Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 65| Part 2

ISSN: 2056-9890

February 2009 issue

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Cover illustration: The compound, C₂₂H₃₀O₇, has anti-cancer and anti-malarial properties. Its crystal structure reveals a fused-five ring system containing six- and seven-membered rings including a peroxy bridge. See Gul, Carvalho, Galal, Avery & El Sohly [Acta Cryst. (2009). E65, o358-o359].

editorial

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Structure Reports Online: successful transition to open access

W. T. A. Harrison, J. Simpson and M. Weil

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inorganic compounds

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Rietveld refinement of a natural cobaltian mansfieldite from synchrotron data

M. Zoppi and G. Pratesi

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Redetermination of EuScO₃

V. Kahlenberg, D. Maier and B. Veličkov

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Holmium dodecaiodidoiron-octahedro-hexaholmium, {FeHo₆}I₁₂Ho

K. Daub and G. Meyer

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LiHo(PO₃)₄

E. Ben Zarkouna, A. Driss and M. Férid

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La variété β-NaMoO₂(AsO₄)

S. Ben Hlila, M. F. Zid and A. Driss

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Cs₁₀Ta_29.27O₇₈

M. Zeuner, A. Hofer and W. Schnick

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metal-organic compounds

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Pentacarbonyl-2κ⁵C-chlorido-1κCl-bis[1(η⁵)-cyclopentadienyl](μ-1-oxidoethylene-1:2κ²O:C)chromium(0)zirconium(IV)

C. Esterhuysen, L. Retief, G. J. Kruger, S. Cronje and H. G. Raubenheimer

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{μ-6,6′-Dimethoxy-2,2′-[propane-1,3-diylbis(nitrilomethylidyne)]diphenolato}dimethanoltrinitratonickel(II)samarium(III) methanol disolvate

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1-Acetyl-5-ferrocenyl-3-phenyl-2-pyrazoline

N. Karadayı, G. Turgut Cin, S. Demirel, A. Çakıcı and O. Büyükgüngör

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Tris(2,2′-bipyridyl-κ²N,N′)copper(II) sulfate 7.5-hydrate

F. Xu, W. You and W. Huang

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Tetrakis(2,2′-bipyridyl)dichloridodi-μ₃-hydroxido-di-μ₂-hydroxido-tetracopper(II) dinitrate hexahydrate

Y. Fan, Y.-T. Cui, H.-F. Qian, J.-L. Liu and W. Huang

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2-(4-Pyridinio)benzimidazolium tetrachloridopalladium(II)

J. Chen and S.-F. Wu

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Poly[(3-nitrobenzoato)(μ₃-1,2,4-triazolato)cobalt(II)]

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catena-Poly[[diaqua(4,4′-trimethylenedipyridine-κN)cobalt(II)]-μ-terephthalato-κ²O¹:O⁴]

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Dichlorido(dipyrido[3,2-a:2′,3′-c]phenazine)manganese(II)

M.-L. Xu, S.-B. Sun, X.-Y. Li and G.-B. Che

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catena-Poly[[aquatrimethyltin(IV)]-{[trimethyltin(IV)]-μ₃-thiophene-2,5-dicarboxylato}]

S.-X. Yang, Y.-Z. Li and K. Jiang

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Dichlorido{[2-(diphenylphosphino)phenyliminomethyl]ferrocene-κ²N,P}platinum(II) dichloromethane hemisolvate

Y. Xie, Y. Wei, J.-G. Hu, J.-S. Zhao and F.-X. Jiang

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Bis{benzyl N′-[(1H-indol-3-yl)methylene]dithiocarbazato-κ²N′,S}copper(II) N,N-dimethylformamide disolvate

H. Khaledi, H. Mohd Ali and S. W. Ng

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Chloridobis[diphenylglyoximato(1–)-κ²N,N′](1H-imidazole-κN³)cobalt(III) hemihydrate

P. Meera, C. Revathi and A. Dayalan

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[(2-Morpholinoethyl)(2-pyridylmethylene)amine]dithiocyanatozinc(II)

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(2,2′-Bipyridine-κ²N,N′)(4-hydroxy-2-oxidobenzaldehyde thiosemicarbazonato-κ³O²,N¹,S)zinc(II)

K. W. Tan, C. H. Ng, M. J. Maah and S. W. Ng

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Di-μ-chlorido-bis[chlorido(1,4,6-trimethyl-6-nitro-1,4-diazepine)copper(II)]

A. J. Bortoluzzi, A. Neves, R. A. Peralta, T. P. Camargo and V. C. Weiss

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catena-Poly[[[triaqua(nitrato-κ²O,O′)neodymium(III)]-bis(μ₂-pyridinium-4-carboxylato-κ²O:O′)] bis(perchlorate) monohydrate]

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Bis(pyridine-3-carboxylic acid-κN)silver(I) perchlorate

X.-Y. Nie and Q.-Z. Li

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Hexakis(1-methyl-1H-imidazole-κN³)cobalt(II) dibromide dihydrate

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Retracted: Tetrakis(μ-2,4-difluorobenzoato)bis[(2,2′-bipyridine)(2,4-difluorobenzoato)terbium(III)]

L. Hao and X. Liu

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Retracted: Bis(6-methoxy-2-{[tris(hydroxymethyl)methyl]iminomethyl}phenolato)copper(II) dihydrate

X. Zhang, P. Wei, J. Dou, B. Li and B. Hu

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Diaqua{6,6′-dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato-κ²O,N,N′,O′}manganese(III) perchlorate 18-crown-6 hemisolvate monohydrate

Z.-X. Li, X. Li, L.-F. Zhang and M.-M. Yu

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catena-Poly[[bis(3-methyl-4-nitropyridine N-oxide-κO)cadmium(II)]-di-μ-dicyanamido-κ⁴N¹:N⁵]

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Dichloridobis(phenyl 2-pyridyl ketone oxime)nickel(II) acetone solvate

J.-Z. Yin and G.-X. Liu

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[1,2-Bis(diphenylphosphino)ethane-κ²P,P′](2-carboxylatothiophenolato-κ²O,S)nickel(II) methanol solvate

J. Miao, F. Li, H. Chen, D. Wang and Y. Nie

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Di-μ-chlorido-bis{aquachlorido[3-ethyl-4-phenyl-5-(2-pyridyl)-4H-1,2,4-triazole-κ²N¹,N⁵]manganese(II)}

Z. Wang, I. Gong, C. Liu and X. Zhang

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[Bis(diphenylphosphino)methane-κ²P,P′]dichloridopalladium(II)

M. Shahid, Imtiaz-ud-Din, M. Mazhar, M. Zeller and A. D. Hunter

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Chlorido[N′-(2-oxidobenzilidene)acetohydrazide-κ²O,N′,O′]copper(II) dihydrate

F. B. Tamboura, M. Gaye, A. S. Sall, A. H. Barry and Y. Bah

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[μ-10,22-Dichloro-3,6-bis(2-furylmethyl)-3,6,14,18-tetraazatricyclo[18.3.1.1^8,12]pentacosa-1(23),8,10,12(25),13,18,20(24),21-octaene-24,25-diolato-κ⁸N³,N⁶,O²⁴,O²⁵:N¹⁴,N¹⁸,O²⁴:O²⁵]bis[chloridocopper(II)] acetonitrile solvate

C. Chen, Y. Cheng, P. Liu, H. Zhou and Z.-Q. Pan

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catena-Poly[diethyl(2-hydroxyethyl)ammonium [[tetra-μ-acetato-κ⁸O:O′-dicuprate(II)(Cu—Cu)]-μ-acetato-κ²O:O′] dichloromethane solvate]

M. Shahid, M. Mazhar, P. O'Brien, M. Afzaal and J. Raftery

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1,3-Bis(2-thienylmethyl)-4,5-dihydroimidazolium trichlorido(η⁶-p-cymene)ruthenate(II)

H. Arslan, D. VanDerveer, İ. Özdemir, N. Gürbüz, Y. Gök and B. Çetinkaya

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catena-Poly[[diaquacalcium(II)]-di-μ-2-chloronicotinato]

L. Quan, H. Yin, L. Cui and M. Yang

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catena-Poly[[diaquacopper(II)]-μ-7-oxabicyclo[2.2.1]heptane-2,3-dicarboxylato]

Y.-Y. Wang, R.-D. Hu and Y.-J. Wang

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fac-Aquadichloridotris(tetramethylene sulfoxide-κS)ruthenium(II)

R. S. Srivastava, C. F. Gonzales and F. R. Fronczek

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(18-Crown-6-κ⁶O)(pyrazolato-κ²N,N′)-potassium(I)

K. Kunz, H.-W. Lerner and M. Bolte

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Tetraaquabis(N-phenylsulfonyl-L-leucinato)cadmium(II) dihydrate

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trans-Bis(acetonitrile-κN)tetraaquacobalt(II) tetrachloridocobaltate(II)

V. Patroniak and M. Kubicki

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2-Acetylpyridinium 3-amino-2-chloropyridinium tetrachloridocobaltate(II)

A. Adamski, V. Patroniak and M. Kubicki

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Poly[[aqua(μ₂-oxalato)(μ₂-2-oxidopyridinium-3-carboxylato)dysprosium(III)] monohydrate]

C.-D. Huang, J.-X. Huang, Y.-Y. Wu, Y.-Y. Lian and R.-H. Zeng

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Bis(μ-dimesitylborinato-κ²O:O)bis[(2-methylpyridine-κN)lithium]

K. T. P. Saravana, J.-H. Son and J. D. Hoefelmeyer

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Bis(2,2′-bipyridine-κ²N,N′)dichloridoplatinum(IV) dichloride monohydrate

N.-H. Kim, I.-C. Hwang and K. Ha

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Diazidobis[4,4,5,5-tetramethyl-2-(1,3-thiazol-2-yl)-2-imidazoline-1-oxyl-3-oxide-κ²O,N]manganese(II)

J. L. Chang, Z. Y. Gao and K. Jiang

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Bis(4-ammonio-4-methylpentan-2-one-κO)dioxalato-κ⁴O¹,O²-copper(II)

Z. Ji, S. Wei and W. Wu

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A second modification of poly[diaquadi-μ-citrato(3−)-trizinc(II)]

X.-H. Li, W.-L. Chen and E.-B. Wang

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catena-Poly[[[aqua(1,10-phenanthroline)cadmium(II)]-μ-benzene-1,4-dicarboxylato] benzene-1,4-dicarboxylic acid hemisolvate]

Z. Wang, W. Han and Z. Liu

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Hydroxonium hydrate tris(2,4,6-triamino-1,3,5-triazin-1-ium) bis[bis(pyridine-2,6-dicarboxylato)cuprate(II)] pyridine-2,6-dicarboxylic acid hexahydrate

H. Aghabozorg, J. Attar Gharamaleki, M. M. Olmstead, Z. Derikvand and S. Hooshmand

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{6,6′-Dimethoxy-2,2′-[o-phenylenebis(nitrilomethylidyne)]diphenolato}cobalt(II) dichloromethane disolvate

A. Nabei, T. Kuroda-Sowa, T. Okubo, M. Maekawa and M. Munakata

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{2-[1-(2-Amino-2-methylpropylimino)ethyl]phenolato-κ³N,N′,O}dioxidovanadium(V)

G. Romanowski, M. Wera and A. Sikorski

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(3,5,7-Tribromotropolonato-κ²O,O′)tris(triphenylphosphine-κP)silver(I)

G. Steyl and T. N. Hill

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fac-[N,N′-Bis(3-chloro-2-fluorobenzylidene)ethylenediamine]bromidotricarbonylrhenium(I)

R. Kia and H.-K. Fun

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Aqua(2,9-dimethyl-1,10-phenanthroline-κ²N,N′)bis(2-hydroxybenzoato-κO)manganese(II) 2,9-dimethyl-1,10-phenanthroline hemisolvate

P.-Z. Zhao, F.-M. Yan and J.-G. Wang

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[1,1′-Diphenyl-3,3′-(propane-1,3-diyldinitrilo)dibut-1-enolato]copper(II)

M. Salehi, S. Meghdadi, M. Amirnasr and K. Mereiter

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[N,N′-Bis(4-chlorobenzylidene)-2,2-dimethylpropane-1,3-diamine-κ²N,N′]iodidocopper(I)

R. Kia, H.-K. Fun and H. Kargar

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Bis{6,6′-dimethoxy-2,2′-[ethane-1,2-diylbis(iminomethylene)]diphenolato(1.5−)-κ⁴O,N,N′,O′}erbium(III)

H.-T. Xia, D.-F. Rong, Y.-Y. Zhang, S.-P. Yang and D.-Q. Wang

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Bis{6,6′-dimethoxy-2,2′-[ethane-1,2-diylbis(iminomethylene)]diphenolato(1.5−)-κ⁴O,N,N′,O′}praeseodymium(III)

H.-T. Xia, Y.-F. Liu, S.-P. Yang and D.-Q. Wang

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Bis{6,6′-dimethoxy-2,2′-[ethane-1,2-diylbis(iminomethylene)]diphenolato(1.5−)-κ⁴O,N,N′,O′}terbium(III)

H.-T. Xia, Y.-F. Liu, S.-P. Yang and D.-Q. Wang

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(4,4′-Di-tert-butyl-2,2′-bipyridine-κ²N,N′)bis(nitrato-κ²O,O′)copper(II)

X. Xiao, Z.-Y. Rao, Y.-Q. Zhang, S.-F. Xue and Z. Tao

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Acta Cryst. (2009). E65, m203-m204
doi: 10.1107/S1600536809001159