Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 68| Part 11

ISSN: 2056-9890

November 2012 issue

Highlighted illustration

Cover illustration: Having enhanced potency, selectivity, and duration of action, the title opioid salvinorin A derivative, C₂₃H₃₀O₈, also exhibits surprising structural mimicry with salvinorin A. This arises as the ether residue adopts a gauche-gauche conformation which traces a helix around the acetate group of salvinorin A. See: Munro, Ho & Cohen [Acta Cryst. (2012). E68, o3225-o3226].

inorganic compounds

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LiNa₅Mo₉O₃₀

H. Hamza, I. Ennajeh, M. F. Zid and A. Driss

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Redetermination of (NH₄)₂HAsO₄

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Redetermination of dysprosium trinickel from single-crystal X-ray data

V. Levytskyy, V. Babizhetskyy, B. Kotur and V. Smetana

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Tetraamminelithium triamminelithium trisulfide, [Li(NH₃)₄][Li(NH₃)₃S₃]

C. Guentner and N. Korber

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Redetermination of durangite, NaAl(AsO₄)F

G. W. Downs, B. N. Yang, R. M. Thompson, M. D. Wenz and M. B. Andrade

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metal-organic compounds

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Bis(chlorido)(dimethylsulfoxide-κO)barium(II)

F. Gschwind and M. Jansen

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Bis(2,4,6-trimethylpyridinium) tetrabromidozincate

B. F. Ali, S. F. Haddad and R. Al-Far

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Bis[4-(dimethylamino)pyridinium] octaaquachloridolanthanum(III) tetrachloride trihydrate

M. Benslimane, H. Merazig, J.-C. Daran and O. Zeghouan

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N,N′-bis[(3-hydroxy-4(4H)-oxypyran-2-yl)methyl]-N,N′-dimethylethylene-1,2-diammonium tetrachloridoplatinate(II) dihydrate

V. Fusi, L. Giorgi, E. Macedi, P. Paoli and P. Rossi

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2-Aminopyridinium trans-diaquabis(oxalato-κ²O,O)chromate(III)

J. Nenwa, G. Bebga, S. Martin, M. M. Bélombé, M. Mbarki and B. P. T. Fokwa

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Trichlorido(6-methyl-2,2′-bipyridine-κ²N,N′)(dimethylsulfoxide-κO)indium(III)

S. A. Shirvan, S. Haydari Dezfuli, E. Golabi and M. A. Gholamzadeh

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Bis[5-(pyridin-2-yl)pyrazine-2-carbonitrile-κ²N⁴,N⁵](trifluoroacetato-κO)silver(I)

J. Li, X. C. Jia, J. Qi, Y. Y. Liu and Y. Ding

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trans-Dichloridobis[dicyclohexyl(2,4,6-trimethylphenyl)phosphane-κP]palladium(II)

I. Buthelezi, H. Chiririwa, H. Ogutu and R. Meijboom

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Dichlorido(6-methyl-2,2′-bipyridine-κ²N,N′)cobalt(II)

N. Akbarzadeh Torbati, A. R. Rezvani and H. Saravani

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Trans-bis(3-tert-butylpyridine-κN)bis(4-tert-butylpyridine-κN)bis(thiocyanato-κN)manganese(II)

T. Reinert, I. Jess and C. Näther

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Poly[tetrabutyltetrakis(μ₂-hydrogen phenylphosphonato)ditin(IV)]

M. Sarr, A. Diasse-Sarr, L. Diop, K. C. Molloy and G. Kociok-Kohn

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Bis[2,3,4-trimethyl-5-[(3,4,5-trimethyl-2H-pyrrol-2-ylidene-κN)methyl]-1H-pyrrolato-κN]copper(II)

S. S. Erdem, F. R. Fronczek and S. F. Watkins

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μ₂-Oxalato-bis[triphenyl(thiourea-κS)tin(IV)]

Y. Sow, L. Diop, K. C. Molloy and G. Kociok-Kohn

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Poly[(μ-1,3-thiocyanato-κN,S)(isonicotinato-κN,O)(ethanol-κO)cadmium(II)]

T. Neumann, J. Werner, I. Jess and C. Näther

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Tetrakis(μ-acetato-κ²O:O′)-bis[(3-pyridinecarboxaldehyde-κN′)]dicopper(II)(Cu—Cu)

A. Cruz-Enriquez, A. Baez-Castro, H. Höpfl, M. Parra-Hake and J. J. Campos-Gaxiola

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Bis[4,4,5,5-tetramethyl-2-(pyridin-2-yl-κ²N)imidazoline-1-oxyl 3-oxide-κO]tris(nitrato-κ²O,O′)terbium(III)

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Tris[4-(dimethylamino)pyridinium][(bis-μ-dichlorido)-decaaquadichloridodineodymium(III)] pentachloride dihydrate

M. Benslimane, H. Merazig, J.-C. Daran and O. Zeghouan

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Tetrakis(5,7-dimethylquinolin-8-olato-κ²N,O)zirconium(IV) dimethylformamide disolvate

M. Steyn, H. G. Visser and A. Roodt

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[Hydridotris(pyrazol-1-yl-κN²)borato]bis(methylamino-κN)(triphenylphosphine-κP)ruthenium(II) chloride dichloromethane solvate monohydrate

Y.-D. Lin, C.-P. Chang, Q.-S. Huang and Y.-H. Lo

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Bis(2,2′-bipyrimidine-κ²N¹,N^1′)palladium(II) bis(tetrafluoroborate) acetonitrile monosolvate

A. Duong, J. D. Wuest and T. Maris

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Poly[aqua(μ₂-pyrimidine-2-carboxylato-κ⁴O,N:O′,N′)(nitrato-κO)cadmium]

O. In-noi, K. Chainok and D. J. Harding

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trans-Dichloridobis(4-nitroaniline-κN¹)palladium(II)

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(Acetato-κO)(acetato-κO,O′)bis(1,3-diazinane-2-thione-κS)cadmium(II)

R. Mahmood, S. Ghulam Hussain, M. Fettouhi, A. A. Isab and S. Ahmad

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Bis(diphenyl-p-tolylphosphane-κP)(2-hydroxy-3,5,7-bromocyclohepta-2,4,6-trienonato-κ²O,O′)copper(I)

N. I. Barnard and T. N. Hill

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Bis[μ-(3-acetyl-2-hydroxy-6-methyl-4H-pyran-4-one-κ³O:O′,O′′)]diaquatetrakis(pyridine-κN)dicopper(II) diperchlorate

A. Ourari, W. Derafa, S. Bouacida, D. Aggoun and J.-C. Daran

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Potassium N-bromo-2-nitrobenzenesulfonamidate monohydrate

B. T. Gowda, S. Foro and H. S. Spandana

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(μ₁-Methanolato-κ¹O)-μ₁-methoxo-κ¹O-(μ₂-2-amino-1-methyl-5H-imidazol-4-one-κ²N:N′)-hexacarbonyldirhenium(I)

M. Schutte, H. G. Visser and A. Roodt

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(Ammine)(carbonyl)[hydridotris(pyrazol-1-yl-κN²)borato](triphenylphosphine-κP)ruthenium(II) chloride dichloromethane disolvate

T.-C. Hu, J.-X. Ye, S.-T. He, G.-R. Chiang and Y.-H. Lo

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Dibromido(6,6′-dimethyl-2,2′-bipyridine-κ²N,N′)cobalt(II)

S. A. Shirvan, S. Haydari Dezfuli, F. Khazali, M. Aghajeri and A. Borsalani

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Poly[di-μ₃-hydroxy[μ₄-5-(4-carboxyphenyl)pyridine-2-carboxylato-κ⁵N,O²:O^2′:O⁴:O^4′]dicadmium]

F.-J. Meng, H.-Q. Jia, N.-H. Hu and H. Zhou

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(μ₂-Chlorido)-(μ₂-pyridine-2-carboxylato-1:2κN,O:O)-dichlorido(ethanol-κO)bis[N-hydroxy-1-(pyridin-2-yl)methanimine-κ²N,N′]dicobalt(II)

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[Bis[μ-bis(diphenylphosphino)methane-1:2κ²P:P′]-bis(nitrito-κ²O,O′)]disilver(I) acetonitrile disolvate

X. Yang, X. Huang, Q.-M. Qiu, Q.-H. Jin and C.-L. Zhang

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Potassium N-bromo-2,4-dichlorobenzenesulfonamidate sesquihydrate

B. T. Gowda, S. Foro and H. S. Spandana

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catena-Poly[[tetraaqua-μ-aqua-bis(μ₄-pyrimidine-2-carboxylato)tetralithium] dichloride]

W. Starosta and J. Leciejewicz

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Sodium pentafluorophenylborate

H. Vitze, H.-W. Lerner and M. Bolte

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Bis(3-tert-butylpyridine-κN)bis(4-tert-butylpyridine-κN)bis(thiocyanato-κN)cadmium

T. Reinert, I. Jess and C. Näther

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Bis[4-(4-bromophenylimino-κN)pent-2-en-2-olato-κO]copper(II)

P. S. E. Bungu, M. Schutte and G. Steyl

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μ-(2,2′-Bipyrimidine)-bis[dichloridopalladium(II)] dimethylformamide monosolvate

C. Young, A. Roodt and B. C. B. Bezuidenhoudt

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Triaqua(cyclohex-4-ene-1,2-dicarboxylato-κO¹)(1,10-phenanthroline-κ²N,N′)cobalt(II)

H.-Y. Li, C. Wang, F.-P. Huang and Y.-M. Jiang

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Bis(acetato-κ²O,O′)(4,4′-dimethyl-2,2′-bipyridine-κ²N,N′)zinc

M. A. Harvey, S. A. Suarez, A. Ibañez, F. Doctorovich and R. Baggio

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Bis(μ-3-nitrobenzene-1,2-dicarboxylato)-κ⁴O¹,O²:O¹,O^1′;κ⁴O¹,O^1′:O¹,O²-bis[triaqua(6-carboxy-2-nitrobenzoato-κ²O¹,O⁶)neodymium(III)] dihydrate

Y. Chang, Z. Pei and Q. Shuai

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Poly[dibutylammonium [nonamethylbis(μ₃-sulfato-κ³O:O′:O′′)tristannate(IV)]]

T. Diop, L. Diop and A. van der Lee

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3′-Ferrocenylcarbonyl-1′-methyl-4′-phenylspiro[indeno[2,3-b]quinoxaline-11,2′-pyrrolidine]

B. Vijayakumar, D. Gavaskar, T. Srinivasan, R. Raghunathan and D. Velmurugan

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Dimethylbis(pyrazine-2-carboxylato-κ²N¹,O)tin(IV)

M. Vafaee, E. Najafi, M. M. Amini and S. W. Ng

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6-Benzyl-2-methyl-1,3-bis(pentafluorophenyl)-1,3,6,2-triazaalumocane

M. M. Kireenko, K. V. Zaitsev, A. V. Churakov, G. S. Zaitseva and S. S. Karlov

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Bis{2-[imino(phenyl)methyl]-5-methoxyphenolato-κ²N,O¹}nickel(II)

Y. Xiao, Z.-Q. Li and X. Y. Peng

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4-(Dimethylamino)pyridinium octaaquaerbium(III) tetrachloride monohydrate

M. Benslimane, H. Merazig, J.-C. Daran and O. Zeghouan

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cis-(2,2′-Bipyridine-κ²N,N′)bis(isonicotinamide-κN¹)palladium(II) bis(hexafluoridophosphate)

R. A. Adrian, B. Quintela, D. R. Powell, S. W. Ng and E. R. T. Tiekink

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(Acetylacetonato-κ²O,O′)dichloridobis(methanolato-κO)niobium(V)

L. Herbst, H. G. Visser, A. Roodt and C. Pretorius

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Tetraaquabis(6-chloropyridine-3-carboxylato-κO)nickel(II) tetrahydrate

Q.-H. Xia, Z.-F. Guo, L. Liu, J.-Q. Lv and B. Li

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Tetraaquabis(6-chloropyridine-3-carboxylato-κO)cobalt(II) tetrahydrate

Q.-H. Xia, Y. Zhang, L. Liu, L.-F. Shi and B. Li

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catena-Poly[[[diaquacopper(II)]-μ-quinoline-2,3-dicarboxylato-κ³N,O²:O³] monohydrate]

Q.-H. Xia, Z.-F. Guo, L. Liu, Z. Wang and B. Li

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(Nitrato-κO)tris[tris(4-fluorophenyl)phosphane-κP]copper(I)

T. N. Hill and A. Roodt

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trans-Bis[4-amino-N-(pyrimidin-2-yl-κN)benzenesulfonamidato-κN]bis(N,N-dimethylformamide-κO)cobalt(II)

J. J. Guo, W. Wang, Y. D. Zhang, L. Yang and S. H. Zhang

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catena-Poly[[chlorido[1-(3-nitrophenyl)-2-(triphenylphosphoranylidene)ethanone-κC²]mercury(II)]-μ-chlorido]

A. Dadrass, J. Khalafy, H. Rahchamani, H. Nasri Koureh and H. Yaghoobnejad Asl

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Bis(diisopropylammonium) hexachloridostannate(IV)

G. J. Reiss and C. Helmbrecht

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A triclinic polymorph of catena-poly[[bis(N,N-dimethylformamide-κO)cobalt(II)]-di-μ-1,5-dicyanamido-κ⁴N¹:N⁵]

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Hexakis(μ₃-1-methylthiourea-κ³S:S:S)hexakis[iodidocopper(I)]

S. Ahmad, M. Mufakkar, I. U. Khan, H.-K. Fun and A. Waheed

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Acta Cryst. (2012). E68, m1407
doi: 10.1107/S160053681204367X