Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 67| Part 9

ISSN: 2056-9890

September 2011 issue

Highlighted illustration

Cover illustration: Polynuclear iron(II/III) clusters containing an Fe-O-Fe linkage are simple and useful model compounds for non-heme metalloproteins containing dinuclear iron units in their active sites. The mixed-valent ionic title compound, tris(1,10-phenanthroline)iron(II) [mu] -oxido-bis[trichloridoferrate(III)], contains a complex [Fe^II(phen)₃]²⁺ cation and a dinuclear Cl₃Fe^III--Fe^IIICl₃ anion composed of two condensed FeOCl₃ tetrahedra with a bent bridging angle of 158.4 (3)°. The packing of the crystal structure is consolidated by intermolecular C-HCl interactions. See Ling, Song & Wang [Acta Cryst. (2011). E67, m1232-m1233].

inorganic compounds

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Reinvestigation of the low-temperature form of Ag₂Se (naumannite) based on single-crystal data

J. Yu and H. Yun

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Manganese(II) octauranium(IV) heptadecasulfide

G. N. Oh and J. A. Ibers

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Redetermination of despujolsite, Ca₃Mn⁴⁺(SO₄)₂(OH)₆·3H₂O

M. C. Barkley, H. Yang, S. H. Evans, R. T. Downs and M. J. Origlieri

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The mixed-valent titanium phosphate, Li₂Ti₂(PO₄)₃, dilithium dititanium(III/IV) tris(orthophosphate)

Y. Kee, S.-S. Lee and H. Yun

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A new mixed group 5 metal selenide, Nb_1.41V_0.59Se₉

E. Lee and H. Yun

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metal-organic compounds

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Tetraaquabis(2-methyl-1H-benzimidazolium-1,3-diacetato-κO)cobalt(II) tetrahydrate

X.-L. Feng and Y.-P. Zhang

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(4,5-Diazafluoren-9-one-κ²N,N′)bis(1H-imidazole-κN³)bis(thiocyanato-κN)cobalt(II)

X.-L. Feng and Y.-P. Zhang

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catena-Poly[[bis(N,N-dimethylformamide-κO)zinc]-μ₂-oxalato-κ⁴O¹,O²:O^1′,O^2′]

J. E. Lee and H.-I. Lee

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{2,2′-[(2,2-Dimethylpropane-1,3-diyldinitrilo)bis(phenylmethylidyne)]diphenolato}nickel(II)

H. Kargar, R. Kia, M. Moghadam, F. Froozandeh and M. N. Tahir

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catena-Poly[[aqua[1,4-bis(1H-imidazol-4-yl)benzene]cadmium]-μ₃-5-methylisophthalato]

S.-L. Yang, D.-H. Wang and S.-S. Chen

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Ethylenediammonium tetraaquadisulfatocadmate

W. Rekik, H. Naïli, T. Mhiri and T. Bataille

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Poly[[{μ₃-2-[4-(2-hydroxyethyl)piperazin-1-yl]ethanesulfonato}silver(I)] trihydrate]

S. M. Bilinovich, M. J. Panzner, W. J. Youngs and T. C. Leeper

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Di-μ-chlorido-bis{[4-amino-3,5-bis(2-pyridyl)-4H-1,2,4-triazole-κN¹]chloridomercury(II)}

J. Guo, M. Tang, J. Chen and C.-P. Li

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Aqua(2,9-dimethyl-1,10-phenanthroline-κ²N,N′)diformato-κ²O,O′;κO-nickel(II) monohydrate

P. Xia, J.-L. Lin and S.-L. Ni

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(2-{[2-(1H-Benzimidazol-2-yl-κN³)phenyl]iminomethyl-κN}-5-methylphenolato-κO)chloridozinc(II)

N. E. Eltayeb, S. G. Teoh, S. Chantrapromma and H.-K. Fun

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Bis(η⁵-1-tert-butylindenyl)nickel(II)

H. Bauer, Y. Sun and H. Sitzmann

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μ-Acetato-diacetato{μ-6,6′-dimethoxy-2,2′-[o-phenylenebis(nitrilomethanylylidene)]diphenolato}gadolinium(III)zinc

F. Yang, G.-M. Li, P. Chen, P.-F. Yan and G.-F. Hou

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trans-Diaquabis[5-carboxy-2-(3-pyridyl)-1H-imidazole-4-carboxylato-κ²N³,O⁴]cobalt(II)

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[6-(4-Bromophenyl)-2,2′-bipyridine-κ²N,N′]bis(triphenylphosphane-κP)copper(I) tetrafluoridoborate

Y.-R. Lin, J.-S. Huang and M.-H. Zhong

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Diaquatris[4,4,4-trifluoro-3-oxo-1-(thiophen-2-yl)but-1-en-1-olato]neodymium(III) acetonitrile monosolvate

P. S. Barber and A. de Bettencourt-Dias

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Bis(chloroacetato-κO)bis(trimethylsilylmethyl)tin(IV)

R.-F. Ding and Q.-B. Wang

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Di-μ-but-2-enoato-bis[diaquabis(but-2-enoato)neodymium(III)] 2,6-diaminopurine disolvate

A. M. Atria, A. Astete, M. T. Garland and R. Baggio

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Dichloridobis[2-methylsulfanyl-4-(pyridin-2-yl)pyrimidine-κ²N³,N⁴]cobalt(II)

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Hexaaquamagnesium bis(3-carboxy-4-hydroxybenzenesulfonate) dihydrate

G. Smith, U. D. Wermuth and M. L. Williams

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Poly[[tetraaquabis(μ₃-pyridine-2,6-dicarboxylato)(μ₂-pyridine-2,6-dicarboxylato)dilanthanum(III)] dihydrate]

S. F. Lush and F. M. Shen

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μ-Bromido-bis{μ-2,2′-[4,7-diazadecane-1,10-diylbis(nitrilomethanylylidene)]diphenolato}tricopper(II) bromide dimethylformamide disolvate

G. Assey, R. J. Butcher and Y. Gultneh

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Bis[3,5-difluoro-2-(4-methylpyridin-2-yl)phenyl-κ²C¹,N](picolinato-κ²N,O)iridium(III) chloroform monosolvate

Y.-I. Kim, H.-J. Seo, S.-J. Yun, Y.-K. Song, I.-C. Kim and S. K. Kang

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catena-Poly[[bis[[bis(3-aminopropyl)amine-κ³N,N′,N′′](thiocyanato-κN)cadmium]-μ₄-sulfato-κ⁴O,O:O′,O′] methanol hemisolvate]

J. Boeckmann and C. Näther

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Bis[2-(2-aminoethylamino)ethanol]copper(II) dinitrate

R. Azadbakht, H. Amiri Rudbari and G. Bruno

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trans-Diaquabis(DL-valinato-κ²N,O)nickel(II)

A. Messai, R. Benali-Cherif, E. Jeanneau and N. Benali-Cherif

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trans-Dibromidobis(1-ethyl-3-methylimidazol-2-ylidene)palladium(II)

S. R. Madsen, N. Lock, J. Overgaard and B. B. Iversen

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catena-Poly[[tetrakis(hexamethylphosphoramide-κO)bis(nitrato-κ²O,O′)yttrium(III)] [silver(I)-di-μ-sulfido-molybdenum(VI)-di-μ-sulfido]]

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Bis[4-(1-iminoethyl)-3-methyl-1-phenyl-1H-pyrazol-5-olato-κ²O,N⁴]copper(II)

H. Zhu, Z. Wang, Z. Wei, Y. Bai and X. Xv

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Diaquabis(4-bromobenzoato-κO)bis(N,N-diethylnicotinamide-κN¹)manganese(II)

H. Necefoğlu, F. E. Özbek, V. Öztürk, V. Adıgüzel and T. Hökelek

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Bis{2-[(2-hydroxy-2-methylpropyl)iminomethyl]-4-nitrophenolato}nickel(II) dimethylformamide monosolvate

K. Ayikoé, Y. Gultneh and R. J. Butcher

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{μ-6,6′-Dimethoxy-2,2′-[butane-1,4-diylbis(nitrilomethanylylidene)]diphenolato}trinitratocopper(II)samarium(III)

J.-C. Xing, B. Zhang, W.-Z. Li and X.-G. Cui

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Dichloridotetrakis(diniconazole)nickel(II)

Z.-Q. Xiong, X.-Y. Song and X.-L. Nie

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Dichloridotetrakis(diniconazole)cobalt(II)

C.-X. Liu, X.-Y. Song, Q. Liu, X.-L. Nie and S.-H. Wen

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Bis(1,10-phenanthroline-κ²N,N′)(sulfato-O)copper(II) ethane-1,2-diol monosolvate

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Bis[bis(diphenylphosphinoyl)acetonitrile-κ²O,O′]copper(II)

S. V. Sithole, R. J. Staples and W. E. Van Zyl

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Poly[di-μ-glycinato-copper(II)]: a two-dimensional coordination polymer

F. Gschwind and M. Jansen

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Aqua{6,6′-diethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethanylylidene)]diphenolato}zinc

C.-Y. Wang, X. Wu, J.-J. Hu and Z.-P. Han

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catena-Poly[[[bis(3-aminopyrazine-2-carboxylato)triaquapraseodymium(III)]-μ-3-aminopyrazine-2-carboxylato-[(3-aminopyrazine-2-carboxylato)diaquaformatopraseodymium(III)]-μ-3-aminopyrazine-2-carboxylato] hexahydrate]

S. Gao and S. W. Ng

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10-Hydroxybenzo[h]quinolinium tetrachlorido(2-methylquinolin-8-olato-κ²N,O)stannate(IV) methanol disolvate

E. Najafi, M. Vafaee, M. M. Amini and S. W. Ng

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4-(Dimethylamino)pyridinium tetrachlorido(quinoline-2-carboxylato-κ²N,O)stannate(IV)

E. Najafi, M. M. Amini and S. W. Ng

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(Pentafluoropropionato-κO)tetrakis(trimethylphosphine oxide-κO)copper(II) pentafluoropropionate

I. B. Szymańska and L. Dobrzańska

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Bis{4-bromo-2-[(2-hydroxyethyl)iminomethyl]phenolato}nickel(II) monohydrate

C.-Y. Wang, J.-F. Li, P. Wang and C.-J. Yuan

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Bis{4-chloro-2-[(2-hydroxyethyl)iminomethyl]phenolato}nickel(II) monohydrate

C.-Y. Wang, J.-Y. Ye, X. Wu and Z.-P. Han

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Dibromido(2,3-di-2-pyridylpyrazine-κ²N¹,N²)platinum(II)

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(η⁶-Isopropyl N-phenylcarbamate)(η⁵-pentamethylcyclopentadienyl)ruthenium(II) tetraphenylborate acetone monosolvate

B. T. Loughrey, M. L. Williams and P. C. Healy

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Tris(1,10-phenanthroline)iron(II) μ-oxido-bis[trichloridoferrate(III)]

C. Ling, L. Song and X. Wang

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Tetrakis(μ-2-phenoxypropionato)-κ³O,O′:O′;κ³O:O,O′;κ⁴O:O′-bis[(1,10-phenanthroline-κ²N,N′)(2-phenoxypropionato-κ²O,O′)terbium(III)]

J.-B. Shen, J.-L. Liu and G.-L. Zhao

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catena-Poly[[tetrakis(μ-pentafluorobenzoato-κ²O:O′)dimolybdenum(II)]-μ-4,4′-bipyridine-κ²N:N′]

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Poly[(μ₆-6-oxidopyridinium-2-carboxylato)caesium]

S. K. Kang and Y. S. Shim

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Diacetato-κO;κ²O,O′-aqua(2,4,6-tri-2-pyridyl-1,3,5-triazine-κ³N²,N¹,N⁶)manganese(II) monohydrate

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Tetrakis(picolinato-κ²N,O)zirconium(IV) dihydrate

M. Steyn, H. G. Visser, A. Roodt and T. J. Muller

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Bis(1-benzyl-3-methylimidazolium-κC²)mercury(II) bis(hexafluoridophosphate)

R. A. Haque, A. W. Salman, M. Hemamalini and H.-K. Fun

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Diaqua(5-carboxybenzene-1,3-dicarboxylato-κ²O¹,O^1′)(6,6′-dimethyl-2,2′-bipyridine-κ²N,N′)nickel(II) heptahydrate

W.-W. Shan, H.-L. Xiong and C.-Z. Mei

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8-Hydroxy-2-methylquinolinium tetrachlorido(pyrazine-2-carboxylato-κ²N¹,O²)stannate(IV) methanol monosolvate

M. Vafaee, E. Najafi, M. M. Amini and S. W. Ng

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Di-μ-acetato-κ³O,O′:O′;κ³O:O,O′-bis[(acetato-κ²O,O′)bis(5-nitro-1,10-phenanthroline-κ²N,N′)cadmium]

F. Cui and S. Zhang

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Poly[diaqua(μ-4,4′-bipyridine-κ²N:N′)[μ-2,2′-(p-phenylenedioxy)diacetato-κ²O:O′]cadmium]

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catena-Poly[[aquabis(N⁶-benzyladenine-κN³)copper(II)]-μ-benzene-1,4-dicarboxylato-κ²O¹:O⁴]

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Tetraaqua{1-[(1H-1,2,3-benzotriazol-1-yl)methyl]-1H-1,2,4-triazole}sulfatocadmium dihydrate

Y. Li, D. Li and D. Zhao

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Acta Cryst. (2011). E67, m1252
doi: 10.1107/S1600536811032764