Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 68| Part 11

ISSN: 2056-9890

November 2012 issue

Highlighted illustration

Cover illustration: Having enhanced potency, selectivity, and duration of action, the title opioid salvinorin A derivative, C₂₃H₃₀O₈, also exhibits surprising structural mimicry with salvinorin A. This arises as the ether residue adopts a gauche-gauche conformation which traces a helix around the acetate group of salvinorin A. See: Munro, Ho & Cohen [Acta Cryst. (2012). E68, o3225-o3226].

inorganic compounds

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LiNa₅Mo₉O₃₀

H. Hamza, I. Ennajeh, M. F. Zid and A. Driss

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Redetermination of (NH₄)₂HAsO₄

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Redetermination of dysprosium trinickel from single-crystal X-ray data

V. Levytskyy, V. Babizhetskyy, B. Kotur and V. Smetana

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Tetraamminelithium triamminelithium trisulfide, [Li(NH₃)₄][Li(NH₃)₃S₃]

C. Guentner and N. Korber

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Redetermination of durangite, NaAl(AsO₄)F

G. W. Downs, B. N. Yang, R. M. Thompson, M. D. Wenz and M. B. Andrade

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metal-organic compounds

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Bis(chlorido)(dimethylsulfoxide-κO)barium(II)

F. Gschwind and M. Jansen

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Bis(2,4,6-trimethylpyridinium) tetrabromidozincate

B. F. Ali, S. F. Haddad and R. Al-Far

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Bis[4-(dimethylamino)pyridinium] octaaquachloridolanthanum(III) tetrachloride trihydrate

M. Benslimane, H. Merazig, J.-C. Daran and O. Zeghouan

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N,N′-bis[(3-hydroxy-4(4H)-oxypyran-2-yl)methyl]-N,N′-dimethylethylene-1,2-diammonium tetrachloridoplatinate(II) dihydrate

V. Fusi, L. Giorgi, E. Macedi, P. Paoli and P. Rossi

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2-Aminopyridinium trans-diaquabis(oxalato-κ²O,O)chromate(III)

J. Nenwa, G. Bebga, S. Martin, M. M. Bélombé, M. Mbarki and B. P. T. Fokwa

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Trichlorido(6-methyl-2,2′-bipyridine-κ²N,N′)(dimethylsulfoxide-κO)indium(III)

S. A. Shirvan, S. Haydari Dezfuli, E. Golabi and M. A. Gholamzadeh

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Bis[5-(pyridin-2-yl)pyrazine-2-carbonitrile-κ²N⁴,N⁵](trifluoroacetato-κO)silver(I)

J. Li, X. C. Jia, J. Qi, Y. Y. Liu and Y. Ding

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trans-Dichloridobis[dicyclohexyl(2,4,6-trimethylphenyl)phosphane-κP]palladium(II)

I. Buthelezi, H. Chiririwa, H. Ogutu and R. Meijboom

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Dichlorido(6-methyl-2,2′-bipyridine-κ²N,N′)cobalt(II)

N. Akbarzadeh Torbati, A. R. Rezvani and H. Saravani

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Trans-bis(3-tert-butylpyridine-κN)bis(4-tert-butylpyridine-κN)bis(thiocyanato-κN)manganese(II)

T. Reinert, I. Jess and C. Näther

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Poly[tetrabutyltetrakis(μ₂-hydrogen phenylphosphonato)ditin(IV)]

M. Sarr, A. Diasse-Sarr, L. Diop, K. C. Molloy and G. Kociok-Kohn

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Bis[2,3,4-trimethyl-5-[(3,4,5-trimethyl-2H-pyrrol-2-ylidene-κN)methyl]-1H-pyrrolato-κN]copper(II)

S. S. Erdem, F. R. Fronczek and S. F. Watkins

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μ₂-Oxalato-bis[triphenyl(thiourea-κS)tin(IV)]

Y. Sow, L. Diop, K. C. Molloy and G. Kociok-Kohn

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Poly[(μ-1,3-thiocyanato-κN,S)(isonicotinato-κN,O)(ethanol-κO)cadmium(II)]

T. Neumann, J. Werner, I. Jess and C. Näther

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Tetrakis(μ-acetato-κ²O:O′)-bis[(3-pyridinecarboxaldehyde-κN′)]dicopper(II)(Cu—Cu)

A. Cruz-Enriquez, A. Baez-Castro, H. Höpfl, M. Parra-Hake and J. J. Campos-Gaxiola

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Bis[4,4,5,5-tetramethyl-2-(pyridin-2-yl-κ²N)imidazoline-1-oxyl 3-oxide-κO]tris(nitrato-κ²O,O′)terbium(III)

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Tris[4-(dimethylamino)pyridinium][(bis-μ-dichlorido)-decaaquadichloridodineodymium(III)] pentachloride dihydrate

M. Benslimane, H. Merazig, J.-C. Daran and O. Zeghouan

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Tetrakis(5,7-dimethylquinolin-8-olato-κ²N,O)zirconium(IV) dimethylformamide disolvate

M. Steyn, H. G. Visser and A. Roodt

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[Hydridotris(pyrazol-1-yl-κN²)borato]bis(methylamino-κN)(triphenylphosphine-κP)ruthenium(II) chloride dichloromethane solvate monohydrate

Y.-D. Lin, C.-P. Chang, Q.-S. Huang and Y.-H. Lo

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Bis(2,2′-bipyrimidine-κ²N¹,N^1′)palladium(II) bis(tetrafluoroborate) acetonitrile monosolvate

A. Duong, J. D. Wuest and T. Maris

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Poly[aqua(μ₂-pyrimidine-2-carboxylato-κ⁴O,N:O′,N′)(nitrato-κO)cadmium]

O. In-noi, K. Chainok and D. J. Harding

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trans-Dichloridobis(4-nitroaniline-κN¹)palladium(II)

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(Acetato-κO)(acetato-κO,O′)bis(1,3-diazinane-2-thione-κS)cadmium(II)

R. Mahmood, S. Ghulam Hussain, M. Fettouhi, A. A. Isab and S. Ahmad

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Bis(diphenyl-p-tolylphosphane-κP)(2-hydroxy-3,5,7-bromocyclohepta-2,4,6-trienonato-κ²O,O′)copper(I)

N. I. Barnard and T. N. Hill

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Bis[μ-(3-acetyl-2-hydroxy-6-methyl-4H-pyran-4-one-κ³O:O′,O′′)]diaquatetrakis(pyridine-κN)dicopper(II) diperchlorate

A. Ourari, W. Derafa, S. Bouacida, D. Aggoun and J.-C. Daran

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Potassium N-bromo-2-nitrobenzenesulfonamidate monohydrate

B. T. Gowda, S. Foro and H. S. Spandana

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(μ₁-Methanolato-κ¹O)-μ₁-methoxo-κ¹O-(μ₂-2-amino-1-methyl-5H-imidazol-4-one-κ²N:N′)-hexacarbonyldirhenium(I)

M. Schutte, H. G. Visser and A. Roodt

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(Ammine)(carbonyl)[hydridotris(pyrazol-1-yl-κN²)borato](triphenylphosphine-κP)ruthenium(II) chloride dichloromethane disolvate

T.-C. Hu, J.-X. Ye, S.-T. He, G.-R. Chiang and Y.-H. Lo

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Dibromido(6,6′-dimethyl-2,2′-bipyridine-κ²N,N′)cobalt(II)

S. A. Shirvan, S. Haydari Dezfuli, F. Khazali, M. Aghajeri and A. Borsalani

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Poly[di-μ₃-hydroxy[μ₄-5-(4-carboxyphenyl)pyridine-2-carboxylato-κ⁵N,O²:O^2′:O⁴:O^4′]dicadmium]

F.-J. Meng, H.-Q. Jia, N.-H. Hu and H. Zhou

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(μ₂-Chlorido)-(μ₂-pyridine-2-carboxylato-1:2κN,O:O)-dichlorido(ethanol-κO)bis[N-hydroxy-1-(pyridin-2-yl)methanimine-κ²N,N′]dicobalt(II)

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[Bis[μ-bis(diphenylphosphino)methane-1:2κ²P:P′]-bis(nitrito-κ²O,O′)]disilver(I) acetonitrile disolvate

X. Yang, X. Huang, Q.-M. Qiu, Q.-H. Jin and C.-L. Zhang

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Potassium N-bromo-2,4-dichlorobenzenesulfonamidate sesquihydrate

B. T. Gowda, S. Foro and H. S. Spandana

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catena-Poly[[tetraaqua-μ-aqua-bis(μ₄-pyrimidine-2-carboxylato)tetralithium] dichloride]

W. Starosta and J. Leciejewicz

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Sodium pentafluorophenylborate

H. Vitze, H.-W. Lerner and M. Bolte

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Bis(3-tert-butylpyridine-κN)bis(4-tert-butylpyridine-κN)bis(thiocyanato-κN)cadmium

T. Reinert, I. Jess and C. Näther

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Bis[4-(4-bromophenylimino-κN)pent-2-en-2-olato-κO]copper(II)

P. S. E. Bungu, M. Schutte and G. Steyl

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μ-(2,2′-Bipyrimidine)-bis[dichloridopalladium(II)] dimethylformamide monosolvate

C. Young, A. Roodt and B. C. B. Bezuidenhoudt

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Triaqua(cyclohex-4-ene-1,2-dicarboxylato-κO¹)(1,10-phenanthroline-κ²N,N′)cobalt(II)

H.-Y. Li, C. Wang, F.-P. Huang and Y.-M. Jiang

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Bis(acetato-κ²O,O′)(4,4′-dimethyl-2,2′-bipyridine-κ²N,N′)zinc

M. A. Harvey, S. A. Suarez, A. Ibañez, F. Doctorovich and R. Baggio

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Bis(μ-3-nitrobenzene-1,2-dicarboxylato)-κ⁴O¹,O²:O¹,O^1′;κ⁴O¹,O^1′:O¹,O²-bis[triaqua(6-carboxy-2-nitrobenzoato-κ²O¹,O⁶)neodymium(III)] dihydrate

Y. Chang, Z. Pei and Q. Shuai

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Poly[dibutylammonium [nonamethylbis(μ₃-sulfato-κ³O:O′:O′′)tristannate(IV)]]

T. Diop, L. Diop and A. van der Lee

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3′-Ferrocenylcarbonyl-1′-methyl-4′-phenylspiro[indeno[2,3-b]quinoxaline-11,2′-pyrrolidine]

B. Vijayakumar, D. Gavaskar, T. Srinivasan, R. Raghunathan and D. Velmurugan

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Dimethylbis(pyrazine-2-carboxylato-κ²N¹,O)tin(IV)

M. Vafaee, E. Najafi, M. M. Amini and S. W. Ng

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6-Benzyl-2-methyl-1,3-bis(pentafluorophenyl)-1,3,6,2-triazaalumocane

M. M. Kireenko, K. V. Zaitsev, A. V. Churakov, G. S. Zaitseva and S. S. Karlov

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Bis{2-[imino(phenyl)methyl]-5-methoxyphenolato-κ²N,O¹}nickel(II)

Y. Xiao, Z.-Q. Li and X. Y. Peng

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4-(Dimethylamino)pyridinium octaaquaerbium(III) tetrachloride monohydrate

M. Benslimane, H. Merazig, J.-C. Daran and O. Zeghouan

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cis-(2,2′-Bipyridine-κ²N,N′)bis(isonicotinamide-κN¹)palladium(II) bis(hexafluoridophosphate)

R. A. Adrian, B. Quintela, D. R. Powell, S. W. Ng and E. R. T. Tiekink

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(Acetylacetonato-κ²O,O′)dichloridobis(methanolato-κO)niobium(V)

L. Herbst, H. G. Visser, A. Roodt and C. Pretorius

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Tetraaquabis(6-chloropyridine-3-carboxylato-κO)nickel(II) tetrahydrate

Q.-H. Xia, Z.-F. Guo, L. Liu, J.-Q. Lv and B. Li

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Tetraaquabis(6-chloropyridine-3-carboxylato-κO)cobalt(II) tetrahydrate

Q.-H. Xia, Y. Zhang, L. Liu, L.-F. Shi and B. Li

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catena-Poly[[[diaquacopper(II)]-μ-quinoline-2,3-dicarboxylato-κ³N,O²:O³] monohydrate]

Q.-H. Xia, Z.-F. Guo, L. Liu, Z. Wang and B. Li

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(Nitrato-κO)tris[tris(4-fluorophenyl)phosphane-κP]copper(I)

T. N. Hill and A. Roodt

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trans-Bis[4-amino-N-(pyrimidin-2-yl-κN)benzenesulfonamidato-κN]bis(N,N-dimethylformamide-κO)cobalt(II)

J. J. Guo, W. Wang, Y. D. Zhang, L. Yang and S. H. Zhang

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catena-Poly[[chlorido[1-(3-nitrophenyl)-2-(triphenylphosphoranylidene)ethanone-κC²]mercury(II)]-μ-chlorido]

A. Dadrass, J. Khalafy, H. Rahchamani, H. Nasri Koureh and H. Yaghoobnejad Asl

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Bis(diisopropylammonium) hexachloridostannate(IV)

G. J. Reiss and C. Helmbrecht

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A triclinic polymorph of catena-poly[[bis(N,N-dimethylformamide-κO)cobalt(II)]-di-μ-1,5-dicyanamido-κ⁴N¹:N⁵]

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Hexakis(μ₃-1-methylthiourea-κ³S:S:S)hexakis[iodidocopper(I)]

S. Ahmad, M. Mufakkar, I. U. Khan, H.-K. Fun and A. Waheed

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Dibromido(2,9-dimethyl-1,10-phenanthroline-κ²N,N′)cobalt(II) acetonitrile monosolvate

S. A. Shirvan, M. Aghajeri, S. Haydari Dezfuli, F. Khazali and A. Borsalani

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Di-μ-carbonyl-bis[bis(triphenylphosphane)rhodium(0)](Rh—Rh) acetone disolvate

P. G. Gueorguieva, S. A. Laneman, G. G. Stanley, F. R. Fronczek and S. F. Watkins

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catena-Poly[zinc-μ₃-{3,3′-[(1,7-dioxa-4,10-diazacyclododecane-4,10-diyl)bis(methylene)]dibenzoato}]

C. W. Ingram, L. Liao and J. Bacsa

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Bis(benzene-1,2-diamine-κ²N,N′)(sulfato-κO)copper(II) monohydrate

Y. Djebli, S. Boufas, L. Bencharif, T. Roisnel and M. Bencharif

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Poly[[diaquabis{μ-4-[6-(4-carboxyphenyl)-4,4′-bipyridin-2-yl]benzoato-κ²O:N^4′}zinc] dimethylformamide tetrasolvate]

X. Ge and S. Song

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Bis(2,2′:6′,2′′-terpyridine)ruthenium(II) bis(perchlorate) hemihydrate

M. Kozlowska, P. Rodziewicz, D. M. Brus, J. Breczko and K. Brzezinski

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catena-Poly[[[aqua(2,2′-bipyridine-κ²N,N′)copper(II)]-μ-furan-2,5-dicarboxylato-κ²O²:O⁵] dihydrate]

Y.-F. Li, Y. Xu, X.-L. Qin, Y.-P. Yuan and W.-Y. Gao

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Iodido[1-(propan-2-ylidene)thiosemicarbazide-κS]bis(triphenylphosphane-κP)copper(I)

Y. Wattanakanjana, C. Pakawatchai, S. Saithong, P. Piboonphon and R. Nimthong

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trans-Iodido(pyrazinyl-κC²)bis(triphenylphosphane-κP)palladium(II)

Y.-J. Tu, H.-F. Wang, G.-H. Lee, K.-H. Yih and X.-Y. Tang

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Poly[[hexaaqua(μ₃-2,2′-bipyridine-4,4′,6,6′-tetracarboxylato-κ⁶O⁴:N,O⁶,O^6′,N′:O^4′)dinickel(II)] dihydrate]

J. Li, K.-W. Lei and D.-G. Xia

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Poly[[aquabis[μ₂-6-(pyridine-3-carboxamido)naphthalene-2-carboxylato]copper(II)] dihydrate]

Y.-S. Song and S. W. Lee

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Bis{2,4-dibromo-6-[(E)-(4-fluorobenzyl)iminomethyl]phenolato-κ²N,O}cobalt(II)

H. Yu, Z.-J. Chen, Y.-B. Jin, Y.-K. Chang and K.-W. Lei

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Bis{2,4-dibromo-6-[(E)-(4-fluorobenzyl)iminomethyl]phenolato-κ²N,O}zinc

D. Zhang, H. Yu, Y.-B. Jin and K.-W. Lei

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Di-μ-sulfido-bis{[rac-1,2-bis(η⁵-4,5,6,7-tetrahydroinden-1-yl)ethane]zirconium(IV)} toluene monosolvate

M. Haehnel, K. Altenburger, A. Spannenberg, P. Arndt and U. Rosenthal

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Poly[(μ₃-hydrogenphosphato)(4H-1,2,4-triazole-κN¹)zinc]

H. Aitenneite, A. El Bouari, S. Sebti, M. Saadi, L. El Ammari and K. Adil

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Bis(2,2′-bipyridine-κ²N,N′)bis(dicyanamido-κN¹)cadmium

D. Mal, R. Sen, P. Brandao and Z. Lin

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Tetraaquabis[2-(pyridin-4-yl-κN)pyrimidine-5-carboxylato]zinc

R. Sen, D. Mal, P. Brandao and Z. Lin

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Di-μ₂-acetato-1:2κ²O:O′;2:3κ²O:O′-bis{μ₂-4,4′-dichloro-2,2′-[2,2-dimethylpropane-1,3-diylbis(nitrilomethanylylidene)]diphenolato}-1:2κ⁶O,N,N′,O′:O,O′;2:3κ⁶O,O′:O,N,N′,O′-tricopper(II)

K. Kubono, K. Tani and K. Yokoi

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(2-Aminoethanethiolato-κ²N,S)bis[1,2-bis(diphenylphosphanyl)ethane-κ²P,P′]ruthenium(II) hexafluoridophosphate

A. Igashira-Kamiyama, M. Tamura and T. Konno

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catena-Poly[[diaquabis[2-(3-oxo-1,3-dihydro-2-benzofuran-1-yl)acetato-κO]cobalt(II)]-μ-1,2-bis(pyridin-4-yl)ethane-κ²N:N′]

C. Sun, Y. Li, W. Li and B. Dong

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Pyridinium cis-diaquabis(oxalato-κ²O,O′)chromate(III)

J. Nenwa, O. Befolo, B. Gouet, M. Mbarki and B. P. T. Fokwa

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organic compounds

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Bioresmethrin: (5-benzylfuran-3-yl)methyl 2,2-dimethyl-3-(2-methylprop-1-en-1-yl)cyclopropane-1-carboxylate

T. H. Kim, K.-M. Park, Y. Jeon and J. Kim

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N-[2-(5-Bromo-2-morpholin-4-ylpyrimidin-4-ylsulfanyl)-4-methoxyphenyl]-2,4,6-trimethylbenzenesulfonamide

M. Kumar, L. Mallesha, M. A. Sridhar, K. Kapoor, V. K. Gupta and R. Kant

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3-(3,4-Dichlorobenzylidene)chroman-4-one

K. Gopaul, N. A. Koorbanally, M. M. Shaikh, H. Su and D. Ramjugernath

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7-Methoxyindan-1-one

Y. J. Chang and K.-Y. Chen

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2-(3,4-Dimethyl-5,5-dioxo-2H,4H-pyrazolo[4,3-c][1,2]benzothiazin-2-yl)-N-(3-methoxybenzyl)acetamide

M. Ahmad, H. L. Siddiqui, M. Zia-ur-Rehman, S. Aslam and M. Parvez

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3-(Ammoniomethyl)pyridinium dibromide

B. F. Ali, R. Al-Far and S. F. Haddad

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N-(4-chlorobenzoyl)-N-(2-chlorophenyl)-O-[2-(2-nitrophenyl)acetyl]hydroxylamine

J. Ma, Y. Ma and D. He

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A monoclinic polymorph of 5-[(1H-benzimidazol-1-yl)methyl]benzene-1,3-dicarboxylic acid

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1-Dodecyl-1H-benzo[d]imidazol-2(3H)-one

D. Belaziz, Y. Kandri Rodi, F. Ouazzani Chahdi, E. M. Essassi, M. Saadi and L. El Ammari

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(N→B)-4-Methyl-3-pyridyl[N-methyliminodiacetate-O,O′,N]borane

M. Dąbrowski, K. Durka and J. Serwatowski

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(3S,7R)-7,14,16-Trihydroxy-3-methyl-3,4,5,6,7,8,9,10,11,12-decahydro-1H-2-benzoxacyclotetradecin-1-one.

S. Drzymala, W. Kraus, F. Emmerling and M. Koch

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N-[4-(2-Propyn-1-yloxy)phenyl]acetamide

Y. H. Belay, H. H. Kinfe and A. Muller

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Diphenyl(pyridin-2-yl)phosphane selenide

W. L. Davis and A. Muller

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N,N-Dibenzyl-O,O′-dimethyl thiophosphate

A. Raissi Shabari, F. Sabbaghi, M. Pourayoubi, M. Nečas and M. Babiak

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3-Oxo-2,3-dihydro-1H-inden-4-yl acetate

H.-Y. Lin, C.-W. Chang, H.-Y. Tsai, M.-H. Luo and K.-Y. Chen

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N-(4-Chlorophenyl)-4-methoxybenzamide

R. Kant, S. Sahi, V. K. Gupta, K. Kapoor and S. Paul

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Diisopropylammonium hydrogen phenylphosphonate

M. Sarr, M. S. Boye, A. Diasse-Sarr, A. Grosjean and P. Guionneau

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2-Cyano-5-({4-[N-methyl-N-(2-hydroxyethyl)amino] phenyl}diazenyl)pyridine

R. Centore and V. Piccialli

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2-Carboxypyridinium maleate

P. Pandi, G. Peramaiyan, R. Akilan, G. Chakkaravarthi and R. Mohankumar

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7H-[1,2]Benzothiazolo[3,2-b]quinazoline 5,5-dioxide

P. Narayanan, S. Karthikeyan, P. C. Srinivasan and K. Sethusankar

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4-Methoxybenzamidinium chloride monohydrate

S. Irrera and G. Portalone

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2-Methyl-3-(4-methylphenyl)-5,6-diphenyl-2,3-dihydropyrazine

A. Thiruvalluvar, N. Anuradha, S. Chitra, D. Devanathan and R. J. Butcher

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3-[Bis(dimethylamino)methylene]-1,1-diphenylurea

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Bicyclo[2.2.1]hept-7-yl p-bromobenzoate

B. A. Lloyd and A. M. Arif

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2,5-Dimethyl-N-[1-(1H-pyrrol-2-yl)ethylidene]aniline

B.-Y. Su, W.-L. Qin and J.-X. Wang

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3-epi-Dammarenediol II 1.075 hydrate: a dammarane triterpene from the bark of Aglaia eximia

H.-K. Fun, S. Chantrapromma, A. Supriadin, D. Harneti and U. Supratman

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(Z)-4-Benzylidene-3-methylisoxazol-5(4H)-one

Chandra, N. Srikantamurthy, S. Jeyaseelan, K. B. Umesha, K. Palani and M. Mahendra

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rac-Ethyl 4-hydroxy-4-trifluoromethyl-6-(2,4,5-trimethoxyphenyl)-2-thio-1,3-diazinane-5-carboxylate

Y.-Q. Li and Z.-Y. Ju

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(2-{[2-(diphenylphosphino)phenyl]thio}phenyl)diphenylphosphine sulfide

A. Alvarez-Larena, F. J. Martinez-Cuevas, T. Flor and J. Real

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(±)-(4bS,8aR,10aS)-10a-Ethynyl-4b,8,8-trimethyl-3,7-dioxo-3,4b,7,8,8a,9,10,10a-octahydrophenanthrene-2,6-dicarbonitrile

S. Zheng, D. Resch, T. Honda and J. P. Jasinski

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4-Hydroxyindan-1-one

C.-W. Chang, S.-K. Fang, M.-H. Luo, H.-Y. Tsai and K.-Y. Chen

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Methyl 2-(3,5-dinitrobenzamido)-3-methylbutanoate

X. Li and Y. Zhao

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Ethyl 7-methyl-2-((1-methyl-1H-pyrrol-2-yl)methylene)-3-oxo-5-phenyl-3,5-dihydro-2H-thiazolo[3,2-a]pyrimidine-6-carboxylate

J. Hu, X.-X. Wu, X.-Q. Shen, L.-G. Tang and X.-K. Li

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3,6-Dibromophenanthrene

R. Yokota, C. Kitamura and T. Kawase

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4-(2-Chlorophenylamino)-pent-3-en-2-one

G. J. S. Venter, A. Brink, G. Steyl and A. Roodt

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(3aS,4S,6S,7aR)-Hexahydro-3a,5,5-trimethyl-2-phenyl-4,6-methano-1,3,2-benzodioxaborole

T. Lejon, O. V. Gozhina and V. N. Khrustalev

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2-Cyclohexylidene-N-methylhydrazinecarbothioamide

S. Tayamon, N. A. Mazlan, T. B. S. A. Ravoof, M. I. Mohamed Tahir and K. A. Crouse

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3-Methyl-4-nitrophenol–4-dimethylaminopyridine (1/1)

S. Muralidharan, P. Nagapandiselvi, T. Srinivasan, R. Gopalakrishnan and D. Velmurugan

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2,4,6-Trinitrophenyl 4-methylbenzoate

R. Moreno-Fuquen, F. Mosquera, J. Ellena, J. C. Tenorio and R. S. Corrêa

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A co-crystal of 3-(3,5-dinitrobenzoyl)-1,1-dimethylthiourea and N,N-dimethyl-3,5-dinitrobenzamide

S. Saeed, N. Rashid, R. J. Butcher, S. Öztürk Yildirim and R. Hussain

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3-[(2-Chloro-1,3-thiazol-5-yl)methyl]-5-methyl-1,3,5-oxadiazinan-4-one

R. Kant, V. K. Gupta, K. Kapoor, C. S. Shripanavar and K. Banerjee

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(2E)-3-(Dimethylamino)-1-(4-fluorophenyl)prop-2-en-1-one

R. Kant, V. K. Gupta, K. Kapoor, M. B. Deshmukh, D. R. Patil and P. V. Anbhule

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rac-(Z)-Methyl 1-benzyl-3-[(3-hydroxyquinuclidin-2-ylidene)methyl]-1H-indole-6-carboxylate

N. R. Penthala, P. R. Ponugoti, S. Parkin and P. A. Crooks

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2′-Acetonaphthone

I. O. Shotonwa and R. T. Boeré

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2-(4-Methoxyphenyl)-4,5-diphenyl-1-(prop-2-en-1-yl)-1H-imidazole

M. Akkurt, A. A. Marzouk, V. M. Abbasov, A. A. Abdelhamid and A. V. Gurbanov

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(3-Chloropropyl)triphenylphosphonium bromide

C. N. Kavitha, H. S. Yathirajan, A. S. Dayananda, T. Gerber, E. Hosten and R. Betz

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Bis(2,4-dinitrophenyl)sulfane

M. Buvaneswari, D. Kalaivani and M. Nethaji

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3,5-Dimethylpyrazolium 3,5-dinitrosalicylate

S. Wei, S. Jin, Z. Hu, Y. Zhou and Y. Zhou

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4-Morpholinecarboxamidine

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3-(6-Aminopyridinium-3-yl)benzoate monohydrate

Z.-Y. Yuan, J. Zhao and Z. Peng

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1-(2-Ammonioethyl)piperazin-1,4-diium dihydrogenophosphate monohydrogenophosphate

M. L. Mrad, V. Ferretti, M. Rzaigui and C. Ben Nasr

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Methyl (2E)-2-cyano-3-(dimethylamino)prop-2-enoate

R. Kant, V. K. Gupta, K. Kapoor, D. R. Patil, D. K. Salunkhe and M. B. Deshmukh

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5-(4-Bromophenoxy)-1-methyl-3-methyl-1H-pyrazole-4-carbaldehyde-O-[(5-methoxy-1,3,4-thiadiazol-2-yl)-methyl]oxime

C.-G. Fan, J.-C. Chen, H. Dai, Y.-H. Wei and Y.-J. Shi

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5-Bromo-2-(thiophen-2-yl)-1-(thiophen-2-ylmethyl)-1H-benzimidazole

D. K. Geiger and M. R. Destefano

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5-Cyclopentyl-2-(4-methylphenyl)-3-methylsulfinyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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(2-(Benzo[d]thiazol-2yl-methoxy)-5-chlorophenyl)(phenyl)methanone

K. N. Venugopala, S. K. Nayak, T. Govender, H. G. Kruger and G. E. M. Maguire

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1-(2-Hydroxy-5-methoxyphenyl)-3-methylbut-2-en-1-one

C. T. Alexander, D. Vargas, F. R. Fronczek and S. F. Watkins

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2,2′-Diiodoazobenzene

P. J. W. Elder and I. Vargas-Baca

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5-(4-Hexyl-1H-1,2,3-triazol-1-yl)-2,1,3-benzoxadiazole

J. A. Key, C. W. Cairo and M. J. Ferguson

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5-(1-Benzyl-1H-1,2,3-triazol-4-yl)-2,1,3-benzoxadiazole

J. A. Key, C. W. Cairo and R. McDonald

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1-[1-(2,1,3-Benzoxadiazol-5-ylmethyl)-1H-1,2,3-triazol-4-yl]hexan-1-one

J. A. Key, C. W. Cairo and R. McDonald

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Dibenzo[b,f][1,4]thiazepin-11-yl-diethyl-amine

M. Altamura, A. Guidi, L. Jierry, P. Paoli and P. Rossi

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1H-Indole-3-carbaldehyde

C. S. Dileep, M. M. M. Abdoh, M. P. Chakravarthy, K. N. Mohana and M. A. Sridhar

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7-[(3-Chloro-6-methyl-6,11-dihydrodibenzo[c,f][1,2]thiazepin-11-yl)amino]heptanoic acid S,S-dioxide hydrochloride

A. Mishnev, A. Zvirgzdins, A. Actins and M. Delina

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1-(Thiophen-2-yl)-N-(4-{(E)-[(thiophen-2-yl)methyl]iminomethyl}benzylidene)methanamine

H. Chiririwa, J. R. Moss, D. Hendricks and R. Meijboom

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2-(1,3-Benzothiazol-2-ylsulfanyl)-N-(2-methylphenyl)acetamide

Y. Sun, X.-J. Wang and P.-W. Zheng

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5-[(Z)-2,3-Dimethoxybenzylidene]-1,2,4-triazolo[3,2-b][1,3]thiazol-6(5H)-one

L. Guo, G.-T. Lin, J. Wang, L. Ni and R.-S. Ge

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2-(1H-Indol-3-yl)acetohydrazide

L. R. Sidra, I. U. Khan, M. Yar and J. Simpson

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N,N-Bis(2-hydroxyethyl)-4-methylbenzenesulfonamide

N. Mushtaq, I. U. Khan, M. Yar, S. Afzal and J. Simpson

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[(E)-1-(Naphthalen-2-yl)ethylidene](naphthalen-1-ylmethyl)amine

S. M. Bruno, J. A. Fernandes, I. S. Gonçalves and F. A. Almeida Paz

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N,N-Diethyl-2-(4-methylbenzenesulfonamido)benzamide

M. Altamura, V. Fedi, R. Nannicini, P. Paoli and P. Rossi

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3-tert-Butyl 5-methyl (2R,4S,5R)-2-(4-methoxyphenyl)-4-(3-nitrophenyl)-1,3-oxazolidine-3,5-dicarboxylate

S. Montiel-Smith, S. Bernès, J. Sandoval-Ramírez, S. Meza-Reyes and J. Dubois

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(Z)-4-[(2-Amino-4,5-dichloroanilino)(phenyl)methylidene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-one

D. Zou, X. Lü, S. Zhao and X. Liu

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Tris[(6S)-6-hydroxy-4-epi-shikimic acid] monohydrate: an enantiomerically pure hydroxylated shikimic acid derived from methyl shikimate

A. G. Griesbeck, C. Miara and J.-M. Neudörfl

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2-Amino-5-methylpyridinium 6-oxo-1,6-dihydropyridine-2-carboxylate

K. Thanigaimani, A. Farhadikoutenaei, N. C. Khalib, S. Arshad and I. A. Razak

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[4-(Dimethylamino)phenyl]diphenylphosphine selenide

W. L. Davis and A. Muller

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Quinolin-3-amine

A. M. Islor, B. Chandrakantha, P. Shetty, T. Gerber, E. Hosten and R. Betz

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1-[5-Acetyl-2,6-dimethyl-4-(5-phenyl-1H-pyrazol-3-yl)-1,4-dihydropyridin-3-yl]ethanone monohydrate

A. M. Islor, S. Malladi, S. Sundershan, T. Gerber, E. Hosten and R. Betz

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(1E,2E)-1,2-Bis[(1-benzyloxymethyl-1H-indol-3-yl)methylidene]hydrazine

J. A. Myers, F. R. Fronczek and S. F. Watkins

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1-[4-Chloro-3-(trifluoromethyl)phenyl]-4-phenyl-1H-1,2,3-triazole

J. M. Altimari, P. C. Healy and L. C. Henderson

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3,4,5-Trimethoxyphenol

X.-C. Jia, J. Li, Z.-R. Yu, H. Zhang and L. Zhou

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N-(2-Phenoxyphenyl)pyrazine-2-carboxamide

M. Noroozi Tisseh, M. Kargar Razi and H. R. Khavasi

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Di-tert-butyl N-{[1-(pyridin-4-yl)-1H-1,2,3-triazol-4-yl]methyl}iminodiacetate

A. François, L. Marty, C. Picard, S. Mallet-Ladeira and E. Benoist

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3-Methoxy-2-[2-({[6-(trifluoromethyl)pyridin-2-yl]oxy}methyl)phenyl]prop-2-enoic acid

R. Kant, V. K. Gupta, K. Kapoor, C. S. Shripanavar, M. B. Deshmukh and K. Banerjee

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(E)-3-(1,3-Benzodioxol-5-yl)-2-{[N-(2-formylphenyl)-4-methylbenzenesulfonamido]methyl}prop-2-enenitrile

M. Bakthadoss, A. Devaraj, R. Madhanraj and S. Murugavel

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3-{[1-(2,3,5-Tri-O-benzoyl-β-D-ribofuranos-1-yl)-1H-1,2,3-triazol-4-yl]methyl}quinazolin-4(3H)-one

A. Ouahrouch, M. Taourirte, M. El Azhari, M. Saadi and L. El Ammari

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(3-Oxo-3H-benzo[f]chromen-1-yl)methyl piperidine-1-carbodithioate

O. Kotresh, K. M. Kumar, N. M. Mahabaleshwaraiah, H. K. Arunkashi and H. C. Devarajegowda

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4-Bromo-2-[(E)-{[4-nitro-2-(trifluoromethyl)phenyl]imino}methyl]phenol

M. Akkurt, A. R. Kennedy, S. K. Mohamed, A. A. Abdelhamid and G. J. Miller

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2-(Prop-2-enyloxy)benzamide

B. Bugenhagen, Y. Al Jasem, F. Barkhad, B. al Hindawi and T. Thiemann

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3-tert-Butyl-1-(3-nitrophenyl)-1H-pyrazol-5-amine

S. Hernández-Ortega, F. Cuenú-Cabezas, R. Abonia-González and A. Cabrera-Ortiz

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4,4′-Dimethyl-2,2′-[imidazolidine-1,3-diylbis(methylene)]diphenol

A. Rivera, L. S. Nerio, J. Ríos-Motta, M. Kučeraková and M. Dušek

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L-Tyrosine isopropyl ester

N. Nuñez-Dallos, K. Wurst and R. Quevedo

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9,10-Dibromophenanthrene

R. Yokota, C. Kitamura and T. Kawase

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Methyl 2-[2-(benzyloxycarbonylamino)propan-2-yl]-5-hydroxy-1-methyl-6-oxo-1,6-dihydropyrimidine-4-carboxylate

Z. Shang, X. Tao, J. Ha and F. Yu

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(E)-N-[(2-Ethoxynaphthalen-1-yl)methylidene]-2-ethylaniline

H. Kargılı, M. Macit, G. Alpaslan, C. Kazak and A. Erdönmez

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4′-(4-Chlorophenyl)-3′-(4-methoxyphenyl)-3,4-dihydro-1H,4′H-spiro[acridine-2,5′-isoxazol]-1-one

P. Narayanan, S. U. Maheswari and K. Sethusankar

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1-(1-Benzofuran-2-yl)ethanone O-(4-chlorobenzyl)oxime

T. Kosmalski and A. K. Gzella

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1-(Benzotriazol-1-yl)-2-bromoethanone

A. M. Asiri, N. E. Abo-Dya, M. N. Arshad and M. Shafiq

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Methyl 3-O-α-L-fucopyranosyl β-D-glucopyranoside tetrahydrate

L. Eriksson and G. Widmalm

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Cyclo(-L-prolyl-L-valinyl-) from Burkholderia thailandensis MSMB43

X.-Y. Liu, C. Wang and Y.-Q. Cheng

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Methyl (E)-2-cyano-3-(6-nitro-1,3-benzodioxol-5-yl)acrylate

M. Bakthadoss, A. Devaraj, D. Lakshmanan and S. Murugavel

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(+)-(1S,5R,6R)-6-[(S)-1-Hydroxy-2-(methoxymethyloxy)ethyl]-1-methyl-3-trichloromethyl-2-aza-4,7-dioxabicyclo[3.3.0]oct-2-en-8-one

T. Oishi, H. Oishi, S. Tsuzaki, T. Sato and N. Chida

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N,N,N′,N′-Tetrabenzyl-N′′-(2,6-difluorobenzoyl)phosphoric triamide

A. Raissi Shabari, M. Pourayoubi, A. Tarahhomi, A. L. Rheingold and J. A. Golen

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2-Amino-5-chloropyridinium 4-aminobenzoate

V. Kannan, P. Sugumar, S. Brahadeeswaran and M. N. Ponnuswamy

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N-(2,3-Dimethylphenyl)-2-nitrobenzenesulfonamide

U. Chaithanya, S. Foro and B. T. Gowda

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(2E)-1-[2,3-Dichloro-6-methyl-5-(trifluoromethyl)phenyl]-2-(1-phenylethylidene)hydrazine

H.-K. Fun, W.-S. Loh, M. Bhat, T. Arulmoli and G. K. Nagaraja

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1-(2-Fluorophenyl)-3-(2,4,6-trimethoxyphenyl)prop-2-en-1-one

M. Prabuswamy, S. Madan Kumar, D. Bhuvaneshwar, C. S. S. S. Murthy and N. K. Lokanath

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4-[(3-Chloro-2-methylphenyl)iminomethyl]phenol

B. C. Manjunath, M. M. M. Abdoh, L. Mallesha, K. N. Mohana and N. K. Lokanath

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2-(4-Fluorophenyl)-5-iodo-3-isopropylsulfonyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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1,5-Dimethyl-2-phenyl-4-[phenyl(pyridin-2-ylamino)methyl]-1H-pyrazol-3(2H)-one

K. Krishnakumar, S. Franklin, G. V. Prabhu and T. Balasubramanian

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4,4′-Bipyridine–3,3′-disulfanediylbis(1H-1,2,4-triazole-5-amine) (1/1)

W. Yang, Q.-M. Qiu, Q.-H. Jin and C.-L. Zhang

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2-Amino-5-methylpyridinium 3-chlorobenzoate

K. Thanigaimani, A. Farhadikoutenaei, N. C. Khalib, S. Arshad and I. A. Razak

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2-Amino-5-methylpyridinium 2-aminobenzoate

K. Thanigaimani, A. Farhadikoutenaei, N. C. Khalib, S. Arshad and I. A. Razak

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3-Ethyl-4-hydroxy-8-methoxyquinolin-2(1H)-one

S. Kafka, A. Pevec, K. Proisl, R. Kimmel and J. Košmrlj

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3-Ethyl-3-hydroxy-8-methoxyquinoline-2,4(1H,3H)-dione monohydrate

S. Kafka, A. Pevec, K. Proisl, R. Kimmel and J. Košmrlj

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A second polymorph of 2,4,6-tris(3,5-dimethyl-1H-pyrazol-1-yl)-1,3,5-triazine

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[4-(Bromomethyl)benzyl]triphenylphosphonium bromide acetonitrile monosolvate

B. P. Burke, P. Greenman, A. M. Smith and S. J. Archibald

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2-Cyano-N′-[1-(pyridin-2-yl)ethylidene]acetohydrazide

X.-Y. Zhang, X.-L. Han and Z.-B. Qian

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2-Cyano-3-(2,3,6,7-tetrahydro-1H,5H-benzo[ij]quinolizin-9-yl)prop-2-enoic acid dimethyl sulfoxide monosolvate

H. Yennawar, G. He, C. Rumble and M. Maroncelli

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Methyl 2-[(tert-butoxycarbonyl)amino]-3-(3-methyl-2-sulfanylidene-2,3-dihydro-1H-imidazol-1-yl)propanoate

C.-F. Chan, Y.-C. Guo, B.-H. Huang and M.-J. Chen

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1-Chloromethylsulfinyl-2-nitrobenzene

S. Benmebarek, M. Boudraa, S. Bouacida and J.-C. Daran

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5-Bromo-3-(4-fluorophenylsulfonyl)-2,7-dimethyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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N-(2-{[5-Bromo-2-(piperidin-1-yl)pyrimidin-4-yl]sulfanyl}-4-methoxyphenyl)benzenesulfonamide

M. Kumar, L. Mallesha, M. A. Sridhar, K. Kapoor, V. K. Gupta and R. Kant

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(±)-(rel-3R,3′R)-1,1′-Dimethyl-3,3′-bipyrrolidine-2,2′-dithione

L. G. Madeley, A. Lemmerer and J. P. Michael

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1-Allyl-1H-1,3-benzimidazol-2(3H)-one

D. Belaziz, Y. Kandri Rodi, F. Ouazzani Chahdi, E. M. Essassi, M. Saadi and L. El Ammari

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Ethyl 2-[2-(4-hydroxy-3-methoxybenzylidene)hydrazin-1-ylidene]-3,4-dimethyl-2,3-dihydro-1,3-thiazole-5-carboxylate

S. Öztürk Yildirim, R. J. Butcher, Y. Köysal, E. N. Kantar and A. Belder

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3-(4-Chlorophenyl)-5-phenyl-4,5-dihydro-1,3-oxazole

A. M. Islor, R. Yaradoni, B. Garudachari, T. Gerber, E. Hosten and R. Betz

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3,5-Bis(4-fluorophenyl)-1-(4-nitrophenyl)-4,5-dihydro-1H-pyrazole

S. Samshuddin, B. Narayana, H. S. Yathirajan, T. Gerber, E. Hosten and R. Betz

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Ethyl (Z)-3-(4-methylanilino)-2-[(4-methylphenyl)carbamoyl]prop-2-enoate

A. M. Islor, B. Garudachari, T. Gerber, E. Hosten and R. Betz

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1,1,1-Trichloro-2,2-bis(4-ethoxyphenyl)ethane

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5,6-Dimethylpyrazine-2,3-dicarbonitrile

G. R. Bardajee, A. J. Lough and M. A. Winnik

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1-(1H-1,2,3-Benzotriazol-1-yl)-2-(4-methoxyphenyl)ethanone

A. M. Asiri, N. E. Abo-Dya, M. N. Arshad, K. A. Alamry and M. Shafiq

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Redetermination and absolute configuration of (+)-7-epiclusianone

O. E. Christian, F. R. Fronczek, K. Ky, S. Pradhan, A. Manandhar and C. Richmond

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5-(Diphenylmethylidene)pyrrolidin-2-one

T.-F. Hsu, Y.-R. Chen, B.-H. Huang and M.-J. Chen

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Salvinorin B methoxymethyl ether

T. A. Munro, D. M. Ho and B. M. Cohen

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DL-Tyrosinium chloride dihydrate

F. Guenifa, L. Bendjeddou, A. Cherouana, S. Dahaoui and C. Lecomte

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N-{(1Z)-1-[(6-Chloropyridin-3-ylmethyl)(ethyl)amino]-3-(3-chlorophenyl)-2-nitro-5-oxohex-1-enyl}-N-methylacetamide

C.-W. Sun, Y. Wu and J. Wang

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3-Methyl-1,2,3,4,5,6,1′,2′,3′,4′-decahydrospiro[benz[f]isoquinoline-1,2′-naphthalen]-1′-one

S. Siaka, A. T. Soldatenkov, A. V. Malkova, E. A. Sorokina and V. N. Khrustalev

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4-Methylphenyl quinoline-2-carboxylate

E. Fazal, J. P. Jasinski, S. T. Krauss, B. S. Sudha and H. S. Yathirajan

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1,3-Dicyclohexylimidazolidine-2,4,5-trione: a second polymorph

O. Talhi, J. A. Fernandes, D. C. G. A. Pinto, A. M. S. Silva and F. A. Almeida Paz

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2-Ethyl-3-hydroxy-1-isopropyl-4-pyridone

P. P. Molokoane, M. Schutte and G. Steyl

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Benzoximate

T. H. Kim, S.-H. Moon, J. Kim and K.-M. Park

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(E)-1-(4-Nitrobenzylidene)-2,2-diphenylhydrazine

A. Mendoza, R. Meléndrez-Luevano, B. M. Cabrera-Vivas, C. Acoltzi-X and M. Flores-Alamo

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5,7,8,10,11,13,14,16-Octahydro-6,15-(ethanoxyethanoxyethano)-1,4:17,20-dietheno[9,12,6,15]benzodioxadiazacyclodocosine

H. A. Barnett, F. R. Fronczek and S. F. Watkins

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3-[(R)-1-Hydroxybutan-2-yl]-1,2,3-benzotriazin-4(3H)-one

F. Rocha-Alonzo, D. Morales-Morales, S. Hernández-Ortega, R. Reyes-Martínez and M. Parra-Hake

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5-Bromo-3-(4-fluorophenylsulfinyl)-2-phenyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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4-(2-Fluorobenzoyl)-1-[2-(4-hydroxyphenyl)-2-oxoethyl]piperazin-1-ium trifluoroacetate

F. Bian, Y. Jin, S. Chi, G. Shi and S. Xu

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4-Methoxybenzamidinium hydrogen sulfate

S. Irrera and G. Portalone

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1,4-Dibromobutane-2,3-dione

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(4-Fluorophenyl)[8-(4-fluorobenzoyl)-2,7-diphenoxynaphthalen-1-yl]methanone

D. Hijikata, K. Sasagawa, S. Yoshiwaka, A. Okamoto and N. Yonezawa

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3,5-Bis(benzyloxy)benzoic acid

R. Moreno-Fuquen, C. Grande, R. C. Advincula, J. C. Tenorio and J. Ellena

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2-Chloro-N-[1-(4-chlorophenyl)-3-cyano-1H-pyrazol-5-yl]acetamide

H. Mu, Y. Yang, Q. Jiang, X. Fu and R. Wan

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2-(4-Chlorophenyl)-6-methyl-4-(3-methylphenyl)quinoline

M. Prabhuswamy, T. R. Swaroop, S. Madan Kumar, K. S. Rangappa and N. K. Lokanath

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6,8-Dihydroxy-8a-methyl-3,5-dimethylidenedecahydronaphtho[2,3-b]furan-2(3H)-one

T. Liu, H.-B. Wu and W.-S. Wang

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10′-Chloro-3′,4′-dihydro-2′H-spiro[cyclopropane-1,7′(6′H)-pyrimido[2,1-a]isoquinolin]-6′-one

K. Okuda, T. Hirota, Y. Nishina and H. Ishida

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Piperidine-1-carboximidamide

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Kudos

Research communications

The first papers in this new format were published in July 2014. Research communications are longer papers with new text sections designed to help authors bring out the science behind their structure determinations. Figures are included in the published paper and, for the first time in Acta E, individual reports are not limited to single structure determinations. The Research communications format will make Acta E the natural home for structure determinations with interesting science to report.

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Editorial Advisory Board

S. BattenX.-M. ChenG. R. DesirajuL. R. FalvelloS. García-GrandaJ. A. K. HowardS. ParsonsI. D. Williams

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