)zinc]-μ-5-carboxybenzene-1,3-dicarboxylato-κ²O¹:O³]

B. Yotnoi and A. Rujiwatra

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{N,N-Bis[bis(2,2,2-trifluoroethoxy)phosphanyl]methylamine-κ²P,P′}bis(η⁵-cyclopentadienyl)titanium(II)

M. Haehnel, S. Hansen, A. Spannenberg and T. Beweries

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Bis(2,2′-bipyridyl-κ²N,N′)(sulfato-κ²O,O′)nickel(II) 2.5-hydrate

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Diaquabis(3-chlorobenzoato-κO)bis(nicotinamide-κN¹)cobalt(II)

N. Bozkurt, N. Dilek, N. Çaylak Delibaş, H. Necefoğlu and T. Hökelek

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Bis[μ-2,5-bis(pyridin-2-yl)-1,3,4-thiadiazole-κ⁴N²,N³:N⁴,N⁵]bis[(nitrato-κO)silver(I)] tetrahydrate

A. Laachir, F. Bentiss, S. Guesmi, M. Saadi and L. El Ammari

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organic compounds

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1,3-Bis(2-methylprop-2-enoyl)-1H-benzimidazol-2(3H)-one

N. Haridharan and V. Ramkumar

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2-Methoxy-4-(prop-2-en-1-yl)phenyl 4-methoxybenzoate

M. R. Pichika, B. K. Yew and S. W. Ng

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2-(4-Fluorophenyl)-5-iodo-7-methyl-3-phenylsulfinyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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3-(2-Fluorophenylsulfinyl)-2,5,7-trimethyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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Ethyl 1′′-benzyl-1′-methyl-2′′-oxodispiro[indeno[1,2-b]quinoxaline-11,3′-pyrrolidine-2′,3′′-indoline]-4′-carboxylate

P. S. Kannan, S. Lanka, S. Thennarasu, E. Govindan and A. SubbiahPandi

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Methyl (3S,10b'S)-5-chloro-9′-fluoro-1-methyl-2-oxo-5′-phenyl-10b'H-spiro[indoline-3,1′-pyrazolo[3,2-a]isoquinoline]-2′-carboxylate

P. S. Kannan, P. S. Yuvaraj, B. S. R. Reddy, R. Raja and A. SubbiahPandi

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Methyl 5′′-chloro-1′,1′′-dimethyl-2,2′′-dioxodispiro[indoline-3,2′-pyrrolidine-3′,3′′-indoline]-4′-carboxylate

P. S. Kannan, P. S. Yuvaraj, K. Manivannan, B. S. R. Reddy and A. SubbiahPandi

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3-Nitrophenol–1,3,5-triazine-2,4,6-triamine (2/1)

V. Sangeetha, N. Kanagathara, G. Chakkaravarthi, M. K. Marchewka and G. Anbalagan

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9-[3-(Carbazol-9-yl)-5-methylphenyl]carbazole

J. E. Kim, J. H. Kim, W. Sim and J. Y. Lee

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N-(2-Bromo-4-methylphenyl)-2-(5-methyl-2-phenylpyrazolo[1,5-a]pyrimidin-7-yl)acetamide

I. Bassoude, S. Berteina-Raboin, E. M. Essassi, G. Guillaumet and L. El Ammari

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(1S,3R,8R)-2,2-Dichloro-3,7,7,10-tetramethyltricyclo[6.4.0.0^1,3]dodec-9-en-11-one

N. Ourhriss, A. Benharref, A. Oukhrib, J.-C. Daran and M. Berraho

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10-Methyl-2-oxo-4-phenyl-2,11-dihydropyrano[2,3-a]carbazole-3-carbonitrile

A. Thiruvalluvar, E. Yamuna, R. Archana, K. J. Rajendra Prasad and R. J. Butcher

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2-Chloro-6-(2,3-dichlorobenzenesulfonamido)benzoic acid

A. Munir, H. Mubashar-ur-Rehman, A. M. Asiri, I. U. Khan and M. N. Arshad

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15-Methoxy-14,15-dihydroandranginine

D.-L. Wang, X.-H. Cai, P. Huang and H.-P. Huang

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2-Bromo-1,6,6-trimethyl-6,7,8,9-tetrahydrophenanthro[1,2-b]furan-10,11-dione

C.-P. Fan, W.-P. Yin, X.-X. Cao and J.-C. Yao

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4-Hydroxy-1,2,6-trimethylpyridinium chloride monohydrate

T. Seethalakshmi, S. Manivannan, S. Dhanuskodi, D. E. Lynch and S. Thamotharan

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Methyl 2-(2-methyl-4-nitro-1H-imidazol-1-yl)acetate

S. Zama, A. Bouraiou, S. Bouacida, T. Roisnel and A. Belfaitah

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1-Methyl-3-(2-oxo-2H-chromen-3-yl)-1H-imidazol-3-ium picrate

N. V. Tuyen, L. T. Anh, A. A. Festa, L. G. Voskressensky and V. N. Khrustalev

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1-[3-(2-Benzyloxy-6-hydroxy-4-methylphenyl)-5-[3,5-bis(trifluoromethyl)phenyl]-4,5-dihydro-1H-pyrazol-1-yl]propane-1-one

U. H. Patel, S. A. Gandhi, V. M. Barot and N. V. S. Varma

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2-Amino-5-nitropyridinium trifluoroacetate

J. V. Jovita, S. Sathya, G. Usha, R. Vasanthi and K. S. Ezhilarasi

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3-(Ammoniomethyl)pyridinium bis(perchlorate)

I. Bayar, R. Kefi, P. Sidonio Pereira da Silva, M. Ramos Silva and C. Ben Nasr

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3-Amino-5,6-dimethyl-1,2,4-triazin-2-ium nitrate

S. Bel Haj Salah, M. L. Mrad, V. Ferretti, F. Lefebvre and C. Ben Nasr

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3,5-Dimethyl-1-{2-[(5-methyl-1,3,4-thiadiazol-2-yl)sulfanyl]acetyl}-2,6-diphenylpiperidin-4-one

S. Ganesan, P. Sugumar, S. Ananthan and M. N. Ponnuswamy

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2-(2,6-Dichlorophenyl)-1-pentyl-4,5-diphenyl-1H-imidazole

M. Akkurt, S. K. Mohamed, K. Singh, A. A. Marzouk and A. A. Abdelhamid

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Ethyl 3-bromo-4-cyano-5-[(2-ethoxy-2-oxoethyl)sulfanyl]thiophene-2-carboxylate

X. Li, X. Jia and J. Li

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(E)-9-(But-2-en-1-yl)-6-chloro-9H-purine

F. Lundvall, J. Kania and L.-L. Gundersen

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1-{(E)-[(2-Fluoro-5-nitrophenyl)imino]methyl}naphthalen-2-ol

A. R. Kennedy, M. Akkurt, A. A. Abdelhamid, S. K. Mohamed and G. J. Miller

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Methyl (2Z)-2-bromomethyl-3-(3-chlorophenyl)prop-2-enoate

K. Swaminathan, K. Sethusankar, R. Selvakumar and M. Bakthadoss

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5-Methyl-N-(1,3-thiazol-2-yl)isoxazole-4-carboxamide

D.-C. Wang, X. Sun, P. Su and P.-K. Ou-Yang

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Ethyl 1′′-benzyl-2′′-oxo-2′,3′,5′,6′,7′,7a'-hexahydro-1′H-dispiro[indeno[1,2-b]quinoxaline-11,2′-pyrrolizine-3′,3′′-indoline]-1′-carboxylate monohydrate

P. S. Kannan, S. Lanka, S. Thennarasu, G. Vimala and A. SubbiahPandi

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Methyl 2-(5-chloro-1-methyl-2-oxo-2,3-dihydro-1H-indol-3-ylidene)acetate

P. S. Kannan, P. S. Yuvaraj, K. Manivannan, B. S. R. Reddy and A. SubbiahPandi

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6′-(1,3-Diphenyl-1H-pyrazol-4-yl)-7′-(1H-indol-3-ylcarbonyl)-2-oxo-1-(prop-2-en-1-yl)-5′,6′,7′,7a'-tetrahydro-1′H-spiro[indoline-3,5′-pyrrolo[1,2-c][1,3]thiazole]-7′-carbonitrile

P. S. Kannan, D. Kathirvelan, B. S. R. Reddy, E. Govindan and A. SubbiahPandi

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(2E)-1-(5-Bromothiophen-2-yl)-3-(4-chlorophenyl)prop-2-en-1-one

H. D. Kavitha, K. R. Roopashree, S. B. Vepuri, H. C. Devarajegowda and V. B. Devaru

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Ammonium 2-(3,4-dimethylbenzoyl)benzoate dihydrate

M.-H. Zhang, Y.-L. Yuan and J.-F. Kou

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4′,4′,6′,6′-Tetrachloro-2-(6-methylpyridin-2-yl)-1H,2H-spiro[naphtho[1,2-e][1,3,2]oxazaphosphinine-3,2′-[1,3,5,2,4,6]triazatriphosphinine]

M. Işıklan, Ö. Sonkaya and T. Hökelek

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N,N-Diethyl-2-hydroxyethanaminium 5-(2,4-dinitrophenyl)barbiturate sesquihydrate

G. Mangaiyarkarasi and D. Kalaivani

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Tetraphenylphosphonium iodide–1,3,5-trifluoro-2,4,6-triiodobenzene–methanol (3/4/1)

G. Cavallo, P. Metrangolo, T. Pilati, G. Resnati and G. Terraneo

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1-(4-Hydroxyphenyl)-2-(2-oxidonaphthalen-1-yl)diazen-1-ium methanol hemisolvate

M. A. Benaouida, S. Chetioui and S. E. Bouaoud

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2-(Pyridin-4-yl)-1H-benzimidazole

D. K. Geiger and C. J. Bond

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Bis(2,3-dimethoxy-10-oxostrychnidinium) phthalate nonahydrate

P. Krishnan, K. Gayathri, N. Sivakumar, B. Gunasekaran and G. Anbalagan

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6-[(2,4-Dimethylanilino)methylidene]-2-hydroxycyclohexa-2,4-dienone

S. Shujah, S. Ali, Zia-ur-Rehman, M. N. Tahir and A. Meetsma

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Alternariol 9-O-methyl ether dimethyl sulfoxide monosolvate

S. Dasari, K. I. Miller, J. A. Kalaitzis, M. Bhadbhade and B. A. Neilan

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2-Chloro-1-(2,4,4-trimethyl-2,3,4,5-tetrahydro-1H-1,5-benzodiazepin-1-yl)ethanone

V. Thiruselvam, D. D. Rajakumari, A. Akila, S. Ponnuswamy and M. N. Ponnuswamy

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2-(4-Chlorophenyl)-4,5-diphenyl-1-(prop-2-en-1-yl)-1H-imidazole

S. K. Mohamed, M. Akkurt, A. A. E. Marzouk, F. Santoyo-Gonzalez and M. A. A. Elremaily

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6,8-Dibromo-3-nitro-2-phenyl-2H-chromene

L.-J. Yan and S.-Y. Zhang

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Ethyl 2,5-di-tert-butyl-5-ethoxy-4-oxo-4,5-dihydro-1H-pyrrole-3-carboxylate

G. M. Rosen, S. Muralidharan, P. Y. Zavalij, S. Fletcher and J. P. Y. Kao

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3β,6β-Diacetoxy-5,9α-dihydroxy-5α-cholest-7-en-11-one acetic acid 0.04-solvate

V. Piccialli, G. Oliviero, N. Borbone, R. Centore and A. Tuzi

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N′-[(E)-2-Hydroxy-5-methoxybenzylidene]pyridine-4-carbohydrazide monohydrate

M. K. Prasanna, M. Sithambaresan, K. Pradeepkumar and M. R. P. Kurup

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4-(Adamantan-1-yl)-2-(4-fluorophenyl)quinoline

Z. Kozubková, E. Babjaková, P. Bartoš and R. Vícha

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8-{(E)-[(4-Chlorophenyl)imino]methyl}-1,1,7,7-tetramethyl-1,2,3,5,6,7-hexahydropyrido[3,2,1-ij]quinolin-9-ol

E. N. Kantar, Y. Köysal, N. Akdemir, A. A. Ağar and M. S. Soylu

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1-Allyl-2-aminopyridin-1-ium bromide

T. Seethalakshmi, P. Venkatesan, M. Nallu, D. E. Lynch and S. Thamotharan

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Pyrimidine-4-carboxylic acid

K. Kiegiel, W. Starosta and J. Leciejewicz

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Ethyl 2-[4-(dimethylamino)phenyl]-1-phenyl-1H-benzimidazole-5-carboxylate

K. Y. Yeong, M. A. Ali, T. S. Choon, M. M. Rosli and I. A. Razak

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5-Cyclohexyl-2-(2-fluorophenyl)-3-methylsulfinyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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2-(1-Amino-4-tert-butylcyclohexyl)acetic acid (tBu-β^3,3-Ac₆c) hemihydrate

N. Ahmad Wani, V. K. Gupta, R. Kant, S. Aravinda and R. Rai

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2-{[3-Chloro-4-(4-chlorophenoxy)phenyl]iminomethyl}-4-nitrophenol

N. Karadayı, Y. Köysal, S. Şahin, E. Coşkun and O. Büyükgüngör

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6,12-Bis[(tricyclohexylsilyl)ethynyl]indeno[1,2-b]fluorene

B. D. Rose, L. N. Zakharov and M. M. Haley

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2-(4-Bromophenyl)-N-(pyrazin-2-yl)acetamide

P. S. Nayak, B. Narayana, J. P. Jasinski, H. S. Yathirajan and B. K. Sarojini

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8,13,26-Trioxa-23-thia-21-azapentacyclo[18.6.0.0^2,7.0^14,19.0^21,25]hexacosa-2(7),3,5,14,16,18-hexaene

S. K. Devi, T. Srinivasan, S. Purushothaman, R. Raghunathan and D. Velmurugan

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4-(2-Hydroxyphenyl)-3,5-dithiaheptanedioic acid

K. Ravichandran, R. Manikannan, S. Muthusubramanian, P. Ramesh and M. N. Ponnuswamy

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5-Cyclohexyl-3-(2-fluorophenylsulfinyl)-2-methyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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2-(4-Hydroxyphenyl)-3-methoxy-4H-chromen-4-one

I. E. Serdiuk, M. Wera, A. D. Roshal and J. Błażejowski

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1,2-Bis{2-[(4-methoxybenzylidene)amino]phenyl}disulfane

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5-Methyl-3-phenylisoxazole-4-carboxylic acid

Chandra, N. Srikantamurthy, G. J. Vishalakshi, S. Jeyaseelan, K. B. Umesha and M. Mahendra

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8,11,24-Trioxa-21-thia-19-azapentacyclo[16.6.0.0^2,7.0^12,17.0^19,23]tetracosa-2(7),3,5,12,14,16-hexaene

S. K. Devi, T. Srinivasan, S. Purushothaman, R. Raghunathan and D. Velmurugan

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N-[3-(Benzyldimethylazaniumyl)propyl]-N′,N′,N′′,N′′-tetramethylguanidinium bis(tetraphenylborate)

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2-(4-Bromophenyl)-N-(3,4-difluorophenyl)acetamide

A. S. Praveen, H. S. Yathirajan, J. P. Jasinski, A. C. Keeley, B. Narayana and B. K. Sarojini

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(Z)-N-tert-Butyl-2-(4-methoxyanilino)-N′-(4-methoxyphenyl)-2-phenylacetimidamide

S. A. Roberts, B. Saha, B. Frett and H.-Y. Li

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4-[(E)-(4-Ethoxybenzylidene)amino]phenol

N. Kaewmanee, S. Chantrapromma, N. Boonnak and H.-K. Fun

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N-[4-(Dimethylamino)benzylidene]-4-methylaniline

R. K. Balachandar, S. Kalainathan, S. M. Eappen and J. Podder

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1-[4-(Dimethylamino)benzylidene]-4-o-tolylthiosemicarbazide

R.-Y. Huang, Q.-J. Xu and L.-R. Lin

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5,5′-(Ethyne-1,2-diyl)diisophthalic acid dimethyl sulfoxide tetrasolvate

A. S. Münch, F. Katzsch, E. Weber and F. O. R. L. Mertens

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2-Amino-4-methylpyridinium 2-nitrobenzoate

S. Muralidharan, N. Elavarasu, T. Srinivasan, R. Gopalakrishnan and D. Velmurugan

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(E)-1,5-Diphenylpent-2-en-4-yn-1-one

A. S. Bunev, V. E. Statsyuk, N. V. Utekhina and V. N. Khrustalev

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5-(Naphthalen-1-yl)isophthalic acid–dimethyl sulfoxide–water (2/1/2)

A. Vetter, W. Seichter and E. Weber

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3,3′-{[(Biphenyl-2,2′-diyl)bis(methylene)]bis(oxy)}bis[N-(4-chlorophenyl)benzamide]

R. Rajadurai, R. Padmanabhan, S. S. Meenakshi Sundaram and S. Ananthan

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Thiophene-2-carbaldehyde azine

D. K. Geiger, H. C. Geiger and L. M. Szczesniak

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2-Acetylamino-1,3,4,6-tetra-O-(trimethylsilyl)-2-deoxy-α-D-glucopyranose

Z.-D. Cheng, Y.-L. Cui and J.-W. Mao

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1-[2-(Trityloxy)phenyl]ethanone

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Dimethyl 2-(4-methylbenzylidene)malonate

A. Barakat, A. M. Al-Majid, Y. N. Mabkhot, M. I. Choudhary and S. Yousuf

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5-Chloro-2-(4-fluorophenyl)-7-methyl-3-methylsulfinyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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1-Ethyl-2-phenyl-3-[2-(trimethylsilyl)ethynyl]-1H-indole

I. Baglai, V. Maraval, C. Duhayon and R. Chauvin

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3-Benzoyl-1-[4-(methylsulfanyl)phenyl]thiourea

R. de P. Castro, F. C. Macedo Jr, T. O. Brito, A. de Fátima and J. R. Sabino

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3,4-Bis[1-(prop-2-ynyl)-1H-indol-3-yl]-1H-pyrrole-2,5-dione

M.-H. Huang, Y.-C. Gao, F.-L. Yang and Y.-J. Luo

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2-Tosyl-2,3,3a,4,9,9a-hexahydro-1H-benzo[f]isoindol-1-one

M. Wu and Y.-M. Hu

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[(2R,3R)-3-(4-Nitrophenyl)aziridin-2-yl]methanol monohydrate

V. Gaumet, C. Denis, F. Leal, M. Madesclaire and V. P. Zaitsev

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4-Diphenylphosphanyl-8-methyl-1,5-naphthyridine

C. Chen, K.-Y. Wang, J.-F. Liu, D.-F. Wang and H.-J. Zhu

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6-Amino-2-methyl-8-phenyl-1,2,3,4-tetrahydroisoquinoline-5,7-dicarbonitrile

D.-C. Wang, H. Song and S. Yao

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N-(2-Methoxyphenyl)phthalamic acid

P. G. Waddell, R. J. Rutledge and J. M. Cole

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4-(4-Bromophenyl)-2-methylamino-3-nitro-5,6,7,8-tetrahydro-4H-chromen-5-one

P. Narayanan, J. Kamalraja, P. T. Perumal and K. Sethusankar

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(1S,3S,8R,9S,11R)-10,10-Dichloro-3,7,7,11-tetramethyltetracyclo[6.5.0.0^1,3.0^9,11]tridecane

A. Benharref, N. Ourhriss, L. El Ammari, M. Saadi and M. Berraho

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tert-Butyl N-[(3R,4R)-1-(2-cyanoacetyl)-4-methylpiperidin-3-yl]-N-methylcarbamate

M. Gehringer, M. Forster, D. Schollmeyer and S. Laufer

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3-{[5-(4-Chlorophenyl)-3-methyl-1H-pyrazol-1-yl]methyl}-4-m-tolyl-1H-1,2,4-triazole-5(4H)-thione

M. A. Farrukh, M. Ahmed, S. K. Mohamed, A. A. Marzouk and S. M. El-Moghazy

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(1R,2S,4S,4aS,8S,8aS)-4-Hydroxy-8,8a-dimethyl-10-oxo-2,3,4,7,8,8a-hexahydro-1H-4a,1-(epoxymethano)naphthalen-2-yl acetate

O. Selaïmia-Ferdjani, C. Bidjou-Haiour, A. Planchat and M. Pipelier

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Pyridine-4-carbaldehyde–fumaric acid (2/1)

B. Sandhu, S. Draguta, M. S. Fonari, M. Antipin and T. V. Timofeeva

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4-Hydroxy-1,2,6-trimethylpyridinium bromide monohydrate

T. Seethalakshmi, S. Manivannan, S. Dhanuskodi, D. E. Lynch and S. Thamotharan

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N-(5-Nitro-1,3-thiazol-2-yl)-4-(trifluoromethyl)benzamide

X.-W. Liu, H. Zhang, Y.-J. Yang, J.-Y. Li and J.-Y. Zhang

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1,3-Bis(prop-2-yn-1-yl)-1H-anthra[1,2-d]imidazole-2,6,11(3H)-trione

Z. Afrakssou, A. Haoudi, F. Capet, A. Mazzah, C. Rolando and L. El Ammari

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1-(Prop-2-en-1-yl)-3-{[3-(pyridin-4-yl)-4,5-dihydroisoxazol-5-yl]methyl}-1H-anthra[1,2-d]imidazole-2,6,11(3H)-trione

Z. Afrakssou, Y. Kandri Rodia, F. Capet, E. M. Essassi, C. Rolando and L. El Ammari

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Ethyl 4-anilino-2,6-bis(4-chlorophenyl)-1-phenyl-1,2,5,6-tetrahydropyridine-3-carboxylate

J. Yu, S. Tang, J. Zeng and Z. Yan

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N-tert-Butyl-2-(2,6-dichlorophenyl)imidazo[1,2-a]pyrazin-3-amine

Z. Fatima, T. Srinivasan, S. Koorathota, S. Thennarasu and D. Velmurugan

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Dimethyl 1,8-bis(4-methylphenyl)-11-oxatricyclo[6.2.1.0^2,7]undeca-2,4,6,9-tetraene-9,10-dicarboxylate

B. Balakrishnan, M. Nandakumar, P. R. Seshadri and A. K. Mohanakrishnan

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Acetoxy-γ-valerolactone

C. Tristram, G. J. Gainsford and S. Hinkley

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5-Isopropyl-5-methyl-2-sulfanylideneimidazolidin-4-one

M. Ichitani, S. Kitoh, S. Fujinami, M. Suda, M. Honda and K.-K. Kunimoto

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N-Benzyl-9-isopropyl-9H-purin-6-amine

D. Gergela, M. Rouchal, P. Bartoš and R. Vícha

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2-(4-Bromophenyl)-4-(4-methoxyphenyl)-6,7,8,9-tetrahydro-5H-cyclohepta[b]pyridine

Í. Çelik, M. Akkurt, H. Gezegen and C. Kazak

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L-Histidinium dipicrate dihydrate

M. Sethuram, M. V. Rajasekharan, M. Dhandapani, G. Amirthaganesan and M. NizamMohideen

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N,N-Dimethyldehydroabietylammonium chloride ethanol monosolvate

X.-Z. Huang, X.-P. Rao and Y.-J. Cui

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(E)-3-(3,4-Difluorophenyl)-1-(3,4-dimethoxyphenyl)prop-2-en-1-one

H.-P. Zhu, P.-T. Yu, Z. Wang, S.-L. Yang and Z.-G. Liu

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2-[(3,4-Dichlorobenzylidene)amino]-4-methylphenol

M. Kose, I. Gonul and V. McKee

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3-Benzyl-6-bromo-1H-imidazo[4,5-b]pyridin-2(3H)-one

Y. Kandri Rodi, A. Haoudi, F. Capet, A. Mazzah, E. M. Essassi and L. El Ammari

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2-(9H-Fluoren-9-yl)-4-(4-fluoroanilino)-4-oxobutanoic acid

T. Matviiuk, M. Baltas, Z. Voitenko, M. Gorichko and C. Lherbet

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2-[(Dimethylphenylphosphanylidene)azaniumyl]-5-methylbenzenesulfonate benzene monosolvate

C. T. Burns, S. Shang and M. S. Mashuta

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2,4,6-Trinitrophenyl 3-chlorobenzoate

R. Moreno-Fuquen, F. Mosquera, J. Ellena, C. A. De Simone and J. C. Tenorio

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N-[(2,6-Diethylphenyl)carbamothioyl]-2,2-diphenylacetamide

M. S. M. Yusof, N. R. Razali, S. Arshad, A. A. Rahman and I. A. Razak

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6-(4-Methylphenyl)-1,3,5-triazine-2,4-diamine–benzoic acid (1/1)

K. Thanigaimani, N. C. Khalib, I. A. Razak, P. Lavanya and K. Balasubramani

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6-(4-Methylphenyl)-1,3,5-triazine-2,4-diamine–4-methylbenzoic acid (1/1)

K. Thanigaimani, S. Arshad, I. A. Razak, D. Makeshvaran and K. Balasubramani

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1-(4-Chlorophenyl)-2-(1,3-diazepan-2-ylidene)ethanone

X.-W. Zhang, J.-H. Xia, Z.-H. Xu, L.-B. Wang and C.-Y. Yu

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6-[3-(p-Tolylsulfonylamino)propyl]diquinothiazine

M. Jeleń, A. Shkurenko, K. Suwińska, K. Pluta and B. Morak-Młodawska

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5-(6-Amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydropyrimidin-5-yl)-1,3-dimethyl-1H-chromeno[2,3-d]pyrimidine-2,4(3H,5H)-dione 3.5-hydrate

S. Roy and S. Das

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1,3,5-Tris(4-bromophenyl)-1,3,5-triazinane dichloromethane monosolvate

M. Chebbah, A. Bouchemma, S. Bouacida, L. Lefrada and M. Bouhenguel

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Ethyl 7-oxo-7H-benzo[de]imidazo[5,1-a]isoquinoline-11-carboxylate–trifluoroacetic acid (1/1)

R. T. Stibrany and J. A. Potenza

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5-Benzyloxy-3-methyl-1-tosyl-1H-indole

G. Pozza Silveira, A. G. Oliver and B. C. Noll

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Rupatadine

M. Kaur, J. P. Jasinski, Z. A. Luopa, N. Kumar, N. G. Patel, O. Gudaparthi and H. S. Yathirajan

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4-Cyano-1-methylpyridinium nitrate

C. A. McCormick, V. D. Nguyen, H. E. Renfro, L. V. Koplitz and J. T. Mague

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2,2′,5′,6-Tetrachloro-4-[(1S)-1-methylpropoxy]biphenyl

H.-J. Lehmler, H. Wu and S. Parkin

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{2-[(1,3-Benzothiazol-2-yl)methoxy]-5-bromophenyl}(phenyl)methanone

K. N. Venugopala, S. K. Nayak and B. Odhav

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(E)-9-(4-Fluorostyryl)-3,3,6,6-tetramethyl-3,4,5,6,7,9-hexahydro-2H-xanthene-1,8-dione

J. K. Lee, S.-J. Min, Y. S. Cho, J. H. Cha and S. O. Won

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[6-(Furan-2-yl)-7-nitro-2,3,4,6,7,8-hexahydro-1H-pyrido[1,2-a]pyrimidin-9-yl](phenyl)methanone

W.-F. Zhang, J.-H. Xia, Z.-H. Xu, L.-B. Wang and C.-Y. Yu

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Ethyl 5-methyl-3-phenylisoxazole-4-carboxylate

Chandra, K. Raghu, S. Jeyaseelan, K. B. Umesha and M. Mahendra

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2,4,5-Triphenyl-1-(prop-2-en-1-yl)-1H-imidazole

M. Akkurt, S. K. Mohamed, A. A. E. Marzouk, V. M. Abbasov and F. Santoyo-Gonzalez

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Methyl 2-[(2-chloroquinolin-3-yl)(hydroxy)methyl]acrylate

T. Anuradha, J. Srinivasan, P. R. Seshadri and M. Bakthadoss

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N,N′-Bis(4-hydroxyphenyl)pyridine-2,6-dicarboxamide dimethylformamide monosolvate

G. Waris, H. M. Siddiqi, U. Flörke, R. Hussain and M. S. Butt

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N′-Hydroxypyridine-2-carboximidamide–succinic acid (2/1)

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6a-Nitro-6-phenyl-6,6a,6b,7,8,9,10,12a-octahydrospiro[chromeno[3,4-a]indolizine-12,3′-indolin]-2′-one

S. K. Devi, T. Srinivasan, J. N. S. Rao, R. Raghunathan and D. Velmurugan

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2-(4-Methylpyridin-2-yl)-4′,4′,6′,6′-tetrakis(pyrrolidin-1-yl)-1H,2H-spiro[naphtho[1,2-e][1,3,2]oxazaphosphinine-3,2′-[1,3,5,2,4,6]triazatriphosphinine]

M. Işıklan, Ö. Sonkaya and T. Hökelek

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2-(4-Chlorophenyl)-N-(3,4-difluorophenyl)acetamide

A. S. Praveen, H. S. Yathirajan, J. P. Jasinski, A. C. Keeley, B. Narayana and B. K. Sarojini

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3-(2-Fluorophenylsulfinyl)-2,4,6-trimethyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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2-Benzoyl-4-chlorophenyl benzoate

B. Begum A, M. Al-Ghorbani, S. Sharma, V. K. Gupta and S. A. Khanum

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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