Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 70| Part 2

ISSN: 2056-9890

February 2014 issue

Highlighted illustration

Cover illustration: The compound C₁₁H₁₃NO₆ exhibits an intramolecular O-HO=C hydrogen bond between the N-hydroxyl H atom and carbonyl O atom of the neighboring acetyl group. This finding contradicts a previously published model in which the hydrogen bond was postulated to occur with the neighboring carbomethoxy group. This relatively strong hydrogen bond [O-HO: D = 2.5583 (11) Å and [theta] = 152°] may underlie the resistance of the title compound to oxidation into the corresponding nitroxide. See: Rosen, Muralidharan, Zavalij & Kao [Acta Cryst. (2014). E70, o110-o111].

inorganic compounds

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Redetermination of β-Ba(PO₃)₂

CCDC reference: 980403

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The mixed-metal tris(disulfide) thiophosphate, KNb_1.77Ta_0.23PS₁₀

Y. Lee, W. Yoon and H. Yun

CCDC reference: 980749

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β-Li_0.37Na_0.63Fe(MoO₄)₂

A. Souilem, M. F. Zid and A. Driss

CCDC reference: 965914

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K₉Y₃[Si₁₂O₃₂]F₂

V. Kahlenberg and T. Manninger

CCDC reference: 965914

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metal-organic compounds

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Diaqua{μ₂-N,N′-bis[(cyclohexanylidene)amino]oxamide}bis(triphenylphosphane)silver(I) dinitrate

R. Nimthong, N. Thepsena, W. Puetpaiboon and Y. Wattanakanjana

CCDC reference: 978377

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Poly[tetrakis(μ-1,1,1,3,3,3-hexafluoropropan-2-olato)iron(II)dipotassium]

A. P. Purdy and R. J. Butcher

CCDC reference: 979172

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(5-Methylpyrazine-2-carboxylato-κ²N¹,O)bis[2-(4-methylpyridin-2-yl-κN)-3,5-bis(trifluoromethyl)phenyl-κC¹]iridium(III) chloroform hemisolvate

Y.-I. Kim, Y.-K. Song and S. K. Kang

CCDC reference: 978885

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Bis(thiocyanato-κN)[tris(pyridin-2-ylmethyl)amine-κ⁴N]iron(II)

J.-W. Dai, Z.-Y. Li and O. Sato

CCDC reference: 979003

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trans-Tetracarbonylbis(triphenylphosphane-κP)molybdenum(0)

G. W. Waldhart and N. P. Mankad

CCDC reference: 980083

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catena-Poly[[aquabis(4-formylbenzoato-κ²O¹,O^1′)cadmium]-μ-pyrazine-κ²N:N′]

F. Çelik, N. Dilek, N. Çaylak Delibaş, H. Necefoğlu and T. Hökelek

CCDC reference: 979254

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μ-1,6,7,12-Tetraazaperylene-κ⁴N¹,N¹²:N⁶,N⁷-bis[chlorido(η⁶-p-cymene)ruthenium(II)] bis(hexafluoridophosphate) acetone disolvate

T. Brietzke, D. Kässler, A. Kelling, U. Schilde and H.-J. Holdt

CCDC reference: 980291

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[1,4-Bis(diphenylphosphanyl)butane-κ²P,P′]dibromidopalladium(II)

K. Ha and Y. S. Song

CCDC reference: 981207

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cis-Triaqua[1,1′-(propane-1,3-diyl)bis(pyridin-1-ium-4-carboxylato)-κO]bis(thiocyanato-κN)manganese(II) dihydrate

Q.-H. Tan and Y.-Q. Wang

CCDC reference: 981052

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Poly[μ₅-{hydrogen bis[(E)-cinnamato]}-caesium]

CCDC reference: 981265

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Tetrachloridodi-μ₃-oxido-tetrakis(μ₂-propan-2-olato-κ²O:O)ditin(II)ditin(IV)

O. Yarushnikov, D. Naumova, N. Klishin, E. Rusanov and O. Brusylovets

CCDC reference: 981323

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Poly[[diaquadeca-μ₂-cyanido-κ²⁰C:N-hexacyanido-κ⁶C-bis(μ₂-5-methylpyrimidine-κ²N:N′)bis(5-methylpyrimidine-κN)tricopper(II)ditungstate(V)] dihydrate]

Y. Tsunobuchi, S. Kaneko, K. Nakabayashi and S. Ohkoshi

CCDC reference: 979660

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Tetrakis(dipropylammonium) tetrakis(oxalato-κ²O¹,O²)stannate(IV) monohydrate: a complex with an eight-coordinate Sn^IV atom

N. Gueye, L. Diop and H. Stoeckli-Evans

CCDC reference: 979175

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(1-Methyl-1H-imidazole-κN³)(1-methyl-2-nitrosobenzene-κN)(5,10,15,20-tetraphenylporphyrinato-κ⁴N)iron(II) dichloromethane monosolvate

E. G. Abucayon, D. Awasabisah, D. R. Powell and G. B. Richter-Addo

CCDC reference: 981329

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Bis(1,10-phenanthrolin-1-ium) tetrachloridozincate monohydrate

E. Govindan, S. Thirumurugan, A. S. Ganeshraja, K. Anbalagan and A. SubbiahPandi

CCDC reference: 979772

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Tetrakis(μ₃-2-{[1,1-bis(hydroxymethyl)-2-oxidoethyl]iminomethyl}-6-nitrophenolato)tetracopper(II)

E. N. Chygorin, Y. O. Smal, V. N. Kokozay and I. V. Omelchenko

CCDC reference: 981257

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Di-μ-tricyanido-tetracyanidobis[hydrotris(pyrazoylborato)]tetramethanoldiiron(III)iron(II) dimethanol disolvate

K. Zhang and O. Sato

CCDC reference: 981575

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(Cyanido-κC)(2,2-diphenylacetamido-κ²N,O)bis(η⁵-pentamethylcyclopentadienyl)zirconium(IV)

L. Becker, A. Spannenberg, P. Arndt and U. Rosenthal

CCDC reference: 981857

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Tetrakis[bis(pyridin-2-yl)amine-κN²](nitrato-κO)silver(I)

Y. Parashchenko, A. Pavlishchuk, N. A. Bokach and M. Haukka

CCDC reference: 981511

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Chlorido[5-methoxy-1H-benzimidazole-2(3H)-thione-κS]bis(triphenylphosphane-κP)copper(I) methanol disolvate

CCDC reference: 982066

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[1H-1,2,4-Triazole-5(4H)-thione-κS]bis(triphenylphosphane-κP)(nitrato-κO)silver(I) methanol monosolvate

Y. Wattanakanjana, S. Palamae, J. Ratthiwan and R. Nimthong

CCDC reference: 981946

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Bis(n-dodecylammonium) bis(chloranilato)diethanolcuprate(II)

A. Himegi and S. Kawata

CCDC reference: 981983

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catena-Poly[[diaquabis(4-formylbenzoato-κO¹)nickel(II)]-μ-pyrazine-κ²N:N′]

F. Çelik, N. Dilek, N. Çaylak Delibaş, H. Necefoğlu and T. Hökelek

CCDC reference: 982792

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Tris(2,6-dibenzoyl-4-methylphenolato-κ²O¹,O²)cobalt(III)

A. K. Gupta, S. Srivastava and R. J. Butcher

CCDC reference: 982976

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catena-Poly[[(N,N-dimethylcyanamide-κN)lithium]-μ₃-bromido]

Q. Xie, H. Tong and M. Zhou

CCDC reference: 982978

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[μ-3,3′-Diisopropyl-1,1′-(propane-1,3-diyl)bis(1,3-diazinan-2-ylidene)]bis[bromido(η⁴-cycloocta-1,5-diene)rhodium(I)]

G. M. Pawar, K. Wurst, D. Wang and M. Buchmeiser

CCDC reference: 981713

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Hydrido(prolinato-κ²N,O)tris(trimethylphosphane-κP)iridium(III) hexafluoridophosphate

J. S. Merola and C. P. Roy

CCDC reference: 983575

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1-(4-Hydroxyphenyl)piperazine-1,4-diium tetrachloridocobalt(II) monohydrate

M. Mghandef and H. Boughzala

CCDC reference: 949157

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μ-Cyanido-κ²C:N-dicyanido-κ²C-bis(N-ethylethylenediamine-κ²N,N′)copper(II)copper(I)

P. W. R. Corfield and J. F. Michalski

CCDC reference: 983245

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organic compounds

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N-(3-Chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-N-propionylpropionamide

N. Idris, R. J. Butcher and O. Bakare

CCDC reference: 978208

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8-{1-[(4′-Fluoro-[1,1′-biphenyl]-4-yl)methyl]piperidin-4-yl}-3,4-dihydroquinolin-2(1H)-one chloroform 0.25-solvate

N. Ullah and H. Stoeckli-Evans

CCDC reference: 978441

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1-Carboxynaphthalen-2-yl acetate monohydrate

B. S. Souza, A. J. Bortoluzzi and F. Nome

CCDC reference: 978267

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1-[6-(1H-Indol-1-yl)pyridin-2-yl]-1H-indole-3-carbaldehyde

C. Ramathilagam, P. R. Umarani, N. Venkatesan, P. Rajakumar, B. Gunasekaran and V. Manivannan

CCDC reference: 978294

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1-[(4-Hydroxyanilino)methylidene]naphthalen-2(1H)-one

S. Chahmana, F. Benghanem, S. Keraghel and A. Ourari

CCDC reference: 978464

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2,6-Dichloro-9-(2′,3′,5′-tri-O-acetyl-β-D-ribofuranosyl)-9H-purine

I. Novosjolova, D. Stepanovs, Ē. Bizdēna, A. Mishnev and M. ¯ Turks

CCDC reference: 968101

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Dimethyl 5-acetyl-1-hydroxy-4-methyl-1H-pyrrole-2,3-dicarboxylate, an oxidation-resistant N-hydroxypyrrole

G. M. Rosen, S. Muralidharan, P. Y. Zavalij and J. P. Y. Kao

CCDC reference: 978380

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(E)-2-(4-Benzyloxy-2-hydroxybenzylidene)-N-methylhydrazinecarbothioamide

N. R. Sajitha, M. Sithambaresan and M. R. P. Kurup

CCDC reference: 979062

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16-Oxapentacyclo[6.6.5.0^1,18.0^2,7.0^9,14]nonadeca-2,4,6,9,11,13,18-heptaen-15-one

E. M. Mathew, M. Sithambaresan, P. A. Unnikrishnan and M. R. P. Kurup

CCDC reference: 979286

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N′-[(1E)-1-(2-Fluorophenyl)ethylidene]pyridine-3-carbohydrazide

P. B. Sreeja, M. Sithambaresan, N. Aiswarya and M. R. P. Kurup

CCDC reference: 979240

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Ethyl 2-{5-[(3-oxo-3,4-dihydro-2H-1,4-benzothiazin-4-yl)methyl]-1H-1,2,3-triazol-1-yl}acetate

N. K. Sebbar, A. Zerzouf, E. M. Essassi, M. Saadi and L. El Ammari

CCDC reference: 978857

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2,2′-(1,4-Phenylene)bis(propane-2,2-diyl) bis(benzodithioate)

R. Moreno-Fuquen, C. Grande, R. C. Advincula, J. C. Tenorio and J. Ellena

CCDC reference: 978819

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1,3,5-Tris(4-methoxyphenyl)-1,3,5-triazinane-2,4,6-trione

L. Fang, F. Li and X. Luo

CCDC reference: 979026

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(R)-N-[(R)-2,2-Dichloro-1-phenyl-2-(phenylsulfonyl)ethyl]-2-methylpropane-2-sulfinamide

H. Huang, Y. Li and J. Chu

CCDC reference: 979063

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(2R,3S,4R,5R)-5-(4-Amino-5-iodo-7H-pyrrolo[2,3-d]pyrimidin-7-yl)-4-fluoro-2-(hydroxymethyl)tetrahydrofuran-3-ol

W. Li, R. Yang and Q. Xiao

CCDC reference: 979239

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2-(3,4-Dimethoxyphenyl)-4-(thiophen-2-yl)-2,3-dihydro-1,5-benzothiazepine

B. C. Manjunath, M. Manjula, K. R. Raghavendra, S. Shashikanth, K. Ajay Kumar and N. K. Lokanath

CCDC reference: 978715

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1,3,5-Tri-p-tolylpentane-1,5-diol

A. Thiruvalluvar, R. Chithiravel, S. Muthusubramanian and R. J. Butcher

CCDC reference: 979742

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1-Fluoro-4-[(E)-2-nitrovinyl]benzene

S. Sreenivasa, M. S. Nanjundaswamy, K. E. Manojkumar, S. Madankumar, N. K. Lokanath and P. A. Suchetan

CCDC reference: 980205

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2-[(E)-2-(3,4-Dichlorobenzylidene)hydrazin-1-yl]quinoxaline

T. C. M. Noguiera, A. C. Pinheiro, M. V. N. de Souza, J. L. Wardell and E. R. T. Tiekink

CCDC reference: 980593

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(E)-3-[(Dimethylamino)methylidene]-4-phenyl-1H-1,5-benzodiazepin-2(3H)-one

M. Loughzail, A. Baouid, J. A. Fernandes, M. Driss and E. H. Soumhi

CCDC reference: 978905

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Bis[3-methyl-5-(pyridin-2-yl)-1H-pyrazol-4-yl] selenide methanol hemisolvate

M. Seredyuk, N. O. Sharkina, E. Gumienna-Kontecka and A. A. Kapshuk

CCDC reference: 978770

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Diethylammonium dihydrogen orthophosphate

CCDC reference: 980665

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2,3-Bis{[2,3-dimethyl-6-(phenylvinyl)phenyl]imino}butane

J. Zhao, J. Yuan, W. Xu, J. Chen and Y. Mu

CCDC reference: 980626

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2-{[2-(2-Hydroxy-5-methoxybenzylidene)hydrazin-1-ylidene]methyl}-4-methoxyphenol

M. Taha, S. A. A. Shah, S. Sultan, N. H. Ismail and S. Yousuf

CCDC reference: 978781

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4,4′-({[(Pyridine-2,6-diyl)bis(methylene)]bis(oxy)}bis(methylene))dibenzonitrile

B. M. Yamin, N. A. Kamalulazmy and N. I. Hassan

CCDC reference: 979689

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2,3-Diphenyl-2,3,5,6-tetrahydro-4H-1,3-thiazin-4-one

H. P. Yennawar and L. J. Silverberg

CCDC reference: 980096

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1,3,4-Tri-O-acetyl-2-N-(trifluoroacetyl)-β-L-fucose

D. C. McCutcheon, P. Norris and M. Zeller

CCDC reference: 979173

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Ethyl 6-(4-cyclopropyl-1H-1,2,3-triazol-1-yl)pyridine-3-carboxylate

M. N. Ahmed, K. A. Yasin, M. N. Tahir, A. Bibi and H. Andleeb

CCDC reference: 978828

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2,6-Bis(4-methoxyphenyl)-1,4-dithiine

S.-S. Zhao, Q. Su, Z.-H. Peng and D.-L. An

CCDC reference: 969198

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Acta Cryst. (2014). E70, o138
doi: 10.1107/S1600536813034880