Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 66| Part 1

ISSN: 2056-9890

January 2010 issue

Highlighted illustration

Cover illustration: The molecule 6-(1-methylethyl)-12-phenyl-5,6,7,12-tetrahydrodibenz[c,f][1,5]azasilocine, C₂₃H₂₅NSi, is an example of a highly coordinated hydrosilane. The silicon atom adopts a distorted trigonal-bipyramidal geometry with a short transannular SiN distance of 2.6294 (18) Å. Unusually, the Si-H hydrogen atom occupies an axial rather than an equatorial site. See Goto, Fukushima & Kawashima [Acta Cryst. (2010). E66, o20].

editorial

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Editorial

W. T. A. Harrison, J. Simpson and M. Weil

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international union of crystallography

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Notes for authors 2010

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inorganic compounds

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LaZnB₅O₁₀, the first lanthanum zinc borate

Z.-W. Jiao, R.-J. Wang, X.-Q. Wang, D.-Z. Shen and G.-Q. Shen

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Scheelite-type NaDy(WO₄)₂

D. Zhao, F. Li, W. Cheng and H. Zhang

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metal-organic compounds

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catena-Poly[[diiodidocadmium(II)]-μ-4,4′-di-4-pyridyl-2,2′-disulfanediyldipyrimidine]

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catena-Poly[[diazidozinc(II)]-μ-di-4-pyridylamine-κ²N:N′]

A. M. Hardy and R. L. LaDuca

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Bis(2-phenyl-1H-imidazole-κN³)silver(I) nitrate

S. Han, W.-C. Li and D.-C. Xia

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catena-Poly[[trimethyltin(IV)]-μ-2-methylbenzoato-κ²O:O′]

M. Danish, I. Saleem, N. Ahmad, W. Starosta and J. Leciejewicz

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Aquabis(2,3-dimethyl-4-oxo-4H-pyrido[1,2-a]pyrimidin-9-olato)nickel(II)

H. Zhang, Y. Sun, X. Chen, F. Yu and Z. Zou

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Bis(N-triisopropylsilylquinolin-8-aminato)nickel(II)

A. Malassa, B. Jäger, H. Görls and M. Westerhausen

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Dibromido(1,10-phenanthroline-κ²N,N′)palladium(II)

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Dibromidodi-μ-hydroxido-di-μ₃-oxido-octaphenyltetratin(IV)

Q. L. Yap, K. M. Lo and S. W. Ng

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Tetrakis(μ₂-3,4-dimethoxyphenylacetato)-κ³O,O′:O′;κ³O:O:O′;κ²O:O′;κ²O:O′-bis[(3,4-dimethoxyphenylacetato-κ²O,O′)(1,10-phenanthroline-κ²N,N)thulium(III)]

J.-L. Liu, H.-Q. Li and G.-L. Zhao

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Poly[[(N,N-dimethylformamide-κO)(μ₃-pyrazine-2,3-dicarboxylato-κ⁴N¹,O²:O³:O³)copper(II)] monohydrate]

Z.-Z. Fan, G.-P. Wang and Y.-S. Li

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Tris(2,2′-bipyridine-κ²N,N′)cobalt(III) octacyanidotungstate(V)

Q. Jun and C. Zhang

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Tetrakis(2-aminothiazole-κN³)dichloridocadmium(II)

C.-H. Kim and I. H. Kim

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Bis[2-(cyclohexyliminomethyl)-5-methoxyphenolato]copper(II)

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catena-Poly[[(3-methylsulfanyl-1,2,4-thiadiazole-5-thiolato)sodium]di-μ-aqua-κ⁴O:O]

J.-H. Zhang, C.-L. Ma, R.-F. Zhang, H.-Z. Wang and G.-J. Fu

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Poly[tetrakis(μ-cyclohexane-1,4-dicarboxylato)di-μ-hydroxido-pentazinc(II)]

J.-X. Chen and W.-W. Meng

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(4′-Allyloxy-2,2′:6′,2′′-terpyridine-κ³N,N′,N′′)(dibenzoylmethanido-κ²O,O′)bis(nitrato-κ²O,O′)neodymium(III) acetonitrile solvate

Q. Mei and B. Tong

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Dimethanolbis[4,4,5,5-tetramethyl-2-(5-methylimidazol-4-yl)-2-imidazoline-1-oxyl-3-oxide-κ²O,N]cobalt(II) diperchlorate

Z. Y. Gao, H. J. Guo and W. B. Zhang

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Sodium 5-amino-1,3,4-thiadiazole-2-thiolate dihydrate

J. Wu, Y. Wang, G. Yi and S. Luo

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Hexakis(dimethyl sulfoxide-κO)cobalt(III) trinitrate

Q. Li and S. W. Ng

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An orthorhombic polymorph of 1-[(ferrocenyl)(hydroxy)methyl]-1,2-dicarba-closo-dodecaborane

H. Chen, J. Miao, P. Zhu, D. Wang and Y. Nie

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catena-Poly[[diaquazinc(II)]-μ₃-2,2′-dihydroxy-1,1′-binaphthyl-3,3′-dicarboxylato-κ³O:O′:O′′]

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Bis[tris(ethane-1,2-diamine)nickel(II)] octacyanidomolybdate(IV) pentahydrate

Q. Jun and C. Zhang

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Diaqua-1κO,2κO-(2,2′-bi-1H-imidazole-1κ²N³,N^3′)(oxalato-2κ²O¹,O²)di-μ-oxido-κ⁴O:O-dioxido-1κO,2κO-dimolybdenum(V) trihydrate

X. Zhang, P. Wei, C. Shi, B. Li and B. Hu

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Di-μ-methoxido-μ-oxido-bis[triphenylantimony(V)] methanol disolvate

R. Betz, S. Junggeburth, P. Klüfers and P. Mayer

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catena-Poly[[(liriodenine-κ²N,O)lead(II)]-di-μ-chlorido]

Y.-T. Qin, L. Tao, T.-J. He, Y.-C. Liu and Z.-F. Chen

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Bis{[μ-bis(diphenylphosphino)methane-1:2κ²P:P′]nonacarbonyl-1κ³C,2κ³C,3κ³C-[tris(4-methoxyphenyl)arsine-3κAs]-triangulo-triruthenium(0)} dichloromethane solvate

O. bin Shawkataly, I. A. Khan, C. S. Yeap and H.-K. Fun

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Poly[bis(2,2′-bipyridine-κ²N,N′)heptadeca-μ-oxido-tetraoxidodicopper(II)divanadate(IV)hexavanadate(V)]

H. Yu and L. Kong

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Poly[hexaaquabis(μ₃-terephthalato)(μ₂-terephthalato)diytterbium(III)]

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Bis(3,4-dimethoxybenzoato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)copper(II)

Y. Liu, J. Sun and X. Niu

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catena-Poly[[[triaquacadmium(II)]-μ-2,2′-[oxalylbis(azanediyl)]diacetato-κ²O,O′] dihydrate]

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[μ-Bis(diphenylarsino)methane-1:2κ²As:As′]nonacarbonyl-1κ³C,2κ³C,3κ³C-[tris(4-methylphenyl)phosphine-3κP]-triangulo-triruthenium(0)

O. bin Shawkataly, I. A. Khan, C. S. Yeap and H.-K. Fun

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Dichlorido(1,10-phenanthroline-κ²N,N′)palladium(II)

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Bis[2-methoxy-6-(3-pyridylmethyliminomethyl)phenolato-κ²N,O]copper(II)

X. Chen, Y. Sun, Q. Yao, H. Zhang and Q. Liang

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Aqua[4-chloro-2-(2-pyridylmethyliminomethyl)phenolato]copper(II) nitrate monohydrate

Q. Liang, X. Chen, H. Zhang and Z. Zou

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catena-Poly[[di-μ-iodido-dicopper(I)(Cu—Cu)]bis(μ-4,4′-di-3-pyridyl-2,2′-disulfanediyldipyrimidine)]

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trans-(2,2′-Bipyrimidine)diiodido(isopropoxido)oxidorhenium(V)

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catena-Poly[4,4′-bipyridinium [[diaquadisulfatocadmium(II)]-μ-4,4′-bipyridine-κ²N:N′] dihydrate]

W. Xu, B.-J. Huang and L.-F. Qiu

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Aquachlorido{μ-6,6′-diethoxy-2,2′-[1,2-phenylenebis(nitrilomethylidyne)]diphenolato}copper(II)sodium(I) N,N-dimethylformamide solvate

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(Carbonato-κ²O,O′)bis(1,10-phenanthroline-κ²N,N′)cobalt(III) nitrate monohydrate

Ö. Andaç, Z. Yolcu and O. Büyükgüngör

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Bromido[(1,2,5,6-η)-cycloocta-1,5-diene]methylplatinum(II)

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1-(4-Ferrocenylphenyl)-3-methylimidazolium iodide monohydrate

D. Onyancha, C. McCleland, T. Gerber, E. Hosten and P. Mayer

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Aquaazido{3,3′-[o-phenylenebis(nitrilomethylidyne)]di-2-naphtholato}manganese(III)

C.-J. Wang, X.-L. Zhou and B.-J. Zhang

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[N,N-Bis(diphenylphosphino)propylamine-κ²P,P′]dichloridoplatinum(II)

N. Cloete, H. G. Visser and A. Roodt

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Poly[diaquabis(μ-4-carboxy-2-propyl-1H-imidazole-5-carboxylato-κ³N³,O⁴:O⁵)calcium(II)]

W.-D. Song, J.-B. Yan, S.-J. Li, D.-L. Miao and X.-F. Li

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Bis(μ-4-hydroxybenzoato-κ²O:O′)bis[triaquabis(4-hydroxybenzoato)-κO;κ²O,O′-terbium(III)] decahydrate

Y.-M. Zhu, P.-P. Feng, Y.-Y. Yang and S. W. Ng

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μ-Adipato-κ²O¹:O⁴-bis{[2,6-bis(1H-benzimidazol-2-yl-κN³)pyridine-κN](nitrato-κO)lead(II)}

L.-Q. Wei, M.-H. Zeng and S. W. Ng

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[1,2-Bis(1H-benzimidazol-2-yl-κN³)ethane]dichloridozinc(II)

Y.-L. Zhou, M.-H. Zeng and S. W. Ng

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catena-Poly[[[dichloridozinc(II)]-μ-1,4-bis(1H-benzimidazol-2-yl-κN³)butane] 1,4-bis(1H-benzimidazol-2-yl)butane solvate]

Y.-L. Zhou, M.-H. Zeng and S. W. Ng

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catena-Poly[zinc(II)-μ₃-{hydrogen [1-hydroxy-2-(3-pyridinio)ethane-1,1-diyl]diphosphonato}]

X. Huang, Z. Liu, C. Huang and Y. Wang

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Tetra-μ-benzoato-bis{[4-(pyrrolidin-1-yl)pyridine]zinc(II)}

S. M. Yu, K. Koo, P.-G. Kim, C. Kim and Y. Kim

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catena-Poly[[trimethyltin(IV)]-μ-(1,1′-binaphthyl-2,2′-diyl phosphonato)]

J. Wu and R. Zhang

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Chlorido[3,3′-dibutyl-5,5′-(pyridine-2,6-diyl)dipyrazol-1-ido]gold(III)

A. S. K. Hashmi, C. Lothschütz and F. Rominger

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Diiodido(1,10-phenanthroline-κ²N,N′)platinum(II)

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mer-Bis[3,5-difluoro-2-(2-pyridyl)phenyl-κ²C¹,N]{5-(2-pyridyl-κN)-3-[3-(4-vinylbenzyloxy)phenyl]-1,2,4-triazol-1-ido}iridium(III) methanol solvate

P. G. Jones, M. Debeaux, A. Weinkauf, H. Hopf, W. Kowalsky and H.-H. Johannes

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Bis(benzo-15-crown-5-κ⁵O)barium tetrakis(isothiocyanato-κN)cobaltate(II)

Z. Cao, K. Liu, M. Niu and D. Wang

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Aqua(2-oxido-2,2-diphenylacetato-κ²O¹,O²)(1,10-phenanthroline-κ²N,N′)copper(II)

X.-X. Yang, F.-Y. Zhang and S.-H. Xu

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Aqua(6,6′-oxydipicolinato-κ²O,N,N′,O′)copper(II)

J. Sun and X. Tong

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{μ-trans-N,N′-Bis[2-(2-hydroxyethylamino)ethyl]oxamidato(2−)}bis[picratonickel(II)]

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Tris[2-methoxy-6-(4-methylphenyliminiomethyl)phenolato-κ²O,O′]tris(thiocyanato-κN)neodymium(III)

J.-L. Liu, J.-B. Shen and G.-L. Zhao

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(Benzyldiphenylphosphine-3κP)[μ-bis(diphenylarsino)methane-1:2κ²As:As′]nonacarbonyl-1κ³C,2κ³C,3κ³C-triangulo-triruthenium(0)

O. bin Shawkataly, I. A. Khan, C. S. Yeap and H.-K. Fun

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Bis[μ-2-(2,4-difluorophenyl)-1,3-bis(1,2,4-triazol-1-yl)propan-2-olato-κ⁴N²,O:O,N^2′]bis[(acetato-κ²O,O′)nickel(II)] methanol hemisolvate

F. Zhang, F.-L. Hu, Z.-J. Huang, J.-C. Zhuang and Y. Zhuang

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