Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 65| Part 6

ISSN: 2056-9890

June 2009 issue

Highlighted illustration

Cover illustration: The molecular compound [Ru( [eta] ⁵-C₅H₅){ [eta] ⁶-C₆H₂(CH₃)₃NH₂}]PF₆ contains an Ru^II atom sandwiched between a cyclopentadienyl and a substituted benzene ring. The mesitylamine unit is significantly non-planar at the ipso-carbon of the amino group and deviates by 0.107 (3) Å from the least-squares plane of the benzene ring. See Becker, Kirchner & Mereiter [Acta Cryst. (2009). E65, m631].

inorganic compounds

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Rb₂Sb₄O₁₁

G. Kalpana and M. T. Weller

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Lithium diaquanickel(II) catena-borodiphosphate(V) monohydrate

J. Zheng and A. Zhang

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Pr₅Si₃N₉

S. Lupart and W. Schnick

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RbCa₂Nb₃O₁₀ from X-ray powder data

Z.-H. Liang, K.-B. Tang, Q.-W. Chen and H.-G. Zheng

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Nd₂(WO₄)₃

M. Weil, B. Stöger and L. Aleksandrov

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Sr₅(V^IVOF₅)₃F(H₂O)₃ refined from a non-merohedrally twinned crystal

A. Le Bail, A.-M. Mercier and I. Dix

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metal-organic compounds

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The ansa-bridged cyclopentadienyl titanium complex [{η⁵-C₅Me₄CH₂-C(NMe₂)=N}TiCl₂]

D. Guo, H.-B. Tong and M. Zhou

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cis-Bis(nitrato-κ²O,O′)bis(triethylphosphine oxide-κO)nickel(II)

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Bis{μ-1,3-bis[(benzimidazol-1-yl)methyl]benzene-κ²N³:N^3′}bis[dichloridozinc(II)] dimethylformamide disolvate

L.-Z. Zhao, P. Li, B.-L. Cao and S. W. Ng

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[13,27-Dichloro-3,6,9,17,20,23-hexaazatetracyclo[23.3.1.1^11,15.0^2,6]triaconta-1(29),9,11,13,15(30),16,23,25,27-nonaene-29,30-diol-κ⁵N¹⁷,N²⁰,N²³,O²⁹,O³⁰]bis(nitrato-κ²O,O′)europium(III) nitrate methanol hemisolvate

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Redetermination of (2,2′-bipyridine-κ²N,N′)dichloridopalladium(II) dichloromethane solvate

N.-H. Kim, I.-C. Hwang and K. Ha

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{N,N′-Bis[(E)-3-phenylprop-2-en-1-ylidene]propane-1,3-diamine-κ²N,N′]dichloridocobalt(II)

M. Montazerozohori, M. H. Habibi, M. Amirnasr, K. Ariyoshi and T. Suzuki

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catena-Poly[[diaqua(1H-imidazo[4,5-f][1,10]phenanthroline)cobalt(II)]-μ-sulfato]

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Bis[2-(2H-benzotriazol-2-yl)-4-methylphenolato]palladium(II)

C.-Y. Tsai, C.-H. Lin and B.-T. Ko

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Hexaaquacadmium(II) dipicrate monohydrate

S. Natarajan, K. Moovendaran, S. A. M. B. Dhas, J. Suresh and P. L. N. Lakshman

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catena-Poly[hemi(hexane-1,6-diammonium) [[aquadibromidomanganese(II)]-μ-pyridine-2-carboxylato]]

N.-H. Kim, I.-C. Hwang and K. Ha

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Diazidobis[2,4-diamino-6-(2-pyridyl)-1,3,5-triazine-κ²N¹,N⁶]zinc(II)

Q.-H. Zhao, A.-L. Fan, L.-N. Li and M.-J. Xie

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Poly[aqua[μ₂-1,2-bis(imidazol-1-ylmethyl)benzene-κ²N³:N^3′](μ₂-5-bromobenzene-1,3-dicarboxylato-κ³O¹,O^1′:O³)nickel(II)]

K. Zhu, H. Chen and G.-X. Liu

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Bis[μ-1,1′-(ferrocene-1,1′-diyl)bis(butane-1,3-dionato)]di-μ-methanol-diiron(II)

Y.-F. Xiao, H.-F. Li, P.-F. Yan and G.-M. Li

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catena-Poly[[tetraaquanickel(II)]-μ₃-benzene-1,3,5-tricarboxylato-3′:1:2-κ⁴O¹:O³,O^3′:O⁵-[tetraaquanickel(II)]-μ₂-benzene-1,3,5-tricarboxylato-2:3κ²O¹:O³-[tetraaquanickel(II)]]

S.-C. Hsu, P.-H. Chiang, C.-H. Chang and C.-H. Lin

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Diaquabis[4-(dimethylamino)benzoato]-κ²O,O′;κO-(isonicotinamide-κN¹)cobalt(II)

T. Hökelek, H. Dal, B. Tercan, Ö. Aybirdi and H. Necefoğlu

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Poly[[μ₄-tartrato-cadmium(II)] 0.167-hydrate]

L.-Z. Zhao, P. Li, B.-L. Cao and S. W. Ng

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Dipyridinium tribromidochloridobis(4-chlorophenyl)stannate(IV)

K. M. Lo and S. W. Ng

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(η⁵-Cyclopentadienyl)(η⁶-mesitylamine)ruthenium(II) hexafluoridophosphate

E. Becker, K. Kirchner and K. Mereiter

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Poly[(μ₂-azido-κ²N¹:N¹)[μ₂-5-(8-quinolyloxymethyl)tetrazolato-κ⁴N¹,O,N⁵:N⁴]zinc(II)]

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trans-Diaquabis[(E)-3-(dimethylamino)-1-(2-pyridyl)prop-2-en-1-one-κ²N¹,O]cobalt(II) dinitrate dihydrate

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Bis[4-(2-hydroxybenzylideneamino)benzoato-κO]tetrakis(methanol-κO)manganese(II)

M. Zhong, J.-H. Lin, J. Shang, T.-H. Huang and X.-J. Wang

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Bis(2,2′-bipyridyl-κ²N,N′)(nitrato-κ²O,O′)(trifluoroacetato-κO)cadmium(II)

W. Duan, J. Sun, Y. Ma and R. Wu

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trans-Tetrachloridobis(diphenylacetonitrile)platinum(IV)

N. A. Bokach, V. Y. Kukushkin and M. Haukka

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trans-Bis(5-carboxy-2-methyl-1H-imidazole-4-carboxylato-κ²N³,O⁴)copper(II)

X. Guo, Y. L. Li, J. X. Wang and Y. C. Wang

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Bis(benzimidazole-κN³)bis(2-benzoylbenzoato-κO)copper(II)

M. H. Yıldırım, Z. Heren, H. Paşaoğlu, D. Hıra and O. Büyükgüngör

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trans-Diaquabis(6-methoxycarbonylpyridazine-3-carboxylato-κ²N,O)zinc(II) dihydrate

W. Starosta and J. Leciejewicz

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Tris(phenyl 2-pyridyl ketone oxime-κ²N,N′)cadmium(II) dinitrate

J. Yan and G.-X. Liu

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Bis(di-2-pyridylmethanediol-κ³N,O,N′)copper(II) bis(tetrafluoridoborate) dihydrate

K. L. Brown, G. Crundwell and B. L. Westcott

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Bis[tris(3-tert-butyl-5-methylpyrazol-1-yl)hydridoborato]ytterbium(II) toluene solvate

K. O. Saliu, J. Takats and M. J. Ferguson

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Bis[4-(dimethylamino)pyridinium] pentabromidochloridostannate(IV)

Y. Jang, K. M. Lo and S. W. Ng

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Tetra-μ-acetato-κ⁸O:O′-bis[(N²,N²-dimethylpyrazin-2-amine-κN⁴)copper(II)]

L. Meng, L. Y. Yang and J. M. Shi

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Aqua(propanedioato-κ²O¹,O³)[2-(1H-pyrazol-1-yl-κN²)-1,10-phenanthroline-κ²N,N′]nickel(II) trihydrate

H. Y. Yan, T. Q. Hu and J. M. Shi

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Poly[[tetraaquabis(μ-hydroxyacetato-κ⁴O¹,O²:O¹,O^1′)-μ₂-sulfato-κ²O:O′-dicadmium(II)] monohydrate]

U. Rychlewska, B. Warzajtis, M. D. Dimitrijević, N. S. Draskovic and M. I. Djuran

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Tris{2-methoxy-6-[(4-methylphenyl)iminiomethyl]phenolato-κ²O,O′}tris(thiocyanato-κN)cerium(III)

J.-F. Liu, H.-D. Xian and G.-L. Zhao

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Diaquabis[4-(dimethylamino)benzoato](isonicotinamide)zinc(II)

T. Hökelek, H. Dal, B. Tercan, Ö. Aybirdi and H. Necefoğlu

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Tetraaqua(1,10-phenanthroline-5,6-dione-κ²N,N′)cobalt(II) dinitrate

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Bis(μ-5-carboxylato-1-carboxylatomethyl-2-oxidopyridinium)-κ²O⁵:O¹;κ²O¹:O⁵-[diaqua(phenanthroline-κ²N,N′)manganese(II)] dihydrate

M.-X. Jiang and Y.-L. Feng

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2,2′-(Hexane-1,6-diyl)diisoquinolinium tetrachloridozincate(II)

P.-H. Ma, Z.-F. Fan, Y.-Q. Zhang, X. Xiao and S.-F. Xue

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Triphenylbis[4-(trifluoromethyl)benzoato-κO]antimony(V)

L. Quan, H. Yin, L. Cui, M. Yang and D. Wang

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A neutral cubane with a Zn^II₄O₄ core: tetrabenzoatotetrakis(μ₃-hydroxydi-2-pyridylmethanolato)tetrazinc(II)–acetone–methanol (1/2/1)

D. H. Shin, S.-H. Han, P.-G. Kim, C. Kim and Y. Kim

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Triaqua(2,2′-bipyridine N,N′-dioxide-κ²O,O′)(5-nitrobenzene-1,3-dicarboxylato-κO¹)zinc(II)

H.-J. Lu and F.-M. Wang

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Bis[2-(pyrrolidin-2-yl)-1H-benzimidazole-κ²N²,N³]copper(II) dinitrate dihydrate

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Redetermination of bis(O,O′-diethyl dithiophosphato-κ²S,S′)nickel(II)

D. Paliwoda, J. Chojnacki, A. Mietlarek-Kropidłowska and B. Becker

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Bis[4-(dimethylamino)pyridinium] tetrabromidobis(3,4-dichlorophenyl)stannate(IV)–1-bromo-3,4-dichlorobenzene (1/1)

Y. C. Koon, K. M. Lo and S. W. Ng

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Aquabis(4-nitrobenzoato)-κ²O,O′;κO-(piperidinium-4-carboxylato-κ²O,O′)cadmium(II)

R.-W. Zhang, L.-L. Wang and X.-J. Zhao

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Aquabis(2-amino-1,3-thiazole-4-acetato-κ²O,N³)nickel(II)

Q.-F. He, D.-S. Li, J. Zhao, X.-J. Ke and C. Li

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Dichloridobis(pyridine-2-carboxylato-κ²N,O)platinum(IV) acetonitrile solvate

N.-H. Kim, I.-C. Hwang and K. Ha

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(5,7,7,12,14,14-Hexamethyl-1,4,8,11-tetraazacyclotetradeca-4,11-diene-κ⁴N¹,N⁴,N⁸,N¹¹)(thiocyanato-κS)nickel(II) perchlorate monohydrate

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Bis[1,3(η³)-allyl][μ-2(η⁴)-1,3-bis(diphenylphosphino)-2,4-diphenylcyclobuta-1,3-diene-1:3κ²P:P′]dichlorido-1κCl,3κCl-[2(η⁵)-isopropylcyclopentadienyl]-2-cobalt(I)-1,3-dipalladium(II) dichloromethane solvate

C.-P. Chang and F.-E. Hong

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Bis[μ-2-(2H-benzotriazol-2-yl)-4-methylphenolato]bis[dimethylaluminium(III)]

C.-Y. Li, C.-H. Lin and B.-T. Ko

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catena-Poly[potassium-di-μ-aqua-μ-4-(5-tetrazolio)pyridine]

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Pentaaqua(1H-benzimidazole-5,6-dicarboxylato-κN³)nickel(II) pentahydrate

W.-D. Song, H. Wang, P.-W. Qin, S.-J. Li and S.-W. Hu

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trans-Dichloridobis(4-methoxyaniline-κN)palladium(II)

V. Bon, S. Orysyk and V. Pekhnyo

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2-(3-Pyridinio)benzimidazolium pentachloridoantimonate(III) monohydrate

L.-J. Cui, H.-J. Xu and K.-J. Pan

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Redetermination of tetrakis(N,N-diethyldithiocarbamato)tin(IV)

C. K. Y. A. Okio and N. L. Speziali

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Poly[[aquabis(μ₃-isonicotinato-κ³O:O′:N)tris(μ₂-isonicotinato-κ³O,O′:N)(nitrato-κO)bis(μ₄-oxalato-κ⁶O¹,O²:O²:O^1′,O^2′:O^1′)dierbium(III)tetrasilver(I)] tetrahydrate]

Y.-M. Wen, T.-J. Feng and L.-X. He

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Bis(di-2-pyridylmethanediol-κ³N,O,N′)nickel(II) dinitrate

S. M. Yu, Y. J. Song, K. C. Kim, C. Kim and Y. Kim

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Acta Cryst. (2009). E65, m680
https://doi.org/10.1107/S1600536809018364