Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 64| Part 3

ISSN: 2056-9890

March 2008 issue

Highlighted illustration

Cover illustration: Dichloridobis(methylamine- [kappa] N)boron(III) chloride is the first crystallographically characterized di(alkylamine)-BCl₂⁺ salt. The boron atom is tetrahedrally coordinated and, in the crystal structure, cations and anions are linked by N-HCl hydrogen bonds, resulting in a layered structure. See Weinmann, Nuss & Jansen [Acta Cryst. (2008), E64, o583].

inorganic compounds

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α-Lead tellurite from single-crystal data

V. E. Zavodnik, S. A. Ivanov and A. I. Stash

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A quaternary germanium(II) phosphate, Na[Ge₄(PO₄)₃]

C.-S. Lee and S.-F. Weng

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The solid solution Na_0.39(NH₄)_1.61SO₄·Te(OH)₆

L. Ktari, M. Abdelhedi, M. Dammak, A. Cousson and A. Kolsi

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Tetrapotassium cis-dioxido-trans-bis(sulfato-κO)sulfato(κ²O,O′)molybdate(VI)

S. J. C. Schäffer and R. W. Berg

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A new sodium dimangnesium trivanadate, NaMg₂V₃O₁₀

B. Ayed and A. Haddad

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Reinvestigation of the crystal structure of lautite, CuAsS

L. Bindi, T. Catelani, L. Chelazzi and P. Bonazzi

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metal-organic compounds

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[N,N′-(1,2-Diphenylethane-1,2-diyl)bis(pyridine-2-carboxamidato)]nickel(II) diethyl ether hemisolvate

L. Yang, D.-Y. Deng, M. Li and X.-G. Zhou

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catena-Poly[[bis[2-(2,3-dimethylanilino)benzoato-κO]cadmium(II)]-di-μ-3-pyridylmethanol-κ²N:O;κ²O:N]

J. Moncol, D. Mikloš, P. Segľa, M. Koman and T. Lis

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cis,trans-Dicarbonyldichlorido[2-(2-pyridyl)-1,8-naphthyridine-κN¹,N²]ruthenium(II)

D. Oyama and T. Hamada

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1,4-Diferrocenylbutane-1,4-dione

M. Tombul, A. Bulut, K. Güven and O. Büyükgüngör

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Tetraaquabis(4-formylbenzoato-κO)cobalt(II) tetrahydrate

Z.-P. Deng, S. Gao, L.-H. Huo and S. W. Ng

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Diaquabis(4-formylbenzoato-κO)zinc(II)

Z.-P. Deng, S. Gao, L.-H. Huo and S. W. Ng

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Poly[μ₄-succinato-μ₂-succinato-bis[diamminecopper(II)]]

S. Jin, D. Wang, Y. Yu, G. Luo and Y. Ye

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(4-Formyl-2-methoxyphenolato)tris(2-methyl-2-phenylpropyl)tin(IV)

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Poly[tetraaquabis(μ₂-2,4,6-trinitrophenolato)barium(II)]

C. Vesta, R. Uthrakumar, S. Jerome Das and B. Varghese

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Diacetato[N,N′-bis(2-pyridylmethylidene)cyclohexane-1,2-diamine]manganese(II) hexahydrate

I.-C. Hwang and K. Ha

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A second polymorph of [1,2-bis(di-tert-butylphosphino)ethane]dichloridoplatinum(II)

A. Gunay, W. W. Brennessel and W. D. Jones

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Dichlorido(9-methyladenine-κN⁷)(η⁵-pentamethylcyclopentadienyl)iridium(III) dichloromethane solvate

C. Bruhn, T. Küger and D. Steinborn

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Dichlorido[(S)-(1-phenylethyl)(2-pyridylmethyl)amine-κ²N,N′]zinc(II)

Q. T. Nguyen and J. H. Jeong

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Diaquabis(4-bromobenzoato-κ²O,O′)zinc(II)

T. Hökelek, N. Çaylak and H. Necefoğlu

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Bis(4-fluorobenzoato-κ²O,O′)bis(nicotinamide-κN¹)zinc(II) monohydrate

T. Hökelek, N. Çaylak and H. Necefoğlu

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Poly[ethanolbis(μ₃-2-thioxo-1,2-dihydropyridin-1-olato)dilithium(I)]

J. Hartung, N. Schneiders, I. Svoboda and H. Fuess

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trans-Carbonylchloridobis(tri-p-tolylphosphine)rhodium(I) acetone solvate

F. Lorenzini, B. O. Patrick and B. R. James

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Guanidinium (aqua-2κO)(4-hydroxy-6-carboxypyridine-2-carboxylato-2κ³O²,N,O⁶)(μ-4-hydroxypyridine-2,6-dicarboxylato-1:2κ⁴O²,N,O⁶:O²)(4-hydroxypyridine-2,6-dicarboxylato-1κ³O²,N,O⁶)dizincate(II) dihydrate

H. Aghabozorg, S. Saadaty, E. Motyeian, M. Ghadermazi and F. Manteghi

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Poly[diaquapentakis(μ₄-benzene-1,2-dicarboxylato)(μ₃-benzene-1,2-dicarboxylato)tetrathulium(III)]

G.-M. Wang, C.-S. Duan, H.-L. Liu and H. Li

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catena-Poly[[silver(I)-μ-[N-(4-pyridylmethyl)pyridine-4-carboxamide-κ²N:N′]] nitrate monohydrate]

Y.-T. Ma, B.-W. Sun and S. W. Ng

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Dichloridobis[(S)-2-hydroxypropionamide-κ²O,O′]manganese(II)

P. Lemoine, B. Viossat, J. D. Brion and A. Bekaert

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μ₂-Iodido-bis{dimethyl[methylbis(quinolin-8-yl)silanyl-κ³N,Si,N′]platinum(IV)} tetrakis(pentafluorophenyl)borate dichloromethane 0.66-solvate

C. A. M. Carr, C. W. Gribble and M. I. Gibson

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Di-μ-tert-butanolato-bis[bis(η⁵-cyclopentadienyl)erbium(III)]

S. Pagano and W. Schnick

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Ammonium tris(tetraethylammonium) hexacosaoxidooctamolybdate

I. Zebiri, L. Bencharif, A. Direm, M. Bencharif and N. Benali-Cherif

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Diaquabis(5-carboxy-2-methyl-1H-imidazole-4-carboxylato-κ²N³,O⁴)manganese(II)

J.-Z. Zeng, X.-G. Yi, J.-Y. Lin, S.-M. Ying and G.-S. Huang

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{N,N-Bis[2-(trimethylsilylamino)ethyl]-N′-(trimethylsilyl)ethane-1,2-diaminato(3–)-κ⁴N}methylzirconium(IV)

S. N. MacMillan, J. M. Tanski and R. Waterman

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catena-Poly[[tetrakis(hexamethylphosphoramide-κO)bis(nitrato-κ²O,O′)neodymium(III)] [silver(I)-di-μ₂-sulfido-tungsten(VI)-di-μ₂-sulfido]]

G. Tang, J. Zhang and C. Zhang

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{2,2′-[1,1′-(3-Azapentane-1,5-diyldinitrilo)diethylidyne]diphenolato}(piperidine)cobalt(III) tetraphenylborate

S. Meghdadi, K. J. Schenk, M. Amirnasr and F. Fadaee

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Dichlorido-1κCl,3κCl-bis{μ-2,2′-[propane-1,3-diylbis(iminomethylene)]diphenolato}-1:2κ⁶O,N,N′,O′:O,O′;2:3κ⁶O,O′:O,N,N′,O′-tricopper(II)

B. M. Ateş, F. Ercan, I. Svoboda, H. Fuess and O. Atakol

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μ₃-Carbonato-κ³O:O′:O′′-tris{(η⁶-benzene)[(R)-1-(1-aminoethyl)naphthyl-κ²C²,N]ruthenium(II)} hexafluoridophosphate dichloromethane solvate

J.-B. Sortais, L. Brelot, M. Pfeffer and L. Barloy

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Bis(2,6-dimethylpyridinium) tetrabromidocobaltate(II)

B. F. Ali, R. H. Al-Far and S. F. Haddad

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cis-Dichlorido[4,4,5,5-tetramethyl-2-(2-pyridyl)-2-imidazoline-1-oxyl]palladium(II) tetrahydrofuran hemisolvate

S. Badeche, D. A. Rouag, S. Benmebarek, S.-E. Bouaoud and S. Golhen

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Tetrakis[(benzene-18-crown-6)potassium]bis[tris(thiocyanato)copper(I)]

X.-M. Song, X.-Q. Huang, J.-M. Dou and D.-C. Li

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[2-(Phenyldiazenyl)pyrrolato]bis(2-pyridylphenyl)iridium(III)

W.-Y. Li, L.-S. Mao, L. Lu and H.-W. He

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Poly[triaquabis(μ₂-3-carboxypyrazine-2-carboxylato)dilithium(I)]

M. Tombul, K. Güven and O. Büyükgüngör

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Diammonium diaquabis(malonato-κ²O,O′)cobaltate(II) dihydrate

H. Xu and F. Wang

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Bis[2-(3-cyanophenyliminomethyl)phenolato]nickel(II)

X.-X. Gong, R. Xia and H.-J. Xu

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(Dicyanamido)[tris(2-pyridylmethyl)amine]zinc(II) perchlorate

H. Li, H. Y. Zhao and S. G. Zhang

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μ-Hydroxido-bis[(2,2′-bipyridine)tricarbonylrhenium(I)] perrhenate

K. Ruth, T. Morawitz, H.-W. Lerner and M. Bolte

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Tetrakis(μ-pivalato-κ²O:O′)bis[(2-methylpyridine-κN)iron(II)](Fe—Fe)

J. Overgaard, G. A. Timco and F. K. Larsen

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catena-Poly[[bis[μ-2-(3-pyridyl)-1H-benzimidazole]-κ²N²:N³;κ²N³:N²-disilver(I)]-μ-2,5-dicarboxybenzene-1,4-dicarboxylato-κ²O²:O⁵]

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Diaqua(2,6-dioxo-1,2,3,6-tetrahydropyrimidin-3-ide-4-carboxylato-κ²N³,O⁴)(1,10-phenanthroline-κ²N,N′)manganese(II)

R. Wu, Y. Huo, J. Li and Z. Zheng

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{2,2′-[4-Methyl-4-azaheptane-1,7-diylbis(nitrilomethylidyne)]diphenolato}zinc(II)

X.-S. Tai, Y.-M. Feng and H.-X. Zhang

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Tris(N-benzoyl-N′,N′-diphenylthioureato-κ²O,S)cobalt(III)

H. Pérez, Y. Mascarenhas, A. M. Plutín, R. de Souza Corrêa and J. Duque

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Bis{μ-2,2′-[o-phenylenebis(nitrilomethylidyne)]diphenolato}dicopper(II) N,N′-dimethylformamide disolvate

G. Yu, Y. Ding, L. Wang, Z. Fu and X. Hu

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Diaquabis(4-chlorobenzoato-κO)bis(N,N-diethylnicotinamide-κN¹)manganese(II)

T. Hökelek, N. Çaylak and H. Necefoğlu

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organic compounds

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4-(5-tert-Butyl-1,3-dithian-2-yl)-5-chloro-2-phenyl-1,3-oxazole

Y. Cui, L. Liu, M. Liu, Y. Duan and S. Liu

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9,9′-Dibromo-9,9′-bifluorene

Y. Mizuhata and N. Tokitoh

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3,8-Bis(4-chlorophenyl)-4,7-dimethyltricyclo[4.2.2.0^2,5]deca-3,7-diene

M. Tomura and Y. Yamashita

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1,5-Bis(2-formylphenoxy)-3-oxapentane

N. C. F. Dionysio, J. Bordinhão, L. do C. Visentin and C. M. Ronconi

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3-Benzyl-5-bromopyrazin-2(1H)-one

J. Alen and L. Dobrzańska

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8-Hydroxy-8-phenyl-2,3,7,8-tetrahydro-6H-1,4-dioxino[2,3-f]isoindol-6-one

V. A. Tafeenko, L. A. Aslanov, M. I. Khasanov and S. S. Mochalov

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N-(n-Decyl)-4-nitroaniline

M. M. Yonkey, C. P. Walczak, P. J. Squattrito, D. K. Mohanty and K. Kirschbaum

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tert-Butyl N-[(S)-3-isopropyl-2-oxooxetan-3-yl]carbamate

L. Sieroń, A. Kudaj, A. Olma and J. Karolak-Wojciechowska

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3,6-Diacetyl-1,4-diphenyl-1,4-dihydro-1,2,4,5-tetrazine

M. Al-Noaimi and S. F. Haddad

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3-[(E)-4-Methoxybenzylidene]-1-methylpiperidin-4-one

D. Gayathri, D. Velmurugan, R. R. Kumar, S. Perumal and K. Ravikumar

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N,N-Dimethyl-3-(1-naphthyloxy)-3-(2-thienyl)propan-1-amine

X. Tao, X.-Q. Zhang, L. Yuan and J.-T. Wang

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Racemic 4-(4-tert-butylphenyl)-2,6-dimethylcyclohex-3-enecarboxylic acid

S. Xie, C. R. O'Hearn and P. D. Robinson

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Acta Cryst. (2008). E64, o555
doi: 10.1107/S1600536808003164