Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 65| Part 12

ISSN: 2056-9890

December 2009 issue

Highlighted illustration

Cover illustration: The mixed-valent iron compound [Fe₂(C₂H₅S)₃(C₁₂H₂₁Si)₂] contains an unusual Fe₂S₃ core with a short Fe-Fe distance of 2.7842 (5) Å which is clear evidence of an intermetallic bond. The Fe atoms are coordinated by two substituted cyclopentadienyl ligands with their C₅ planes nearly perpendicular to the Fe-Fe vector and are bridged by three thiolate ligands. Such a diiron-sulfur compound might act as a model structure of active sites in some metalloproteins. See Jing Li [Acta Cryst. (2009). E65, m1542].

inorganic compounds

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Copper(II) hydrogenphosphate, CuHPO₄

C. Günther, H. Görls and D. Stachel

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Sodium scandium diphosphate, NaScP₂O₇, isotypic with α-NaTi(III)P₂O₇

J. Cempírek, R. Škoda and Z. Žák

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Tricaesium dimolybdate(VI) bromide

A. S. Pakhomova and S. V. Krivovichev

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Octarubidium di-μ-sulfato-κ⁴O:O′-bis[cis-dioxido-cis-disulfatotungstate(VI)]

K. Ståhl and R. W. Berg

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catena-Poly[[tetraaquacopper(II)]-μ-trithionato-κ²O:O′]

E. R. T. Tiekink

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Non-isovalent substitution in a Zintl phase with the TiNiSi type structure, CaMg_1–xAg_xGe [x = 0.13 (3)]

C. Banenzoué, S. Ponou and J. N. Lambi

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The type IV polymorph of KEu(PO₃)₄

A. Oudahmane, M. Daoud, B. Tanouti, D. Avignant and D. Zambon

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metal-organic compounds

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Tetra-μ-benzoato-bis{[trans-1-(2-pyridyl)-2-(4-pyridyl)ethylene]zinc(II)}

Y. J. Song, S.-W. Lee, K. H. Jang, C. Kim and Y. Kim

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Diaquabis(2,2′-bi-1H-imidazole-κ²N³,N^3′)nickel(II) bis(3-methylbenzoate) 3-methylbenzoic acid disolvate

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Bis(2,2′-bi-1H-imidazole-κ²N³,N^3′)bis(4-methylbenzoato-κO)copper(II)

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(m-Phenylenedimethylene)bis(triphenylphosphonium) bis[chlorido(pentafluorophenyl)aurate(I)] dichloromethane disolvate

C. E. Strasser, K. Coetzee, S. Cronje and H. G. Raubenheimer

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catena-Poly[[diaquastrontium]-bis(μ-2-bromobenzoato)-κ²O,O′:O′;κ³O:O,O′]

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Bis(μ-2′-carboxylatobiphenyl-2-carboxylic acid-κ²O²:O^2′)bis[(2,2′-bipyridine-κ²N,N′)(2′-carboxylatobiphenyl-2-carboxylic acid-κO^2′)zinc(II)]

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Tetrakis(2-aminopyrazine-κN⁴)dichloridocobalt(II)

W. Kang, L.-H. Huo, S. Gao and S. W. Ng

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Hexaaquacobalt(II) tetraaquabis(2-aminopyrazine-κN⁴)cobalt(II) disulfate dihydrate

W. Kang, L.-H. Huo, S. Gao and S. W. Ng

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Hexaaquamanganese(II) tetraaquabis(2-aminopyrazine-κN⁴)manganese(II) disulfate dihydrate

L.-H. Huo, S. Gao and S. W. Ng

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Aqua{N-[1-(2-oxidophenyl)ethylidene]-L-serinato}copper(II) monohydrate

G.-Q. Zhao, D.-M. Tian, Y.-J. Han, L.-W. Xue and Q.-L. Peng

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Poly[bis[μ-1,4-bis(imidazol-1-yl)butane]dicyanatocadmium(II)]

X. Zhu, Y. Guo and Y.-L. Zou

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Di-μ-chlorido-bis(chlorido{2,2′-[3-(1H-imidazol-4-ylmethyl)-3-azapentane-1,5-diyl]diphthalimide}copper(II))

Z.-P. Qi, A.-D. Wang, H. Zhang and X.-X. Wang

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catena-Poly[[(6,7,9,10,17,18,20,21-octahydro-5,8,11,16,19,22-hexaoxadibenzo[a,j]cyclooctadecene)barium]-di-μ-thiocyanato-[thiocyanatodiaurate(I)(Au—Au)]-μ-thiocyanato]

T. L. Stroud, N. L. Coker and J. A. Krause

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A polymorph of diaquabis(pyrazine-2-carboxylato-κ²N¹,O)copper(II)

G.-H. Wang, R.-L. He, F.-J. Meng, N.-H. Hu and J.-W. Xu

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catena-Poly[[[bis(N,N-dimethylformamide)iron(II)]-{μ-2,2′-bis(diphenylphosphinoyl)-N,N′-[(1R,2R)-cyclohexane-1,2-diyl]dibenzamide}] bis(perchlorate) N,N-dimethylformamide disolvate]

G. R. Ferrell, C. Moore, A. L. Rheingold and C. J. A. Daley

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Tetrakis(quinolin-8-olato-κ²N,O)hafnium(IV) toluene disolvate

J. A. Viljoen, H. G. Visser, A. Roodt and M. Steyn

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Bis(μ-5-nitro-2-oxidobenzoato)bis[triaquazinc(II)]

Q.-S. Li, M. Yin, H. Wei and G.-J. Zhou

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Bis(2-aminothiazole-4-acetato)aquazinc(II)

L.-J. Zhang, X.-C. Shen, Y. Yang and H. Liang

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Bis(dicyanamido-κN¹)bis[2-(2-hydroxyethyl)pyridine-κ²N,O]nickel(II)

L.-Q. Kong, X.-P. Ju and D.-C. Li

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catena-Poly[[[aquasilver(I)]-μ-1,1′-(butane-1,4-diyl)di-1H-imidazole-κ²N³:N^3′] hemi(biphenyl-4,4′-dicarboxylate) dihydrate]

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Bis(quinolin-8-ol)silver(I) 2-hydroxy-3,5-dinitrobenzoate

C.-L. Zhang and F.-F. Jian

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Tris(ethylenediamine)zinc(II) hexafluoridosilicate

Y. Li, Q. Shi, A. M. Z. Slawin, J. D. Woollins and J. Dong

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(μ-5-Carboxy-1H-imidazole-4-carboxylato-κ⁴N¹,O⁵:N³,O⁴)bis[amminesilver(I)]

R.-S. Zhou and J.-F. Song

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Bis(1-ferrocenylmethylidene-4-phenylthiosemicarbazidato-κ²N¹,S)zinc(II) monohydrate

M. R. Vikneswaran, S. G. Teoh, C. S. Yeap and H.-K. Fun

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Diaquabis(N,N′-dibenzylethane-1,2-diamine-κ²N,N′)nickel(II) dichloride N,N-dimethylformamide solvate

Y.-F. Liu, H.-T. Xia, D.-Q. Wang and X.-L. Gong

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Di-μ-iodido-bis[acetyl(4-methyl-2,6,7-trioxa-1-phosphabicyclo[2.2.2]octane)(N-nitroso-N-oxidoaniline-κ²O,O′)rhodium(III)]

J. A. Venter, W. Purcell and H. G. Visser

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Bis(tripyrazol-1-ylmethane)nickel(II) tetracyanidonickelate(II) dihydrate

G. Lyubartseva and S. Parkin

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Di-μ-ethanolato-bis[diethanolato(2-methylquinolin-8-olato)titanium(IV)]

Y. Fazaeli, E. Najafi, M. M. Amini and H. R. Khavasi

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(Benzoato-κO)(benzoic acid-κO)(4,4′-dimethyl-2,2′-bipyridine-κ²N,N′)hydroxidocopper(II) monohydrate

L. Yao and W.-J. Li

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trans-Bis(1-cyclohexylpyrrolidin-2-one)dinitratopalladium(II)

Y. Takahashi and Y. Ikeda

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Bis(2-methyl-1H-imidazole-κN³)silver(I) nitrate dihydrate

F.-D. Cong, F.-Y. Yu, Z. Wei and S. W. Ng

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trans-Dichloridobis[tris(4-methoxyphenyl)phosphine]palladium(II) benzene monosolvate

C. van Blerk and C. W. Holzapfel

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Poly[bis(4,4′-bipyridine)(μ₃-4,4′-dicarboxybiphenyl-3,3′-dicarboxylato)iron(II)]

Q.-H. Meng, H.-L. Lai, H. Lu, Y.-F. Luo and R.-H. Zeng

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[4-(2-Aminoethyl)piperazin-1-ium]trichloridocopper(II) monohydrate

B. Ikram and Z. Fatma

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Tetraguanidinium bis[citrato(3−)]cuprate(II) dihydrate

M. T. M. Al-Dajani, H. H. Abdallah, N. Mohamed, C. S. Yeap and H.-K. Fun

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Tri-μ-ethanethiolato-bis{[η⁵-1,2,3,4-tetramethyl-5-(trimethylsilyl)cyclopentadienyl]iron(II,III)}(Fe^II–Fe^III)

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Poly[aquabis(μ₄-naphthalene-1,4-dicarboxylato)(1,10-phenanthroline-5,6-dione)dimanganese(II)]

F.-D. Cong, F.-Y. Yu, Z. Wei and S. W. Ng

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catena-Poly[[(1,10-phenanthroline-5,6-dione-κ²N,N′)lead(II)]-μ-terephthalato-κ²O¹:O⁴]

F.-D. Cong, F.-Y. Yu, Z. Wei and S. W. Ng

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Tetracarbonylbis(η⁵-cyclopentadienyl)bis[(dec-9-en-1-yl)diphenylphosphine]dimolybdenum(0)(Mo—Mo) tetrahydrofuran disolvate

G. Shultz, L. N. Zakharov and D. R. Tyler

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(3-Allyloxypicolinato-κ²N,O²)bis[3,5-difluoro-2-(2-pyridyl)phenyl-κ²C¹,N]iridium(III)

Y.-L. Zhao and J. Meng

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Hexaaquacobalt(II) bis(4-amino-3-methylbenzenesulfonate)

W. Zhang and Y.-T. Chen

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Hexaaquamagnesium bis(4-amino-3-methylbenzenesulfonate)

W. Zhang and Y.-T. Chen

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catena-Poly[[bis(dimethylformamide-κO)cadmium(II)]-di-μ₂-dicyanamido-κ⁴N¹:N⁵]

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Poly[[tetraaquabis[μ₄-2,2′-(p-phenylenedioxy)diacetato][μ₂-2,2′-(p-phenylenedioxy)diacetato]dierbium(III)] hexahydrate]

D.-Y. Wei, Y.-G. Zhang, M.-L. Wang and Z.-K. Zhu

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catena-Poly[diaquatris(μ₃-biphenyl-2,2-dicarboxylato)disamarium(III)]

D.-Y. Wei, Y.-G. Zhang, M.-L. Wang and Z.-K. Zhu

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Poly[triaqua(μ-butane-1,2,3,4-tetracarboxylato)dicadmium(II)]

C.-H. Ma and Y.-S. Yan

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[4-Carboxyimidazole-5-carboxylato(2–)-κ²N¹,O⁵](5,5,7,12,12,14-hexamethyl-1,4,8,11-tetraazacyclotetradecane-κ⁴N,N′,N′′,N′′′)nickel(II) monohydrate

G.-C. Ou, Q. Zhou and S. W. Ng

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[(Z)-N-Isopropyl-O-methylthiocarbamato-κS](tri-p-tolylphosphine-κP)gold(I)

P. P. Tadbuppa and E. R. T. Tiekink

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[(Z)-O-Methyl-N-propylthiocarbamato-κS](triphenylphosphine-κP)gold(I)

P. P. Tadbuppa and E. R. T. Tiekink

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Tetraaquatetrakis{μ₃-3,3′-[(E,E)-ethane-1,2-diylbis(nitrilomethylidyne)]benzene-1,2-diolato}octazinc(II) N,N-dimethylformamide hexasolvate

Q.-J. Xu, L.-R. Lin, D. Sun, R.-B. Huang and L.-S. Zheng

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catena-Poly[[diaquazinc(II)]-μ-piperazine-1,4-diacetato-κ⁴N¹,O¹:N⁴,O⁴]

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Bis[2-(ethoxycarbonylamino)ethanaminium] hexabromidostannate

R. A. Howie, G. M. de Lima, E. R. T. Tiekink, J. L. Wardell and S. M. S. V. Wardell

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Bis(μ-2,2′-biimidazole-κ²N³:N^3′)bis[aquacopper(I)] sulfate

X. Zhang, P. Wei, B. Hu, B. Li and C. Shi

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trans-Dibromidobis[diphenyl(p-tolyl)phosphine]palladium(II)

L. Kirsten, G. Steyl and A. Roodt

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trans-Dibromidobis[tris(4-chlorophenyl)phosphine]palladium(II)

L. Kirsten and G. Steyl

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Poly[diaquabis(μ₃-1H-benzimidazole-5,6-dicarboxylato-κ⁴N³:O⁵,O^5′:O⁶)bis(μ₂-1H,3H-benzimidazolium-5,6-dicarboxylato-κ³O⁵,O^5′:O⁶)digadolinium(III)]

J.-X. Huang, Y.-Y. Wu, C.-D. Huang, Q.-Y. Lian and R.-H. Zeng

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catena-Poly[diammonium [diaquabis(pyridine-2,4-dicarboxylato-κ²N,O²)cuprate(II)] [[diaquacopper(II)]-μ-pyridine-2,4-dicarboxylato-κ³N,O²:O^2′-[tetraaquacadmium(II)]-μ-pyridine-2,4-dicarboxylato-κ³O²:N,O^2′] hexahydrate]

G.-H. Wang, Z.-G. Li, H.-Q. Jia, N.-H. Hu and J.-W. Xu

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Acta Cryst. (2009). E65, m1570
doi: 10.1107/S1600536809047084