Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 64| Part 5

ISSN: 2056-9890

May 2008 issue

Highlighted illustration

Cover illustration: This tricyclododecanol crystallizes in space group P2₁/c with homochiral chains of molecules along b, held together by O-HO hydrogen bonds. Adjacent chains along a are of the same chirality, leading to chirally pure layers in the crystal structure. The layer is generated by a combination of the 2₁ screw axis along b and translation along the short a axis, neither of which generates a change in chirality. See Chan, Bishop, Craig, Scudder & Yue [Acta Cryst. (2008), E64, o841].

inorganic compounds

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Redetermination of the borax structure from laboratory X-ray data at 145 K

G. J. Gainsford, T. Kemmitt and C. Higham

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Zn₂(TeO₃)Br₂

D. Zhang and M. Johnsson

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Hafnium germanium telluride

G.-J. Jang and H. Yun

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metal-organic compounds

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Three-dimensional hydrogen-bonded supramolecular assembly in tetrakis(1,3,5-triaza-7-phosphaadamantane)copper(I) chloride hexahydrate

A. M. Kirillov, P. Smoleński, M. F. C. Guedes da Silva, M. N. Kopylovich and A. J. L. Pombeiro

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catena-Poly[[diaquazinc(II)]-μ-L-cysteinato(2−)-κ⁴S:S,N,O-[di-μ-sulfido-bis[oxidomolybdate(V)](Mo—Mo)]-μ-L-cysteinato(2−)-κ⁴S,N,O:S]

T. Shibahara, S. Ogasahara and G. Sakane

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Bis(pyridine-κN)bis(triphenylphosphine-κP)copper(I) tetrafluoridoborate

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Decacarbonyl-1κ³C,2κ³C,3κ⁴C-μ-hydrido-1:2κ²H:H-(μ-quinoline-2-thiolato-1:2κ²S:S)diosmium(I)osmium(0)(3 Os—Os)

Y. Sun, X.-B. Li and B.-W. Sun

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Bis[4-(4-methoxyphenyl)-4H-1,2,4-triazole-κN¹]bis(thiocyanato-κN)zinc(II)

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Bis(chloroacetato)-κ²O,O′;κO-methanol-κO-bis(2-methylfuro[3,2-c]pyridine-κN)copper(II)

D. Mikloš, J. Miklovič, V. Mrázová, J. Moncol and P. Segľa

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Di-μ-iodido-bis{[(4-fluorobenzoylmethylene)triphenyl-λ⁵-phosphorane]iodidomercury(II)}

M. Akkurt, K. Karami, Ş. P. Yalçın and O. Büyükgüngör

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Low-temperature phase of hexaguanidinium heptamolybdate monohydrate

S. Reinoso, M. H. Dickman, A. Praetorius and U. Kortz

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μ-4,4′-Bipyridyl-1:2κ²N:N′-methanol-2κO-tetrakis(tri-tert-butoxysilanethiolato)-1κ⁴O,S;2κ²S-dizinc(II)

A. Dołęga and K. Baranowska

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Poly[diaqua-μ₂-oxalato-di-μ₂-pyrimidine-2-carboxylato-dimanganese(II)]

A. Rodríguez-Diéguez, H. Aouryaghal, A. J. Mota and E. Colacio

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Tetraaquabis(biuret-κ²O,O′)yttrium(III) trichloride

W. T. A. Harrison

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Tetraaquabis(biuret-κ²O,O′)gadolinium(III) trichloride

W. T. A. Harrison

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trans-Dichloridobis(triphenylphosphine)palladium(II)

J. Pons, J. García-Antón, X. Solans, M. Font-Bardia and J. Ros

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(meso-5,5,7,12,12,14-Hexamethyl-1,4,8,11-tetraazacyclotetradecane)nickel(II) bis(O,O′-dibenzyl dithiophosphate)

B. Xie, L.-K. Zou, Y.-G. He, J.-S. Feng and X.-L. Zhang

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Dichlorido(2-chloro-9-mesityl-1,10-phenanthroline-κ²N,N′)cobalt(II) dichloromethane hemisolvate

Y. Yang, P. Yang, C. Zhang and B. Wu

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Diaquadimethanolbis[4-(1H-tetrazol-1-yl)benzoato]zinc(II) dihydrate

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{μ-6,6′-Dimethoxy-2,2′-[1,2-phenylenebis(nitrilomethylidyne)]diphenolato}methanolcopper(II)sodium(I)

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The cocrystal aquachlorido{6,6′-di-tert-butyl-2,2′-[1,2-phenylenebis(nitrilomethylidyne)]diphenolato-κ⁴O,N,N′,O′}manganese(III)–chlorido{6,6′-di-tert-butyl-2,2′-[1,2-phenylenebis(nitrilomethylidyne)]diphenolato-κ⁴O,N,N′,O′}(methanol-κO)manganese(III) (1/1)

N. E. Eltayeb, S. G. Teoh, S. Chantrapromma, H.-K. Fun and R. Adnan

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1,1′-(Butane-1,4-diyl)diimidazole-3,3′-diium tetrachloridozincate(II) dihydrate

Y.-H. Yu, A.-E. Shi, Y. Su, G.-F. Hou and J.-S. Gao

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[1,2-Bis(diphenylphosphino)ethane]{2-[bis(diphenylphosphinomethyl)amino]pyridinium}fluoridohydrazidatomolybdenum(IV) bis(tetrafluoridoborate)

G. Stephan, C. Näther and F. Tuczek

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Diaquabis(2,5-di-4-pyridyl-1,3,4-thiadiazole-κN²)bis(thiocyanato-κN)copper(II) dihydrate

W.-W. Ma and M.-H. Yang

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Bis{μ-2,2′-[(3-azapentane-1,5-diyl)bis(nitrilomethylidyne)]diphenolato}dicopper(II) dimethyl sulfoxide disolvate

G. Quintero-Tellez, C. M. González Álvarez, S. Bernès, J. L. Alcántara-Flores and Y. Reyes-Ortega

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(3,5-Dichlorosalicylaldehyde thiosemicarbazonato-κ³S,N¹,O)(N,N′-dimethylformamide-κO)copper(II) dimethylformamide solvate

Y. Wang, Z. Liu and J.-Y. Gao

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(Carbonyl-1κC)bis[2,3(η⁵)-cyclopentadienyl][μ₃-(S-methyl trithiocarbonato)methylidyne-1:2:3κ⁴C,S′′:C:C](triphenylphosphine-1κP)(μ₃-sulfido-1:2:3κ³S)dicobalt(II)iron(II) trifluoromethanesulfonate

A. R. Manning, C. J. McAdam, A. J. Palmer and J. Simpson

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Bis(2-bromopyridinium) hexachloridostannate(IV)

B. F. Ali, R. Al-Far and S. F. Haddad

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(2,2′-Bipyridine-κ²N,N′)iodido(pyrrolidine-1-dithiocarboxylato-κ²S,S′)copper(II)

L.-Q. Fan and J.-H. Wu

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(Di-2-pyridylamine-κ²N¹,N^1′)bis(methacrylato-κO)nickel(II) sesquihydrate

F. Meng, L. Xia and X. Zhu

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Poly[bis[chloridocopper(I)]-μ₄-1,4-bis[1-(3-pyridylmethyl)-1H-benzimidazol-2-yl]butane]

W.-P. Zhang, Y.-Y. Liu and J.-F. Ma

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Bis{4-[(Z)-(4-fluorobenzylamino)(phenyl)methylene]-3-methyl-1-phenyl-1H-pyrazol-5(4H)-onato-κ²N⁴,O}nickel(II)

X. Zhang, G.-Y. Zhang, D. Chen and Y.-J. Song

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Bis(5-amino-4-aminocarbonyl-1H-imidazol-3-ium) (5-amino-4-aminocarbonyl-1H-imidazol-3-ium-κO)-di-μ-chlorido-heptachlorido-dibismuth(III) monohydrate

L.-P. Lv, L.-J. He, W.-W. Li, W.-B. Yu and X.-C. Hu

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Hexaaquacobalt(II) bis[4-(2-hydroxybenzylideneamino)benzenesulfonate]

X.-S. Tai, Y.-M. Feng and F.-Y. Kong

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Bis{2-methoxy-6-[3-(methylamino)propyliminomethyl]phenolato}nickel(II) bis(perchlorate)

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Aquabis(1H-imidazole-κN³)bis(4-methylbenzoato)-κO;κO,O′-nickel(II)

W.-D. Song, R.-Z. Fan and H.-M. Wu

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Poly[aqua(μ₂-oxalato)(4-oxidopyridinium)erbium(II)]

C.-S. Gu, X.-M. Hao, W.-D. Song, H.-S. Lin and D.-Y. Ma

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Poly[(μ-3,5-dinitro-2-oxidobenzoato)(μ-3-hydroxypyridine)copper(II)]

J.-B. Yan, W.-D. Song, H. Wang and L.-L. Ji

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Bis(1H-imidazole-κN³)bis(1-naphthaleneacetato-κ²O,O′)cadmium(II)

W.-D. Song, L.-L. Ji and H.-M. Wu

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Poly[[diaquabis[μ-(2,4-dichlorophenoxy)acetato]calcium(II)] monohydrate]

W.-D. Song, X.-H. Huang, J.-B. Yan and D.-Y. Ma

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(2,2′-Bipyridine-κ²N,N′)bis(4-methylbenzoato-κ²O,O′)zinc(II)

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Bis[2-acetyl-3-methylpyrazine (2-hydroxybenzoyl)hydrazonato]zinc(II) monohydrate

X.-S. Tai, Y.-M. Feng and H.-X. Zhang

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cis-Dichloridobis[2-(hydroxymethyl)tetrahydrofuran-κ²O,O′]manganese(II)

L. B. Jerzykiewcz, J. Utko and P. Sobota

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Bis(μ-disulfur dinitrido)bis[diphenyltin(IV)]

A. P. M. Robertson, A. M. Z. Slawin and J. D. Woollins

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{2-[(3,5-Dichloro-2-oxidobenzylidene)amino-κ²N,O]-3-methylpentanoato-κO}(N,N′-dimethylformamide-κO)copper(II)

J. H. Xia, Z. Liu, Y. Wang and X. Z. Feng

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catena-Poly[[tetraaqua(μ-4,4′-bipyridine-κ²N:N′)zinc(II)] fumarate tetrahydrate]

Y. Tian, Y.-P. Wu, D.-S. Li, H. Wang and J.-W. Wang

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Bis[(2-pyridylmethyl)(triisopropylsilyl)amido]zinc(II)–toluene–tetrahydrofuran (4/2/1)

C. Koch, H. Görls and M. Westerhausen

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Di-μ-nicotinato-κ²N:O;κ²O:N-bis[aqua(ethylenediamine-κ²N,N′)(nicotinato-κN)cadmium(II)] dihydrate

J. Moncol, D. Mikloš, P. Segla and M. Koman

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Bis(η⁵-cyclopentadienyl)bis(2,4,6-trimethylphenyltellurolato)zirconium(IV)

A. L. Hector, W. Levason, G. Reid, S. D. Reid and M. Webster

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Bis[1-(2-hydroxyethyl)-2-methyl-5-nitro-1H-imidazole-κN³]silver(I) nitrate

H.-K. Fun, S. R. Jebas and T. Balasubramanian

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Chlorido{5,5′-dimethoxy-2,2′-[1,2-phenylenebis(nitrilomethylidyne)]diphenolato-κ⁴O,N,N′,O′}manganese(III)

N. E. Eltayeb, S. G. Teoh, S. Chantrapromma, H.-K. Fun and R. Adnan

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Tris[tris(1,10-phenanthroline-κ²N,N′)iron(II)] dodecatungstoferrate dihydrate

F.-X. Ma, Y.-G. Chen and D.-M. Shi

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Aquadioxidobis(pentane-2,4-dionato)uranium(VI) pyrazine solvate

T. Kawasaki and T. Kitazawa

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Tetrakis(μ₃-2-{[1,1-bis(hydroxymethyl)-2-oxidoethyl]iminomethyl}-6-methoxyphenolato)tetranickel(II) tetrahydrate

Y. Guo, L. Li, Y. Liu, J. Dong and D. Wang

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(2,2′-Bipyridyl-κ²N,N′)tetrakis(4-methylbenzoato-κO)manganese(II)

W.-D. Song, H. Wang and D.-Y. Ma

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(2-Formyl-6-methoxyphenolato-κ²O¹,O²)(perchlorato-κO)(1,10-phenanthroline-κ²N,N′)copper(II)

F.-Y. Dong, Y.-M. Sun, Y.-T. Li and Z.-Y. Wu

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Tetraaquabis(pyridine-3-sulfonato-κN)nickel(II)

B.-Y. Zhang, J.-J. Nie and D.-J. Xu

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μ-1,2-Di-4-pyridylethane-κ²N:N′-bis[bis(N,N-diisopropyldithiocarbamato-κ²S,S′)zinc(II)]

V. Avila and E. R. T. Tiekink

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Hydroxonium triaquabis(biuret-κ²O,O′)dichloridolanthanum(III) dichloride dihydrate

W. T. A. Harrison

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mer-Triaqua(1,10-phenanthroline-κ²N,N′)(sulfato-κO)magnesium(II)

L. Zhu, J. Huang, S.-Y. Han and Z. An

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(−)₅₄₅-fac-Δ-Tris(L-prolinato)cobalt(III) trihydrate

M. Kato, M. Hayashi, T. Fujihara and A. Nagasawa

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Retracted: Diaquabis(pyridine-2-carboxylato-κ²N,O)cobalt(II)

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{4-Bromo-2-[2-(isopropylamino)ethyliminomethyl]phenolato}thiocyanatocopper(II)

J.-Y. Ma and Y.-T. He

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Di-μ-chlorido-bis({9-[(2,6-diisopropylphenyl)iminomethyl]anthracen-1-yl}palladium(II))

J. Zhou, Q. Wang and H. Sun

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Acta Cryst. (2008). E64, m689-m690
doi: 10.1107/S1600536808010