Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 68| Part 6

ISSN: 2056-9890

June 2012 issue

Highlighted illustration

Cover illustration: The compound brusatol, C₂₆H₃₂O₁₁, is a natural product originally isolated from the seeds of Brucea sumatrana. It has also been isolated from the Chinese herbal medicine Brucea javanica and shown to have potent anticancer activity and antiviral activity against the tobaccomosaic virus. It is composed of an [alpha] , [beta] -unsaturated cyclohexanone ring, two cyclohexane rings, a six-membered lactone ring and a tetrahydrofuran ring. An intramolecular O-HO hydrogen bond occurs. In the crystal, O-HO hydrogen bonds link the molecules into helical chains propagating along [010]. See: Hu, Jin, Yu, Tian & Jiang [Acta Cryst. (2012). E68, o1592-o1593].

inorganic compounds

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Wyllieite-type Ag_1.09Mn_3.46(AsO₄)₃

W. Frigui, M. F. Zid and A. Driss

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A novel monoclinic phase of impurity-doped CaGa₂S₄ as a phosphor with high emission intensity

A. Suzuki, T. Takizawa, C. Hidaka, N. Shigetaka and I. Kitajima

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Sodium pentapotassium pentanickel tetra(diphosphate), NaK₅Ni₅(P₂O₇)₄

M. Moutataouia, M. Lamire, M. Saadi and L. El Ammari

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Na₇Mg₁₃Nd(PO₄)₁₂

H. Jerbi, M. Hidouri and B. A. Mongi

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Bis[hexaamminecobalt(III)] pentachloride nitrate

Q. Wu, C. Du, Y. Lv, G. Chen and Q. Pan

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K₂[Fe^II₃(P₂O₇)₂(H₂O)₂]

J. Yang, X. Zhang, B. Liu, W. Sun and Y.-X. Huang

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MnBa₂(HPO₄)₂(H₂PO₄)₂

W. Sun, L.-Z. Sun, T.-T. Zhu, B.-C. Zhao and J.-X. Mi

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Redetermination of Mg₂B₂₅ based on single-crystal X-ray data

L. Bindi, A. Figini Albisetti, G. Giunchi, L. Malpezzi and N. Masciocchi

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KMg_0.09Fe_1.91(PO₄)₂

M. M. Yatskin, I. V. Zatovsky, V. N. Baumer, I. V. Ogorodnyk and N. S. Slobodyanik

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metal-organic compounds

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Bis[2-(2-aminoethyl)-1H-benzimidazole-κ²N²,N³](nitrato-κ²O,O′)cobalt(II) chloride trihydrate

J. Zhao, H. Zhang and G. Zhu

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Bis(2,2′-bipyridyl-κ²N,N′)dichloridorhodium(III) perchlorate

A. Dikhtiarenko, L. Torre-Fernández, S. García-Granda, J. R. García and J. Gimeno

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catena-Poly[[(tetraaquacadmium)-μ-4,4′-bipyridine-κ²N:N′] 4-hydroxy-3-sulfonatobenzoate monohydrate]

S. Gao and S. W. Ng

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Bis(2-trifluoromethyl-1H-benzimidazol-3-ium) tetrachloridomercurate dihydrate

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Dichlorido(5,10,15,20-tetraphenylporphyrinato-κ⁴N)antimony(V) hemi{di-μ-chlorido-bis[trichloridoantimonate(III)]} dichloromethane monosolvate

R. Soury, M. S. Belkhiria, H. Nasri and M. Parvez

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N-(2,6-Diisopropylphenyl)-N-{3-[(2,6-diisopropylphenyl)imino]butan-2-yl}azanide trichloridostannate(II)

X. Ma, S. Sun, P. Hao, Y. Yang and Z. Yang

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catena-Poly[[[diaqua(1,10-phenanthroline-κ²N,N′)cobalt(II)]-μ-4-hydroxy-3-sulfonatobenzoato-κ²O³:O¹] sesquihydrate]

X.-Q. Fang, S. Gao and S. W. Ng

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catena-Poly[[[diaqua(1,10-phenanthroline-κ²N,N′)zinc]-μ-4-hydroxy-3-sulfonatobenzoato-κ²O³:O¹] sesquihydrate]

X.-Q. Fang, S. Gao and S. W. Ng

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catena-Poly[[[bis(acetato-κ²O,O′)aquacadmium]-μ-[(pyridin-3-yl)(pyridin-4-yl)methanone]-κ²N:N′] dihydrate]

Z.-W. Wang, A.-M. Li and Y. Zhang

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Diaquadichloridobis[quinazolin-4(1H)-one-κN³]nickel(II)

S. Shomurotova, K. K. Turgunov, N. Mukhamedov and B. Tashkhodjaev

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Bis{benzyl 2-[4-(4-methoxyphenyl)butan-2-ylidene]hydrazinecarbodithioato-κ²N²,S}nickel(II)

M.-Y. Tan, T. B. S. A. Ravoof, M. I. M. Tahir, K. A. Crouse and E. R. T. Tiekink

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cyclo-Tetrakis{μ-N′-[(8-oxidoquinolin-7-yl)methylidene]isonicotinohydrazidato}tetrazinc tetrahydrate

X.-W. Wu, Q.-L. Li, J.-P. Ma and Y.-B. Dong

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catena-Poly[[(2,9-dimethyl-1,10-phenanthroline-κ²N,N′)lead(II)]-di-μ-bromido]

B. Sabour, E. Najafi, M. M. Amini and S. W. Ng

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(μ-Naphthalene-1,5-disulfonato-κ²O¹:O⁵)bis[triaqua(glycinato-κ²N,O)copper(II)]

S. Gao and S. W. Ng

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Bis(3,5-di-tert-butyl-4H-1,2,4-triazol-4-amine-κN¹)(nitrato-κO)silver(I) ethanol monosolvate monohydrate

Y.-M. Liu, J.-H. Chen, G. Yang and S. W. Ng

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2-[(Propan-2-yloxy)carbonyl]quinolin-1-ium tetrachlorido(quinoline-2-carboxylato-κ²N,O)stannate(IV)

E. Najafi, M. M. Amini and S. W. Ng

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A triclinic polymorph of poly[[bis[μ-1,2-bis(pyridin-4-yl)ethene-κ²N:N′]bis(thiocyanato-κN)cobalt(II)] 1,2-bis(pyridin-4-yl)ethene monosolvate]

S. Wöhlert, I. Jess and C. Näther

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Bis[(E)-N-(pyridin-3-ylmethylidene)hydroxylamine-κN¹]silver(I) perchlorate

J. Xu, S. Gao, S. W. Ng and E. R. T. Tiekink

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(Acetylacetonato-κ²O,O′)carbonyl[dicyclohexyl(2,6-diisopropylphenyl)phosphane-κP]rhodium(I)

W. L. Davis, S. D. Mathobela and R. Meijboom

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8-Hydroxy-2-methylquinolinium tetrachlorido(quinolin-8-olato-κ²N,O)stannate(IV)

E. Najafi, M. M. Amini and S. W. Ng

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Tris(5,6-dimethyl-1H-benzimidazole-κN³)(pyridine-2,6-dicarboxylato-κ³O²,N,O⁶)nickel(II)

Y.-H. Li, F.-F. Li, X.-H. Liu and L.-Y. Zhao

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Tris(1H-benzimidazole-κN³)(pyridine-2,6-dicarboxylato-κ³O²,N,O⁶)nickel(II)

Y.-H. Li, F.-F. Li, X.-H. Liu and L.-Y. Zhao

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[Bis(pyridin-2-ylmethyl)amine-κ³N,N′,N′′]tricarbonylrhenium(I) bromide hemihydrate

M. Schutte, T. J. Muller, H. G. Visser and A. Roodt

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10-Hydroxybenzo[h]quinolin-1-ium tetrachlorido(pyridine-2-carboxylato-κ²N,O)stannate(IV) methanol monosolvate

E. Najafi, M. M. Amini and S. W. Ng

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4-(Dimethylamino)pyridinium tetrachlorido(pyridine-2-carboxylato-κ²N,O)stannate(IV)

E. Najafi, M. M. Amini and S. W. Ng

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Bis(dicyanamido-κN)tetrakis(pyridine-κN)nickel(II)

S. Wöhlert, M. Wriedt, I. Jess and C. Näther

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Triaqua-1κO,2κ²O-bis(2,2′-bipyridine)-1κ²N,N′;2κ²N,N′-chlorido-1κCl-μ-terephthalato-1:2κ²O¹:O⁴-dicopper(II) nitrate monohydrate

Y. Liu, Y.-L. Feng and D.-Z. Kuang

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N,N′-Dibutyl-N,N,N′,N′-tetramethylethane-1,2-diaminium μ-oxido-bis[trichloridoferrate(III)]

S. M. Närhi, J. Kostamo, J. Asikkala, R. Oilunkaniemi and R. S. Laitinen

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Lithium bis(2-methyllactato)borate monohydrate

J. L. Allen, E. Paillard, P. D. Boyle and W. A. Henderson

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catena-Poly[[(1,10-phenanthroline-κ²N,N′)zinc]-μ-furan-2,5-dicarboxylato-κ⁴O²,O^2′:O⁵,O^5′]

Y.-F. Li, Y. Xu, X.-L. Qin, W.-Y. Gao and Y. Gao

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Poly[chlorido[μ₄-2,2′-(2-methyl-1H-benzimidazol-3-ium-1,3-diyl)diacetato]zinc]

J.-Q. Liu, Z.-J. Jiang, Z.-H. Xu and Y. Zhang

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{4,4′,6,6′-Tetraiodo-2,2′-[2,2-dimethylpropane-1,3-diylbis(nitrilomethanylylidene)]diphenolato}copper(II)

H. Kargar, R. Kia, T. Shakarami and M. N. Tahir

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{4,4′,6,6′-Tetrabromo-2,2′-[2,2-dimethylpropane-1,3-diylbis(nitrilomethanylylidene)]diphenolato}nickel(II)

H. Kargar, R. Kia and M. N. Tahir

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Diaquabis{1-[(1H-benzimidazol-2-yl)methyl]-1H-imidazole-κN³}dichloridocadmium hexahydrate

X.-N. Xie, M. Lu, J. Yuan and H.-X. Yang

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Poly[(μ₃-benzene-1,3-dicarboxylato-κ⁴O¹:O^1′:O³,O^3′)bis(pyridine-κN)cobalt(II)]

F. Xie, D. Zhang and X. Zhang

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Di-μ-iodido-bis[(dimethyl 2,2′-biquinoline-4,4′-dicarboxylate-κ²N,N′)copper(I)]

R. Starosta, U. K. Komarnicka, J. Nagaj, K. Stokowa-Sołtys and A. Bykowska

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Tris[(2E)-1,3-bis(4-chlorophenyl)triaz-2-en-1-ido-κ²N¹,N³]cobalt(III)

G. Yu, S.-Z. Zhan and S. W. Ng

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A new dabco-templated metal sulfate: 1,4-diazoniabicyclo[2.2.2]octane hexaaquacadmium bis(sulfate)

B.-Q. Wang, H.-B. Yan, C.-J. Fang and Z. Zhang

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9-Aminoacridinium bis(pyridine-2,6-dicarboxylato-κ³O²,N,O⁶)ferrate(III) tetrahydrate

M. Mirzaei, H. Eshtiagh-Hosseini, E. Eydizadeh, Z. Yousefi and K. Molčanov

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catena-Poly[[diaquanickel(II)]-bis(μ-2-{[5-(pyridin-4-yl)-1,3,4-oxadiazol-2-yl]sulfanyl}acetato)]

R.-Q. Gao, C.-H. Xia and G.-T. Li

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Bis{N²,N⁶-bis[(pyridin-3-yl)methyl]pyridine-2,6-dicarboxamide-κN}bis(methanol-κO)bis(thiocyanato-κN)cobalt(II)

G.-R. Yang, J. Ren and G.-T. Li

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[2-Formyl-4-methyl-6-({2-[2-(4-nitrobenzylamino)ethylamino]ethylimino}methyl)phenolato]nickel(II) perchlorate

Y. Wang, J.-W. Mao, H.-T. Song and H. Zhou

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Bis(2-aminomethyl-1H-benzimidazole-κ²N²,N³)bis(nitrato-κO)copper(II)

J. Zhao, H. Zhang, X. Zhai and G. Zhu

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Poly[[(methanol)(μ₄-2,4,5,6-tetrafluorobenzene-1,3-dicarboxylato)copper(II)] methanol monosolvate]

D. Yan and Q. Duan

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catena-Poly[[tetrakis(hexamethylphosphoramide-κO)bis(nitrato-κ²O,O′)lutetium(III)] [silver(I)-di-μ-sulfido-tungstate(VI)-di-μ-sulfido]]

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Bis(2-amino-5-methyl-1,3,4-thiadiazole-κN³)dichloridocobalt(II)

Y. Song, Y.-F. Ji, M.-Y. Kang and Z.-L. Liu

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[4,6-Dimethylpyrimidine-2(1H)-thione-κS]iodidobis(triphenylphosphane-κP)copper(I)

C. Pakawatchai, Y. Wattanakanjana, P. Choto and R. Nimthong

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Bis(acetato-κ²O,O′)(4,4′-dimethyl-2,2′-bipyridine-κ²N,N′)copper(II) monohydrate

A. Kaewthong, M. Sukwattanasinitt and N. Muangsin

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catena-Poly[cadmium-μ-[1,3-bis(imidazol-1-yl)propane]-di-μ-chlorido]

Q.-L. Shen and H. Lin

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Bis(4′-chloro-2,2′:6′,2′′-terpyridine-κ³N,N′,N′′)ruthenium(II) dichloride dihydrate

Y. Wang, R. Jiao, X.-L. Qiu, J. Wang and W. Huang

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Bis(2,S-dimethyldithiocarbazate-κ²N³,S)(nitrato-κO)copper(II) nitrate

S. K. S. Hazari, B. K. Dey, B. Ganguly, S. W. Ng and E. R. T. Tiekink

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Tris(2-acetylcyclopentan-1-onato-κ²O,O′)aluminium

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Tetrakis(4-chloroanilinium) hexachloridostannate(IV) dichloride

B. Zhou and H. Liu

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Aqua[6-carboxylato-N′-(pyridin-2-ylmethylidene)pyridine-2-carbohydrazidato]copper(II) trihydrate

Y.-M. Huang, W.-S. Wu and X.-Y. Wang