Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 65| Part 5

ISSN: 2056-9890

May 2009 issue

Highlighted illustration

Cover illustration: The asymmetric unit of C₂₇H₃₆O₃, a chalcone derivative with antimicrobial activity, consists of two bow-shaped molecules, with the long alkoxyl chains adopting all-trans conformations. Intramolecular O-HO hydrogen bonds and weak intermolecular C-H [pi] interactions are seen in the crystal structure. See Razak et al. [Acta Cryst. (2009). E65, o1133-o1134].

inorganic compounds

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K₃VO₂(V₂As₂O₁₂)

S. Ezzine, M. F. Zid and A. Driss

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A new aquamanganese(II) oxalate phosphate, Mn(C₂O₄)Mn₃(PO₄)₂(H₂O)₂

J. Zheng, Y. Shen, T. Song and A. Zhang

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A synchrotron study of Na_2.27Ho_7.73(SiO₄)₆O_0.72

I. Rosales, E. Orozco, L. Bucio, M. E. Fuentes and L. Fuentes

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The Chevrel phase HgMo₆S₈

D. Salloum, P. Gougeon and M. Potel

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Dilead(II) hydrogenphosphite dinitrate

R. Ouarsal, M. Lachkar, M. Dušek, K. Fejfarová and B. El Bali

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Cubic ZrW_1.75Mo_0.25O₈ from a Rietveld refinement based on neutron powder diffraction data

X. Deng, Y. Cao, J. Tao and X. Zhao

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Potassium nickel(II) gallium phosphate hydrate, K[NiGa₂(PO₄)₃(H₂O)₂]

A. M. Chippindale, A. V. Sharma and S. J. Hibble

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An open-framework borophosphate, LiCu₂BP₂O₈(OH)₂

J. Zheng and A. Zhang

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metal-organic compounds

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Tetraaquabis[4-(4-pyridyl)pyrimidine-2-sulfonato]copper(II) dihydrate

L. Li, G. Xu and H.-B. Zhu

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Bis(2,3-dimethylbutane-2,3-diamine)nickel(II) dinitrate monohydrate

S.-X. Li, L.-K. Zou, B. Xie, J. Wang and J.-Z. Li

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(Diethyl ether){1-[2-(1-methyl-1H-imidazol-2-yl-κN³)-1,1-diphenylethyl]-(1,2,3,3a,7a-η)-indenyl}lithium(I)

G. Sun, C. Tian, W. Nie and M. V. Borzov

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2,9-Dimethyl-4,7-diphenyl-1,10-phenanthrolin-1-ium tetrachloridoaurate(III)

S. Ö. Yıldırım, M. Akkurt, N. Safari, A. Abedi, V. Amani and V. McKee

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Diaquabis(2-bromobenzoato-κO)bis(N,N-diethylnicotinamide-κN¹)zinc(II)

T. Hökelek, H. Dal, B. Tercan, F. E. Özbek and H. Necefoğlu

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Dibromido(2,9-dimethyl-1,10-phenanthroline-κ²N,N′)mercury(II)

R. Alizadeh, A. Heidari, R. Ahmadi and V. Amani

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Aqua(3-formyl-2-oxidobenzoato-κ²O¹,O²)(1,10-phenanthroline-κ²N,N′)copper(II) dimethylformamide solvate

Z.-W. Yu, L. Chang, P. Song and M.-H. He

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Bis(μ-dithieno[3,2-b:2′,3′-d]thiophene-2,6-dicarboxylato-κ²O²:O⁶)bis[bis(1,10-phenanthroline-κ²N,N′)cobalt(II)] dimethylformamide disolvate

C. M. MacNeill, C. S. Day and R. E. Noftle

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Tetraaquabis(3,5-di-4-pyridyl-1,2,4-triazolato-κN)cobalt(II) dihydrate

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(Ethanol-κO)[2-(4-hydroxyphenyl)quinoline-4-carboxylato-κO]triphenyltin(IV)

K. M. Lo and S. W. Ng

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Tricyclohexyl(2,3-dibromo-3-phenylpropionato-κO)tin(IV)

P. Y. Thong, K. M. Lo and S. W. Ng

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2-[3-(2-Pyridyl)pyrazin-2-yl]pyridinium tetrachloridoaurate(III)

S. Ö. Yıldırım, M. Akkurt, N. Safari, V. Amani and V. McKee

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(Biphenyl-2-yl)bromidobis(2-methyltetrahydrofuran-κO)magnesium(II)

S. Nordschild, D. Wohlgemuth and M. Bolte

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Aquabis(methacrylato-κO)bis(pyridine-κN)copper(II)

B. Wu and H. Yao

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(2,6-Difluorobenzophenone)tris(trimethylphosphine)cobalt(0)

J. Ding and X.-Y. Li

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catena-Poly[sodium(I)-μ-tetrabutoxyborato]

G. J. Gainsford and T. Kemmitt

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catena-Poly[[aquanickel(II)]-μ-pyridine-2,6-dicarboxylato-[aquanickel(II)]-μ-2,5-di-4-pyridyl-1,3,4-thiadiazole]

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{6,6′-Diethoxy-2,2′-[4,5-dimethyl-o-phenylenebis(nitrilomethylidyne)]diphenolato}nickel(II) dihydrate

H. Kargar, R. Kia, A. Jamshidvand and H.-K. Fun

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Bis[cis-bis(diphenylphosphino)ethene-κ²P,P′]copper(I) tetrafluoridoborate ethanol solvate

P. C. Healy, B. T. Loughrey and M. L. Williams

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Poly[di-μ₂-azido-μ₃-pyrazine-2-carboxylato-cadmium(II)]

C.-Y. Li, P.-F. Li and H.-M. Jin

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Bis(guanidinium) tetraiodidomercurate(II)

H. Terao, T. M. Gesing, H. Ishihara, Y. Furukawa and B. T. Gowda

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Diaquabis(5-carboxy-2-methyl-1H-imidazole-4-carboxylato-κ²N³,O⁴)cobalt(II) dimethylformamide disolvate

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Poly[[2-(3-pyridinio)-1H,3H⁺-benzimidazolium] [μ₄-oxido-di-μ₃-oxido-tetra-μ₂-oxido-hexaoxidotetramolybdenum(VI)]]

L.-J. Chen, S. Lin, X.-Y. Wu and X.-H. Chen

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Poly[μ₂-chlorido-(μ₂-3H⁺-1,3,4-thiadiazolium-2-thiolato-κ²S:S)silver(I)]

J.-G. Wang, J.-H. Qin and P.-Z. Hu

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catena-Poly[[(2,2′-bipyridine-κ²N,N′)cobalt(II)]-μ-oxalato-κ⁴O¹,O²:O^1′,O^2′]

P.-Z. Li and Q. Xu

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catena-Poly[[diaquazinc(II)]-μ-trans-4,4′-diazenediyldibenzoato-κ⁴O,O′:O′′,O′′′]

B. Liu and Q. Xu

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Poly[di-μ₂-acetato-diaquabis(2,2′-bipyridine)bis(μ₃-5-nitroisophthalato)tricobalt(II)]

H.-D. Wang, M.-M. Li and H.-Y. He

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Bis(4-amino-3,5-di-2-pyridyl-4H-1,2,4-triazole)diaquanickel(II) bis(perchlorate)

C.-F. Shao and L.-C. Geng

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Diaquabis(2-chlorobenzoato-κO)bis(N,N-diethylnicotinamide-κN¹)manganese(II)

T. Hökelek, H. Dal, B. Tercan, F. E. Özbek and H. Necefoğlu

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{6,6′-Diethoxy-2,2′-[2,2-dimethylpropane-1,3-diylbis(nitrilomethylidyne)]diphenolato}copper(II) monohydrate

H. Kargar, R. Kia, H.-K. Fun and A. Jamshidvand

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2-Ferrocenyl-3-methoxy-6-methylpyridine

C. Xu, X.-Q. Hao, F. Liu, X.-J. Wu and M.-P. Song

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Poly[[diaqua{N-[1-(3-pyridyl)ethylidene]-4H-1,2,4-triazol-4-amine}zinc(II)] bis(perchlorate)]

X. Sun, X. He, W. Wang, D. Miao and Q. Sun

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catena-Poly[[[pyridinecopper(II)]-(μ-2-oxidonaphthalene-1-carbaldehyde picolinoylhydrazonato)-[pyridinecopper(II)]-μ-sulfato] diethyl ether hemisolvate]

Q. Wang, D. Li and D. Wang

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Bis(4-aminopyridinium) tetrachloridocobaltate(II)

S. R. Jebas, A. Sinthiya, B. Ravindran Durai Nayagam, D. Schollmeyer and S. A. C. Raj

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[μ-10,21-Dimethyl-3,6,14,17-tetraazatricyclo[17.3.1.1^8,12]tetracosa-1(23),8(24),9,11,19,21-hexaene-23,24-diolato-κ⁸N³,N⁶,O²³,O²⁴:N¹⁴,N¹⁷,O²³,O²⁴]bis[(nitrato-κ²O,O′)nickel(II)]

Q.-J. Li, J.-F. Ma, J. Liu and T.-T. Han

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mer-(3,5-Dichloro-2-oxidobenzaldehyde thiosemicarbazonato-κ³S,N¹,O)(methanol-κO)(1,10-phenanthroline-κ²N,N′)nickel(II)

J. Y. Gao, Z. Liu and Y. Wang

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Bis[2-(aminomethyl)pyridine-κ²N,N′]bis(thiocyanato-κN)copper(II)

N. K. Karan, K.-T. Chan and H. M. Lee

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Tetra-μ-methacrylato-κ⁸O:O′-bis[(pyridin-2-amine-κN¹)copper(II)]

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Aqua(2,2′-bipyrimidine-κ²N,N′)(succinato-κ²O¹,O⁴)copper(II) dihydrate

X.-J. Ke, D.-S. Li, J. Zhao, Q.-F. He and C. Li

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[5-(4-Bromophenoxymethyl)-1,3,4-thiadiazole-2-thiolato]triphenyltin(IV)

Z. Wang, G. Zhao and L. Tian

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Bromido{dicyclohexyl[2′-(dimethylamino)biphenyl-2-yl]phosphine-κP}[2-(4,6-dimethylpyrimidin-2-yl)ferrocenyl-κ²C¹,N]palladium(II) dichloromethane solvate

X.-Q. Hao, H.-M. Li, H. Jiang, Y.-T. Ma and M.-P. Song

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Methyl 3-[ferrocenyl(hydroxy)methyl]-1-methyl-2′-oxospiro[pyrrolidine-2,3′-indoline]-3-carboxylate

E. T. S. Kamala, S. Nirmala, L. Sudha, S. Kathiravan and R. Raghunathan

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Diaquabis(2-bromobenzoato-κO)bis(N,N-diethylnicotinamide-κN¹)manganese(II)

T. Hökelek, H. Dal, B. Tercan, F. E. Özbek and H. Necefoğlu

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catena-Poly[[[di-μ₂-hydroxido-bis[(di-2-pyridylamine)nickel(II)]]-μ-fumarato] dihydrate]

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catena-Poly[[dichloridozinc(II)]-μ-1,4-bis(3-pyridylmethyl)piperazine]

A. M. Hardy and R. L. LaDuca

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Poly[[diaquabis(μ₂-4,4′-bipyridine)manganese(II)] bis[2-(2-carboxyphenyldisulfanyl)benzoate]]

M. Hu, S.-T. Ma, L.-Q. Guo and S.-M. Fang

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Bis[μ-2-(2-naphthoxy)acetato]bis{aqua[2-(2-naphthoxy)acetato]zinc(II)}

F.-J. Chen, H. Xu, H. Xu and K.-L. Huang

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Bis[4-hydroxy-N′-(4-methoxy-2-oxidobenzylidene-κO²)benzohydrazidato-κ²O,N′]cadmium(II) dimethyl sulfoxide disolvate

N. Mohd Lair, H. Mohd Ali and S. W. Ng

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trans-Diaquabis[5-(1H-imidazol-4-yl-κN³)-1H-tetrazolato-κN¹]zinc(II)

H. Zhao and J. Xiao

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Bis(μ-2,2′-bi-1H-imidazole-1,1′-diacetato)bis[diaquacobalt(II)] hexahydrate

T. Zhang, T. Zhang, F. Xu and H. Liang

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Diaquabis(2-chlorobenzoato-κO)bis(N,N-diethylnicotinamide-κN¹)nickel(II)

T. Hökelek, H. Dal, B. Tercan, F. E. Özbek and H. Necefoğlu

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Bis(2,2′-bipyridine N,N′-dioxide)bis(tricyanomethanido)manganese(II)

J. Luo, F. Yang, L.-J. Qiu, X.-X. Wang and B.-S. Liu

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Bis(μ-4-hydroxy-2-oxidobenzaldehyde 4-ethylthiosemicarbazone)-κ⁴O²,N¹,S:O²;κ⁴O²:O²,N¹,S-bis[chloridozinc(II)] dimethyl sulfoxide trisolvate

K. W. Tan, C. H. Ng, M. J. Maah and S. W. Ng

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Poly[tetraaqua-μ₃-benzene-1,2-dicarboxylato-μ₃-bromido-penta-μ₂-bromido-octa-μ₃-isonicotinato-heptacopper(I)trilanthanum(III)]

G.-M. Wang, Z.-X. Li, S.-Y. Xue and H.-L. Liu

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Bis(2,2′-bipyridyl)-1κ²N,N′;3κ²N,N′-bis(4-bromo-2-formylphenolato)-1κ²O,O′;3κ²O,O′-bis[μ-2-(5-bromo-2-oxidobenzylideneamino)ethanesulfonato]-1:2κ³O:N,O²;2:3κ³N,O²:O-tricopper(II) monohydrate

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Acta Cryst. (2009). E65, m553
doi: 10.1107/S1600536809014202